CN101705579A - Anti-electrostatic antibiotic non-woven fabric, preparation process thereof and mask made of same - Google Patents
Anti-electrostatic antibiotic non-woven fabric, preparation process thereof and mask made of same Download PDFInfo
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- CN101705579A CN101705579A CN200910110331A CN200910110331A CN101705579A CN 101705579 A CN101705579 A CN 101705579A CN 200910110331 A CN200910110331 A CN 200910110331A CN 200910110331 A CN200910110331 A CN 200910110331A CN 101705579 A CN101705579 A CN 101705579A
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Abstract
The invention relates to an anti-electrostatic antibiotic non-woven fabric, a preparation process thereof and a mask made of the same. The anti-electrostatic antibiotic non-woven fabric is prepared from the following components: 60-98 parts of polypropylene, 1-20 parts of antimicrobial agent and 1-20 parts of master batch. The preparation method of the anti-electrostatic antibiotic non-woven fabric comprises the following steps: preparing raw materials: providing 60-98 parts of polypropylene, 1-20 parts of master batch and 1-20 parts of antimicrobial agent for preparing silver-loaded zirconium phosphate or silver-loaded zeolite; and forming the raw materials into the anti-electrostatic antibiotic non-woven fabric by a non-woven fabric preparation process. The anti-electrostatic antibiotic mask comprises a mask body compounded by a plurality of layers of anti-electrostatic antibiotic non-woven fabrics. In the forming process of the polypropylene non-woven fabric, the invention prepares the anti-electrostatic antibiotic non-woven fabrics by adding the silver-loaded zeolite and the master batch and obtains the anti-electrostatic antibiotic mask by compounding the anti-electrostatic antibiotic non-woven fabrics; and the mask can prevent pathogen invasion and avoid generating static electricity.
Description
Technical field
The present invention relates to the health care products field, more particularly, relate to a kind of anti-electrostatic antibiotic mouth mask that can be applied to the anti-electrostatic antibiotic non-woven fabric of electron trade and adopt its making.
Background technology
Mouth mask is a health care products commonly used in people's daily life, initial mouth mask commonly used mostly is to be made by gauze, fine cloth or common non-woven fabric to form, and this type of mouth mask generally just plays the effect that dust, impurity and fiber substance in the secluding air enter oral cavity and nasal cavity.
SARS in 2003 wreaks havoc, the wide-scale distribution of bird flu in recent years and all kinds of respiratory infectious diseases, and nearly section the global of time H1N1 spreads, human beings'health has been brought serious threat, these diseases are all propagated by the air spittle or contact patient secretion, prevent important safeguard procedures of these diseases to be with exactly and muzzle.Yet common anti-dust respirator can't meet the demands, so people research and develop novel antibacterial mask energetically, for example: increase antibiotic layer, antibacterials or add various means such as active carbon plate to reach the purpose of sterilizing on mouth mask.
Chinese patent CN2606602Y discloses a kind of antibacterial mask, comprise gauze surface layer, internal layer, frenulum and interlayer, 1～3 layer of anti-bacteria cloth of place mat between interlayer, has the function of killing various germs and virus, particularly the mycoplasma germ to current trend has powerful sterilizing ability, can effectively prevent germ or viral per os, nasal cavity intrusion.Chinese patent CN2613278Y discloses a kind of negative ion antibiotic mouth mask, it is to be sewed up by surface layer and intermediate layer to form, negative ion powder is contained in the intermediate layer, anion has higher activity, very strong redox is arranged, can destroy the activity of cell membrane or the cellular plasm organized enzyme of bacterium, thereby reach the purpose of antibiotic and sterilizing, can prevent the intrusion of viruses such as SARS effectively, have the effect of anti-inflammation.Patent CN2691646Y discloses a kind of anti-flu antibacteria and fragrance mouth mask, is provided with medicine core chamber in mouth mask, and the medicine core that one deck at least is soaked with Chinese medicine is housed in the chamber, a mouth mask wherein side is provided with opening, when wearing mouth mask, the sustainable flavour of a drug of having given play to of medicine core are to realize the antibiotic effect of anti-flu.This class research has at present obtained development faster, and effect is better, has a extensive future.
In recent years, along with developing rapidly of electron trade, electronics producer is more and more, and in electron trade, the accumulation of static electricity that electromagnetic induction and friction produce produces electrion to various sensitiveness electronic components, instrument and meter etc., can cause great economic loss.Therefore, the Protection Product that is applied to electron trade all need have antistatic property, especially all the more so in the toilet that has relatively high expectations, for example: the electronic homework personnel all need use anti-electrostatic clothing, footwear, gloves and mouth mask etc. in the toilet, yet, the antibacterial mask that present industry is researched and developed does not generally have antistatic property, thereby is necessary existing antibacterial mask is improved.
Summary of the invention
The technical problem that the present invention will solve is do not have the shortcoming of antistatic property at the cloth that above-mentioned existing antibacterial mask adopted, and a kind of anti-electrostatic antibiotic non-woven fabric is provided, and has antistatic and antibiotic performance simultaneously.
Another technical problem that the present invention will solve is, the preparation method of above-mentioned anti-electrostatic antibiotic non-woven fabric is provided, and preparation technology is simple, can prepare the anti-electrostatic antibiotic non-woven fabric that suits the requirements.
The technical problem again that the present invention will solve is, the shortcoming that does not have antistatic performance at above-mentioned existing antibacterial mask, a kind of anti-electrostatic antibiotic mouth mask is provided, adopt above-mentioned anti-electrostatic antibiotic non-woven fabric to make, have antistatic and antibiotic function simultaneously, can prevent that germ invasion and attack from can avoid producing static again.
The present invention solves the technical scheme that its technical problem adopts: a kind of anti-electrostatic antibiotic non-woven fabric is provided, and its constituent is: polypropylene: 60～98 parts; Antiseptic: 1～20 part; Antistatic master granule: 1～20 part.
In anti-electrostatic antibiotic non-woven fabric of the present invention, described antiseptic is silver-loaded zirconium phosphate or zeolite with carrying silver.
The present invention solves another technical scheme that its technical problem adopts: a kind of preparation method of anti-electrostatic antibiotic mouth mask is provided, comprises the steps:
Step 1: prepare raw material: 1～20 part of 60～98 parts of polypropylene, 1～20 part of antistatic master granule, preparation silver-loaded zirconium phosphate or zeolite with carrying silver antiseptic is provided;
Step 2: raw material is passed through nonwoven fabric manufacture craft moulding anti-electrostatic antibiotic non-woven fabric.
In the preparation method of anti-electrostatic antibiotic non-woven fabric of the present invention, the preparation technology of described silver-loaded zirconium phosphate is: zirconia, oxalic acid, phosphoric acid are reacted after mixing, remove foreign ion, obtain the basic zirconium phosphate carrier, again the basic zirconium phosphate carrier is mixed with silver nitrate, remove the inorganic silver-loaded zirconium phosphate antiseptic that obtains containing Ag+ behind the foreign ion.
In the preparation method of anti-electrostatic antibiotic non-woven fabric of the present invention, the hybrid reaction temperature of described basic zirconium phosphate carrier and silver nitrate is 60～100 ℃, and the time is 4～10h.
In the preparation method of anti-electrostatic antibiotic non-woven fabric of the present invention, the preparation technology of described zeolite with carrying silver antiseptic is: with the 4A zeolite is carrier, AgNO
3Solution is reactant liquor, presses the solid-to-liquid ratio of 1g/10ml, prepares the zeolite with carrying silver antiseptic after the hybrid reaction.
In the preparation method of anti-electrostatic antibiotic non-woven fabric of the present invention, described 4A zeolite and AgNO
3The reaction condition of solution: temperature is 40～80 ℃, pH=6.0～8.0, and the reaction time is 2～6h.
The present invention solves the technical scheme again that its technical problem adopts: a kind of anti-electrostatic antibiotic mouth mask is provided, comprise: the mouth mask body that adopts several layers of above-mentioned anti-electrostatic antibiotic non-woven fabric to be composited, and on described mouth mask body, be crimped with the connecting line that is used to wear.
In anti-electrostatic antibiotic mouth mask of the present invention, described mouth mask body is three layers of anti-electrostatic antibiotic non-woven fabric composite construction.
In anti-electrostatic antibiotic mouth mask of the present invention, described connecting line is De Salle's line and the tramline that is crimped on the mouth mask body.
Implement the present invention and can bring following beneficial effect: by in the polypropylene non-woven fabric forming process, add a certain amount of zeolite with carrying silver and antistatic master granule, melt extrude jointly, reinforce into anti-electrostatic antibiotic non-woven fabric, its preparation technology is simple, and prepared anti-electrostatic antibiotic non-woven fabric has antistatic and anti-microbial property preferably; And then carry out three layers of anti-electrostatic antibiotic non-woven fabric compound, be pressed into tramline, De Salle's line, had the mouth mask of antistatic and antibacterial functions simultaneously, can prevent that germ invasion and attack from can avoid producing static again, can be widely used in electron trade, have vast market and development prospect.
The specific embodiment
Anti-electrostatic antibiotic mouth mask of the present invention comprises the mouth mask body, and is crimped on De Salle's line and tramline on the mouth mask body, and its improvements are that described mouth mask body adopts three layers of anti-electrostatic antibiotic non-woven fabric to be composited.
The constituent of described anti-electrostatic antibiotic non-woven fabric is: polypropylene: 60～98 parts, and silver-loaded zirconium phosphate or zeolite with carrying silver antiseptic: 1～20 part, and antistatic master granule: 1～20 part.
The preparation method of described anti-electrostatic antibiotic non-woven fabric comprises the steps: step 1: prepare raw material: 60～98 parts of polypropylene, 1～20 part of antistatic master granule are provided and prepare silver-loaded zirconium phosphate or 1～20 part of zeolite with carrying silver antiseptic. wherein, the preparation process of described silver-loaded zirconium phosphate is: zirconia, oxalic acid, phosphoric acid are mixed, react back suction filtration, washing, remove foreign ion, obtain the basic zirconium phosphate carrier; The basic zirconium phosphate carrier is mixed with silver nitrate, control exchange temperature is between 60～100 ℃, and the time is washed out foreign ion between 4～10h, obtaining containing the inorganic antiseptic silver-loaded zirconium phosphate (Ag-ZrP) of Ag+. described zeolite with carrying silver preparation process is: with the 4A zeolite is carrier, AgNO
3Solution is reactant liquor, press the solid-to-liquid ratio of 1g/10ml, 40～80 ℃, pH=6.0～8.0, stir under the condition of 2～6h, prepare the zeolite with carrying silver antiseptic, described 4A zeolite is the β cage that silica and aluminum-oxygen tetrahedron form, the cubic structure that is coupled together by cubic cage, be that crystal type is an A type zeolite, chemical composition is: Na
96[(AlO
2)
96(SiO
2)
96] 216H
2O.And described polypropylene (PP) can adopt commercially available polypropylene commonly used (PP), antistatic master granule also can adopt commercially available PP antistatic master granule, prepared silver-loaded zirconium phosphate antiseptic, zeolite with carrying silver antiseptic have antibiotic resistance performance, and selected antistatic master granule has antistatic performance preferably.
Step 2: raw material is passed through nonwoven fabric manufacture craft moulding anti-electrostatic antibiotic non-woven fabric; Described nonwoven fabric manufacture craft can realize by existing polypropylene non-woven fabric moulding process, comprise following operation: anti-electrostatic antibiotic non-woven fabric raw material feeding-raw materials melt is extruded-is stretched formation fiber-fiber cooling-fiber lay down and is set as net-reinforce into cloth.
Embodiment 1:
Commercially available 70 parts of polypropylene, 15 parts of antistatic master granules is provided, prepares 15 parts of silver-loaded zirconium phosphates then: zirconia, oxalic acid, phosphoric acid are mixed, react back suction filtration, washing, remove foreign ion, obtain the basic zirconium phosphate carrier; The basic zirconium phosphate carrier is mixed with silver nitrate, and control exchange temperature is between 60～200 ℃, and the time is washed out foreign ion between 4～10h, obtain containing the inorganic antiseptic silver-loaded zirconium phosphate (Ag-ZrP) of Ag+.70 parts of polypropylene, 15 parts of antistatic master granules and 15 parts of silver-loaded zirconium phosphate raw materials are melt extruded jointly, stretching forms fiber again, treats to be laid to net after the fiber cooling, reinforces into the antibiotic antistatic nonwoven fabric.And then through port cover body machine carries out three layers of antibiotic antistatic nonwoven fabric that makes compound, is pressed into De Salle's line, tramline by the electric welding machine ultrasonic welding, finally obtains the anti-electrostatic antibiotic mouth mask.
Embodiment 2:
Commercially available 80 parts of polypropylene, 10 parts of antistatic master granules is provided, and prepare 10 parts of zeolite with carrying silver then: with the 4A zeolite is carrier, AgNO
3Solution is reactant liquor, presses the solid-to-liquid ratio of 1g/10ml, 40～80 ℃, pH=6.0～8.0, stirs under the condition of 2～6h, prepares the zeolite with carrying silver antiseptic.80 parts of polypropylene, 10 parts of antistatic master granules and 10 parts of zeolite with carrying silver raw materials are melt extruded jointly, stretching forms fiber again, treats to be laid to net after the fiber cooling, reinforces into the antibiotic antistatic nonwoven fabric.And then through port cover body machine carries out three layers of antibiotic antistatic nonwoven fabric that makes compound, is pressed into De Salle's line, tramline by the electric welding machine ultrasonic welding, finally obtains the anti-electrostatic antibiotic mouth mask.
In sum, the present invention is by in the polypropylene non-woven fabric forming process, add a certain amount of zeolite with carrying silver and antistatic master granule, melt extrude jointly, reinforce into anti-electrostatic antibiotic non-woven fabric, its preparation technology is simple, and prepared anti-electrostatic antibiotic non-woven fabric has antistatic and anti-microbial property preferably; And then carry out three layers of anti-electrostatic antibiotic non-woven fabric compound, be pressed into tramline, De Salle's line, had the mouth mask of antistatic and antibacterial functions simultaneously, can prevent that germ invasion and attack from can avoid producing static again, can be widely used in electron trade, have vast market and development prospect.
The above; only for the preferable specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and anyly is familiar with those skilled in the art in the technical scope that the present invention discloses; the variation that can expect easily or replacement all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.
Claims (10)
1. an anti-electrostatic antibiotic non-woven fabric is characterized in that, its constituent is:
Polypropylene: 60～98 parts;
Antiseptic: 1～20 part;
Antistatic master granule: 1～20 part.
2. anti-electrostatic antibiotic non-woven fabric as claimed in claim 1 is characterized in that, described antiseptic is silver-loaded zirconium phosphate or zeolite with carrying silver.
3. the preparation method of an anti-electrostatic antibiotic non-woven fabric is characterized in that, comprises the steps:
Step 1: prepare raw material: 1～20 part of 60～98 parts of polypropylene, 1～20 part of antistatic master granule, preparation silver-loaded zirconium phosphate or zeolite with carrying silver antiseptic is provided;
Step 2: raw material is passed through nonwoven fabric manufacture craft moulding anti-electrostatic antibiotic non-woven fabric.
4. the preparation method of anti-electrostatic antibiotic non-woven fabric as claimed in claim 3, it is characterized in that, the preparation technology of described silver-loaded zirconium phosphate is: zirconia, oxalic acid, phosphoric acid are reacted after mixing, remove foreign ion, obtain the basic zirconium phosphate carrier, again the basic zirconium phosphate carrier is mixed with silver nitrate, remove the inorganic silver-loaded zirconium phosphate antiseptic that obtains containing Ag+ behind the foreign ion.
5. the preparation method of anti-electrostatic antibiotic non-woven fabric as claimed in claim 4 is characterized in that, the hybrid reaction temperature of described basic zirconium phosphate carrier and silver nitrate is 60～100 ℃, and the time is 4～10h.
6. the preparation method of anti-electrostatic antibiotic non-woven fabric as claimed in claim 3 is characterized in that, the preparation technology of described zeolite with carrying silver antiseptic is: with the 4A zeolite is carrier, AgNO
3Solution is reactant liquor, presses the solid-to-liquid ratio of 1g/10ml, prepares the zeolite with carrying silver antiseptic after the hybrid reaction.
7. the preparation method of anti-electrostatic antibiotic non-woven fabric as claimed in claim 6 is characterized in that, described 4A zeolite and AgNO
3The reaction condition of solution: temperature is 40～80 ℃, pH=6.0～8.0, and the reaction time is 2～6h.
8. an anti-electrostatic antibiotic mouth mask is characterized in that, comprising: the mouth mask body that adopts several layers of anti-electrostatic antibiotic non-woven fabric as claimed in claim 1 or 2 to be composited, and on described mouth mask body, be crimped with the connecting line that is used to wear.
9. anti-electrostatic antibiotic mouth mask as claimed in claim 8 is characterized in that, described mouth mask body is three layers of anti-electrostatic antibiotic non-woven fabric composite construction.
10. anti-electrostatic antibiotic mouth mask as claimed in claim 8 is characterized in that, described connecting line is De Salle's line and the tramline that is crimped on the mouth mask body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910110331A CN101705579A (en) | 2009-10-26 | 2009-10-26 | Anti-electrostatic antibiotic non-woven fabric, preparation process thereof and mask made of same |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910110331A CN101705579A (en) | 2009-10-26 | 2009-10-26 | Anti-electrostatic antibiotic non-woven fabric, preparation process thereof and mask made of same |
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| CN101705579A true CN101705579A (en) | 2010-05-12 |
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| CN200910110331A Pending CN101705579A (en) | 2009-10-26 | 2009-10-26 | Anti-electrostatic antibiotic non-woven fabric, preparation process thereof and mask made of same |
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| CN103360679A (en) * | 2013-05-23 | 2013-10-23 | 建德市新裕塑胶材料有限公司 | High-efficient reinforced anti-agglomeration antibacterial filler masterbatch for non-woven fabric and preparation process thereof |
| CN103757825A (en) * | 2014-02-18 | 2014-04-30 | 杭州杭润布艺有限公司 | Non-woven fabric for masks and production process thereof |
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| CN103757825A (en) * | 2014-02-18 | 2014-04-30 | 杭州杭润布艺有限公司 | Non-woven fabric for masks and production process thereof |
| CN103938291A (en) * | 2014-03-21 | 2014-07-23 | 深圳市新纶科技股份有限公司 | Silver-coated hollow bead compound filament yarn antibiosis fiber and preparation method thereof |
| CN103938291B (en) * | 2014-03-21 | 2016-03-30 | 深圳市新纶科技股份有限公司 | A kind of silver-plated cenosphere bicomponent filament yarn anti-bacterial fibre and preparation method thereof |
| CN106400527A (en) * | 2015-08-03 | 2017-02-15 | 上海亚都塑料有限公司 | Antimicrobial braided fabric |
| CN105332084A (en) * | 2015-12-01 | 2016-02-17 | 东华大学 | Preparation method for copper oxide-loaded mesoporous zirconium phosphate antibacterial polylactic acid fiber |
| CN105568562B (en) * | 2016-03-21 | 2018-09-07 | 恒天嘉华非织造有限公司 | A kind of medical non-woven fabrics composite material and preparation method |
| CN105568562A (en) * | 2016-03-21 | 2016-05-11 | 万全军 | Medical nonwoven composite material and preparation method thereof |
| CN106948088A (en) * | 2017-04-21 | 2017-07-14 | 天守(福建)超纤科技股份有限公司 | A kind of non-woven fabrics preparation method led surely |
| CN111227345A (en) * | 2020-02-18 | 2020-06-05 | 江苏亿茂滤材有限公司 | Antibacterial and antiviral mask and preparation method thereof |
| CN111227345B (en) * | 2020-02-18 | 2023-12-01 | 江苏亿茂滤材有限公司 | Antibacterial and antiviral mask and preparation method thereof |
| IT202000011641A1 (en) * | 2020-05-19 | 2021-11-19 | Univ Degli Studi Magna Graecia Di Catanzaro | PERSONAL PROTECTIVE EQUIPMENT AGAINST PATHOGENIC MICROORGANISMS AND ITS PRODUCTION PROCESS |
| EP3912500A1 (en) * | 2020-05-19 | 2021-11-24 | Università Degli Studi Magna Graecia Catanzaro | Personal protective equipment against pathogenic microorganisms and related production method |
| TWI722901B (en) * | 2020-05-21 | 2021-03-21 | 豪紳纖維科技股份有限公司 | Antibacterial cloth mask and manufacturing method thereof |
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Open date: 20100512 |