CN106283614A - Negative oxygen ion finishing agent and preparation method thereof - Google Patents
Negative oxygen ion finishing agent and preparation method thereof Download PDFInfo
- Publication number
- CN106283614A CN106283614A CN201610655163.2A CN201610655163A CN106283614A CN 106283614 A CN106283614 A CN 106283614A CN 201610655163 A CN201610655163 A CN 201610655163A CN 106283614 A CN106283614 A CN 106283614A
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- China
- Prior art keywords
- finishing agent
- oxygen ion
- negative oxygen
- suspension
- ammonia
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
- D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
- D06M11/60—Ammonia as a gas or in solution
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of anionic finishing agent, it includes tourmaline powder 10 ~ 20, ammonia 2 ~ 4, dispersant 1 ~ 3, water 75 ~ 85 by weight percentage.Negative oxygen ion finishing agent, its preparation method is first to take dispersant to be added to the water and be sufficiently stirred for dissolving, then is added thereto by tourmaline powder and stirs；The mixed liquor obtained adds the sand mill of a diameter of 0.3 ~ 0.5mm of zirconium pearl, and the suspension that corase grind obtains adds the sand mill of a diameter of 0.1 ~ 0.3mm of zirconium pearl, adds ammonia, and fine grinding obtains negative oxygen ion finishing agent.The generation efficiency accelerating anion of the present invention, thus reach high-negative ion amount, and the suspension system of finishing agent is the most stable.
Description
Technical field
The present invention relates to a kind of finishing agent, particularly to negative oxygen ion finishing agent and preparation method thereof.
Background technology
Modern study shows, negative aeroion not only has plurality of health care functions to human body, and to a lot of diseases
Also has auxiliary therapeutic action.It is mainly manifested in: regulate body fluid Acidity of Aikalinity, raising Immunoresistance, treatment respiratory tract disease, delay
Solve pain, oxygen-derived free radicals Non-toxic.Negative aeroion also has depositing dust, antibacterial, degerming and deodorization etc. and purifies the function of air,
It is called " air vitamin " or " long-living element ".There is the textile much rich in negative oxygen ion function at present, but this type of has spun
The weak effect producing negative oxygen ion of fabric, in air, negative oxygen ion content is few, especially the preparation side of negative oxygen ion finishing agent
Method, there is presently no method the most easily.
Summary of the invention
In order to overcome drawbacks described above, the invention provides a kind of negative oxygen ion finishing agent and preparation method thereof, the present invention is led to
Cross techniques below scheme to realize:
Anionic finishing agent, it includes following component by weight percentage:
Tourmaline powder 10 ~ 20, ammonia 2 ~ 4, dispersant 1 ~ 3, water 75 ~ 85.
Described dispersant is PEG4000.
Negative oxygen ion finishing agent, its preparation method is: comprise the following steps,
(1) the most first take dispersant to be added to the water and be sufficiently stirred for dissolving, then tourmaline powder is added thereto stirring all
Even；
(2) mixed liquor step (1) obtained adds the sand mill of a diameter of 0.3 ~ 0.5mm of zirconium pearl, roughly grinds 2 ~ 4h, and temperature controls
Between 40 DEG C-50 DEG C, obtain the particle diameter suspension at 300 ~ 800nm；
(3) suspension step (2) obtained adds the sand mill of a diameter of 0.1 ~ 0.3mm of zirconium pearl, adds ammonia, refines 0.5-
1h, temperature controls, between 5 DEG C-10 DEG C, to obtain the suspension of particle diameter≤200nm, is negative oxygen ion finishing agent.
Beneficial effects of the present invention:
One, anion needs tourmaline could produce the common effect of oxygen and water, and the steam in air only has 1.3%, because of
This is by the fabric of finishing technique, and water is the key factor of restriction anion generation amount.The present invention selects PEG4000 as dispersion
Agent, owing to it has hydrophilic, therefore can be gathered in fabric face by the hydrone in air endlessly, so this is just
Accelerate the generation efficiency of anion, thus reach high-negative ion amount.
Two, the Acidity of Aikalinity of finishing agent of the present invention can not collide, and its ZETA current potential also requires that it is of the same race, otherwise will send out
Raw gathering and sedimentation.Finishing agent is alkalescence in the present invention, and ZETA current potential is negative value, and PEG4000 is non-ionic dispersing agent.Separately
Outward, ammonia is as a kind of weakly alkaline solution, and its effect is alkali tune, increases system pH value.In the case of pH value is the biggest, it
ZETA current potential absolute value is the biggest.And ZETA current potential absolute value is the biggest, system is the most stable, when the finishing agent of the making of the present invention is deposited
Between can reach 3 to 4 days, can take at any time during this period.
Detailed description of the invention
Embodiment 1
Take 10 parts of tourmaline powders by weight percentage, 4 parts of ammonia, the ammonia concentration that i.e. industry is conventional 25% ~ 28% ammonia, 1
Part PEG40001 ~ 3,85 parts of water.
(1) first PEG4000 is added to the water and is sufficiently stirred for dissolving, then tourmaline powder is added thereto stirs；
(2) mixed liquor step (1) obtained adds the sand mill of a diameter of 0.5mm of zirconium pearl, roughly grinds 4h, temperature 40 DEG C, obtains
Particle diameter is at the suspension of 800nm；
(3) suspension step (2) obtained adds the sand mill of a diameter of 0.2mm of zirconium pearl, adds ammonia, refines 1h, temperature
Control between 5 DEG C, obtain the particle diameter suspension at 200nm, be negative oxygen ion finishing agent.
The finishing agent resting period that the present embodiment obtains is 4 days, during this period, and the tourmaline powder in finishing agent suspension
Will not reunite.The negative oxygen ion burst size of the fabric arranged through the present embodiment finishing agent is 20000 ion/cm3。
Embodiment 2
Take 15 parts of tourmaline powders by weight percentage, 3 parts of ammonia, the ammonia concentration that i.e. industry is conventional 25% ~ 28% ammonia, 2
Part PEG4000,80 parts of water.
(1) first PEG4000 is added to the water and is sufficiently stirred for dissolving, then tourmaline powder is added thereto stirs；
(2) mixed liquor step (1) obtained adds the sand mill of a diameter of 0.4mm of zirconium pearl, roughly grinds 3h, and temperature controls at 45 DEG C
Between, obtain the particle diameter suspension at 500nm；
(3) suspension step (2) obtained adds the sand mill of a diameter of 0.3mm of zirconium pearl, adds ammonia, refines 0.8h, temperature
Degree controls between 7 DEG C, obtains the particle diameter suspension at 200nm, is negative oxygen ion finishing agent.
The finishing agent resting period that the present embodiment obtains is 4 days, during this period, and the tourmaline powder in finishing agent suspension
Will not reunite.The negative oxygen ion burst size of the fabric arranged through the present embodiment finishing agent is 20000 ion/cm3。
Embodiment 3
Take 20 parts of tourmaline powders by weight percentage, 2 parts of ammonia, the ammonia concentration that i.e. industry is conventional 25% ~ 28% ammonia, 3
Part PEG4000,75 water.
(1) first PEG4000 is added to the water and is sufficiently stirred for dissolving, then tourmaline powder is added thereto stirs；
(2) mixed liquor step (1) obtained adds the sand mill of a diameter of 0.3mm of zirconium pearl, roughly grinds 2h, and temperature controls at 50 DEG C
Between, obtain the particle diameter suspension at 300nm；
(3) suspension step (2) obtained adds the sand mill of a diameter of 0.1mm of zirconium pearl, adds ammonia, refines 0.5h, temperature
Degree controls, between 10 DEG C, to obtain the suspension of particle diameter 180nm, is negative oxygen ion finishing agent.
The finishing agent resting period that the present embodiment obtains is 3 days, during this period, and the tourmaline powder in finishing agent suspension
Will not reunite.The negative oxygen ion burst size of the fabric arranged through the present embodiment finishing agent is 30000 ion/cm3。
Claims (3)
1. anionic finishing agent, it includes following component by weight percentage:
Tourmaline powder 10 ~ 20, ammonia 2 ~ 4, dispersant 1 ~ 3, water 75 ~ 85.
Anionic finishing agent the most according to claim 1, it is characterised in that: described dispersant is PEG4000.
3., according to the negative oxygen ion finishing agent described in any one of claim 1 or 2, its preparation method is: comprise the following steps,
(1) the most first take dispersant to be added to the water and be sufficiently stirred for dissolving, then tourmaline powder is added thereto stirring all
Even；
(2) mixed liquor step (1) obtained adds the sand mill of a diameter of 0.3 ~ 0.5mm of zirconium pearl, roughly grinds 2 ~ 4h, and temperature controls
Between 40 DEG C-50 DEG C, obtain the particle diameter suspension at 300 ~ 800nm；
(3) suspension step (2) obtained adds the sand mill of a diameter of 0.1 ~ 0.3mm of zirconium pearl, adds ammonia, refines 0.5-
1h, temperature controls, between 5 DEG C-10 DEG C, to obtain the suspension of particle diameter≤200nm, is negative oxygen ion finishing agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610655163.2A CN106283614A (en) | 2016-08-11 | 2016-08-11 | Negative oxygen ion finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610655163.2A CN106283614A (en) | 2016-08-11 | 2016-08-11 | Negative oxygen ion finishing agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106283614A true CN106283614A (en) | 2017-01-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610655163.2A Pending CN106283614A (en) | 2016-08-11 | 2016-08-11 | Negative oxygen ion finishing agent and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107164946A (en) * | 2017-05-25 | 2017-09-15 | 海盐派特普科技有限公司 | A kind of clothing anion finishing liquor |
| CN111019412A (en) * | 2019-12-25 | 2020-04-17 | 孙波 | Method for preparing liquid capable of generating negative oxygen ions |
| CN111286803A (en) * | 2019-02-01 | 2020-06-16 | 上海依欧实业发展有限公司 | Polylactic acid anion fiber and preparation method thereof |
| CN116751422A (en) * | 2023-08-16 | 2023-09-15 | 广州海天塑胶有限公司 | Negative ion polypropylene composite polymer material for automobile and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1473759A (en) * | 2002-08-07 | 2004-02-11 | 上海弘康科技发展有限公司 | Method for producing superfine white tourmaline powder |
| CN1563228A (en) * | 2004-04-14 | 2005-01-12 | 郭顺开 | Environmental protection type negative ion coating material and fabricating method |
| CN1724145A (en) * | 2005-06-30 | 2006-01-25 | 复旦大学 | Nano Titanium dioxide/fluorite photocataly tic material and preparation process thereof |
| CN101525836A (en) * | 2009-04-08 | 2009-09-09 | 无锡泰达纺织科技有限公司 | Method for preparing nanometer antibacterial anionic finishing agent |
-
2016
- 2016-08-11 CN CN201610655163.2A patent/CN106283614A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1473759A (en) * | 2002-08-07 | 2004-02-11 | 上海弘康科技发展有限公司 | Method for producing superfine white tourmaline powder |
| CN1563228A (en) * | 2004-04-14 | 2005-01-12 | 郭顺开 | Environmental protection type negative ion coating material and fabricating method |
| CN1724145A (en) * | 2005-06-30 | 2006-01-25 | 复旦大学 | Nano Titanium dioxide/fluorite photocataly tic material and preparation process thereof |
| CN101525836A (en) * | 2009-04-08 | 2009-09-09 | 无锡泰达纺织科技有限公司 | Method for preparing nanometer antibacterial anionic finishing agent |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107164946A (en) * | 2017-05-25 | 2017-09-15 | 海盐派特普科技有限公司 | A kind of clothing anion finishing liquor |
| CN111286803A (en) * | 2019-02-01 | 2020-06-16 | 上海依欧实业发展有限公司 | Polylactic acid anion fiber and preparation method thereof |
| CN111019412A (en) * | 2019-12-25 | 2020-04-17 | 孙波 | Method for preparing liquid capable of generating negative oxygen ions |
| CN116751422A (en) * | 2023-08-16 | 2023-09-15 | 广州海天塑胶有限公司 | Negative ion polypropylene composite polymer material for automobile and preparation method thereof |
| CN116751422B (en) * | 2023-08-16 | 2023-11-03 | 广州海天塑胶有限公司 | Negative ion polypropylene composite polymer material for automobile and preparation method thereof |
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Application publication date: 20170104 |
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