CN106281113A - A kind of high temperature resistant seccotine - Google Patents
A kind of high temperature resistant seccotine Download PDFInfo
- Publication number
- CN106281113A CN106281113A CN201610745464.4A CN201610745464A CN106281113A CN 106281113 A CN106281113 A CN 106281113A CN 201610745464 A CN201610745464 A CN 201610745464A CN 106281113 A CN106281113 A CN 106281113A
- Authority
- CN
- China
- Prior art keywords
- parts
- sulfur
- seccotine
- ester
- high temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J109/00—Adhesives based on homopolymers or copolymers of conjugated diene hydrocarbons
- C09J109/02—Copolymers with acrylonitrile
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/06—Sulfur
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/101—Esters; Ether-esters of monocarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/15—Heterocyclic compounds having oxygen in the ring
- C08K5/156—Heterocyclic compounds having oxygen in the ring having two oxygen atoms in the ring
- C08K5/1565—Five-membered rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/45—Heterocyclic compounds having sulfur in the ring
- C08K5/46—Heterocyclic compounds having sulfur in the ring with oxygen or nitrogen in the ring
- C08K5/47—Thiazoles
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
Abstract
The invention discloses a kind of high temperature resistant seccotine, this seccotine is made up of following components: LNBR/sulfur, dimethylethanolamine, formic acid phenethyl ester, 4 methylvaleric acid methyl ester, 2 (2 bromoethyls) 1, 3 dioxolanes and (R) 2 sulfur are for tetrahydro-thiazoles 4 carboxylic acid, ethyl ester, the weight content of its each component is: 50 ~ 70 parts of LNBR/sulfur, dimethylethanolamine 23 ~ 35 parts, formic acid phenethyl ester 30 ~ 45 parts, 4 methylvaleric acid methyl ester 15 ~ 26 parts, 2 (2 bromoethyls) 1, 3 dioxolanes 10 ~ 30 parts and (R) 2 sulfur are for tetrahydro-thiazoles 4 carboxylic acid, ethyl ester 25 ~ 45 parts.Quick solidifying of the present invention, resistance to impact are good, media-resistant, can be used below at 80 DEG C.
Description
Technical field
The present invention relates to seccotine field, particularly relate to a kind of high temperature resistant seccotine.
Background technology
The concept of adhesive: adhesive is that one leans on interface interaction (chemical force or physical force) firm for various solid materials
The material bonded together, be again bonding agent or adhesive, be called for short " glue ".
The application of adhesive widely, relate to building, packaging, space flight, aviation, electronics, automobile, plant equipment,
The every field of the national economy such as health care, light textile.
But, currently used seccotine solidification is fast not, the pliable and tough difference of glued membrane, poor impact resistance, not media-resistant, Zhi Neng
Use under room temperature.
Summary of the invention
The technical problem that present invention mainly solves is to provide a kind of high temperature resistant seccotine, quick solidifying, resistance to impact Jie good, resistance to
Matter, can be used below at 80 DEG C.
For solving above-mentioned technical problem, the technical scheme that the present invention uses is: provide a kind of high temperature resistant seccotine, should
Seccotine is made up of following components: LNBR/sulfur, dimethylethanolamine, formic acid phenethyl ester, 4-methylvaleric acid first
Ester, 2-(2-bromoethyl)-1,3-dioxolane and (R)-2-sulfur contain for tetrahydro-thiazoles-4-carboxylic acid's ethyl ester, the weight of its each component
Amount is: 50 ~ 70 parts of LNBR/sulfur, dimethylethanolamine 23 ~ 35 parts, formic acid phenethyl ester 30 ~ 45 parts, 4-methylpent
Acid methyl ester 15 ~ 26 parts, 2-(2-bromoethyl)-1,3-dioxolane 10 ~ 30 parts and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic acid's ethyl ester
25 ~ 45 parts.
In a preferred embodiment of the present invention, the weight content of described LNBR/sulfur is 55 ~ 65 parts.
In a preferred embodiment of the present invention, described 2-(2-bromoethyl)-1, the weight content of 3-dioxolane is
15 ~ 25 parts.
In a preferred embodiment of the present invention, described (R)-2-sulfur contains for the weight of tetrahydro-thiazoles-4-carboxylic acid's ethyl ester
Amount is 30 ~ 40 parts.
The invention has the beneficial effects as follows: quick solidifying of the present invention, resistance to impact are good, media-resistant, can be used below at 80 DEG C.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described enforcement
Example is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this area is common
All other embodiments that technical staff is obtained under not making creative work premise, broadly fall into the model of present invention protection
Enclose.
Embodiment 1
A kind of high temperature resistant seccotine, this seccotine is made up of following components: LNBR/sulfur, dimethylethanolamine, ant
Acid phenethyl ester, 4-methylvaleric acid methyl ester, 2-(2-bromoethyl)-1,3-dioxolane and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic acid
Ethyl ester, the weight content of its each component is: 55 parts of LNBR/sulfur, dimethylethanolamine 23 parts, formic acid phenethyl ester 30
Part, 4-methylvaleric acid methyl ester 15 parts, 2-(2-bromoethyl)-1,3-dioxolane 15 parts and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic
Acetoacetic ester 30 parts.
Embodiment 2
A kind of high temperature resistant seccotine, this seccotine is made up of following components: LNBR/sulfur, dimethylethanolamine, ant
Acid phenethyl ester, 4-methylvaleric acid methyl ester, 2-(2-bromoethyl)-1,3-dioxolane and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic acid
Ethyl ester, the weight content of its each component is: 65 parts of LNBR/sulfur, dimethylethanolamine 35 parts, formic acid phenethyl ester 45
Part, 4-methylvaleric acid methyl ester 26 parts, 2-(2-bromoethyl)-1,3-dioxolane 25 parts and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic
Acetoacetic ester 40 parts.
Embodiment 3
A kind of high temperature resistant seccotine, this seccotine is made up of following components: LNBR/sulfur, dimethylethanolamine, ant
Acid phenethyl ester, 4-methylvaleric acid methyl ester, 2-(2-bromoethyl)-1,3-dioxolane and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic acid
Ethyl ester, the weight content of its each component is: 60 parts of LNBR/sulfur, dimethylethanolamine 32 parts, formic acid phenethyl ester 37
Part, 4-methylvaleric acid methyl ester 20 parts, 2-(2-bromoethyl)-1,3-dioxolane 20 parts and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic
Acetoacetic ester 35 parts.
The present invention is high temperature resistant, and seccotine provides the benefit that: quick solidifying of the present invention, resistance to impact are good, media-resistant, can be 80
DEG C used below.
The foregoing is only embodiments of the invention, not thereby limit the scope of the claims of the present invention, every utilize this
Equivalent structure or equivalence flow process that bright description is made convert, or are directly or indirectly used in other relevant technology neck
Territory, is the most in like manner included in the scope of patent protection of the present invention.
Claims (4)
1. a high temperature resistant seccotine, it is characterised in that this seccotine is made up of following components: LNBR/sulfur, two
Methylethanolamine, formic acid phenethyl ester, 4-methylvaleric acid methyl ester, 2-(2-bromoethyl)-1,3-dioxolane and (R)-2-sulfur generation four
Hydrogen thiazole-4-carboxylic acid ethyl ester, the weight content of its each component is: 50 ~ 70 parts of LNBR/sulfur, dimethylethanolamine
23 ~ 35 parts, formic acid phenethyl ester 30 ~ 45 parts, 4-methylvaleric acid methyl ester 15 ~ 26 parts, 2-(2-bromoethyl)-1,3-dioxolane 10 ~
30 parts and (R)-2-sulfur are for tetrahydro-thiazoles-4-carboxylic acid's ethyl ester 25 ~ 45 parts.
High temperature resistant seccotine the most according to claim 1, it is characterised in that the weight of described LNBR/sulfur
Amount content is 55 ~ 65 parts.
High temperature resistant seccotine the most according to claim 1, it is characterised in that described 2-(2-bromoethyl)-1,3-dioxy
The weight content of pentane is 15 ~ 25 parts.
High temperature resistant seccotine the most according to claim 1, it is characterised in that described (R)-2-sulfur is for tetrahydro-thiazoles-4-
The weight content of carboxylic acid, ethyl ester is 30 ~ 40 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745464.4A CN106281113A (en) | 2016-08-29 | 2016-08-29 | A kind of high temperature resistant seccotine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745464.4A CN106281113A (en) | 2016-08-29 | 2016-08-29 | A kind of high temperature resistant seccotine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106281113A true CN106281113A (en) | 2017-01-04 |
Family
ID=57677864
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610745464.4A Pending CN106281113A (en) | 2016-08-29 | 2016-08-29 | A kind of high temperature resistant seccotine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106281113A (en) |
-
2016
- 2016-08-29 CN CN201610745464.4A patent/CN106281113A/en active Pending
Non-Patent Citations (6)
| Title |
|---|
| 《中国茶学词典》编纂委员会编纂: "《中国茶学词典》", 31 October 1995, 上海科学技术出版社 * |
| 夏铮南等: "《香料与香精》", 30 April 1998, 中国物资出版社 * |
| 李子东等: "《胶黏剂助剂》", 30 June 2009, 化学工业出版社 * |
| 许戈文等: "《合成香料产品技术手册》", 29 February 1996, 中国商业出版社 * |
| 顾继友等: "《胶黏剂与涂料 第2版》", 30 September 2012, 中国林业出版社 * |
| 黄化民等: "（R）-2-硫代四氢噻唑-4-羧酸及其酯的合成", 《有机化学》 * |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170104 |