CN106278194A - A kind of manufacture method of long rod pottery - Google Patents
A kind of manufacture method of long rod pottery Download PDFInfo
- Publication number
- CN106278194A CN106278194A CN201510266324.4A CN201510266324A CN106278194A CN 106278194 A CN106278194 A CN 106278194A CN 201510266324 A CN201510266324 A CN 201510266324A CN 106278194 A CN106278194 A CN 106278194A
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- silica gel
- gel tube
- long rod
- ceramic powder
- pottery
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Abstract
The invention discloses the manufacture method of a kind of long rod pottery, the method includes: select the silica gel tube of predetermined inner diameter as mould;Ceramic powder is circulated in silica gel tube, and ceramic powder is carried out ram-jolt;Ceramic powder is sealed in silica gel tube;Cold isostatic compaction is carried out in being fixed to the pressurization water vat of cold isostatic press after silica gel tube stretching preset length after sealing;After cold isostatic compaction, silica gel tube is taken out in pressurization water vat;The biscuit of long rod pottery is taken out from silica gel tube;Carry out high temperature sintering process in the biscuit of long rod pottery is put into default V-groove, obtain long rod pottery.Compared with prior art, ceramic powder is circulated in silica gel tube by the present invention, and seal and tensile silicon sebific duct, then cold isostatic compaction is carried out, eliminate the dispensing before molding and batch mixing process, the i.e. present invention need not do binder removal process, and the time therefore making long rod pottery cost is shorter, improves the production efficiency of product.
Description
Technical field
The present invention relates to ceramic product manufacture technology field, particularly relate to the making side of a kind of long rod pottery
Method.
Background technology
Long rod pottery is with aluminium oxide, zirconium oxide etc. as main component.In industry manufacture field, due to long rod pottery
Porcelain has the characteristics such as good wearability, is therefore widely used.
At present, prior art use the mode of injection mo(u)lding to make long rod pottery.Specifically, for convenience
The molding of ceramic powder, firstly, it is necessary to be equipped with multiple slurry, then by slurry good for proportioning and ceramic powder
Put into after mixing in mould and be shaped processing, obtain the biscuit of long rod pottery.Further, in order to prevent
There is gross distortion or produce bubble in the biscuit of long rod pottery during sintering, before sintering, it is right to need
The biscuit of long rod pottery obtained above carries out binder removal process, i.e. removes the slurry in biscuit, so that after Shao Jie
Obtain the long rod pottery of high-quality.During above-mentioned making long rod pottery, due to binder removal process spend time
Between longer, it usually needs several days, so the production efficiency of product is the highest.
Summary of the invention
The purpose of the embodiment of the present invention is to provide the manufacture method of a kind of long rod pottery, to improve the life of product
Produce efficiency.Concrete technical scheme is as follows:
A kind of manufacture method of long rod pottery, including:
Select the silica gel tube of predetermined inner diameter as mould;
Ceramic powder is circulated in described silica gel tube, and described ceramic powder is carried out ram-jolt;
Described ceramic powder is sealed in described silica gel tube;
Carry out in being fixed to the pressurization water vat of cold isostatic press after silica gel tube stretching preset length after sealing
Cold isostatic compaction;
After cold isostatic compaction, described silica gel tube is taken out in described pressurization water vat;
The biscuit of long rod pottery is taken out from described silica gel tube;
Carry out high temperature sintering process in the biscuit of described long rod pottery is put into default V-groove, grown
Rod pottery.
In a kind of detailed description of the invention of the present invention, described ceramic powder is circulated in described silica gel tube,
And the step that described ceramic powder carries out ram-jolt includes:
One end of described silica gel tube is sealed;
Described ceramic powder is poured into from the other end of described silica gel tube;
Described ceramic powder is carried out ram-jolt.
In a kind of detailed description of the invention of the present invention, described will seal after silica gel tube stretching preset length after
The step carrying out cold isostatic compaction in being fixed to the pressurization water vat of cold isostatic press includes:
Silica gel tube after described sealing is stretched preset length;
Silica gel tube after stretching is fixed in the pressurization water vat of cold isostatic press;
It is pressurized to the silica gel tube in described pressurization water vat preset pressure;
Keep described default pressure that the silica gel tube in described pressurization water vat is pressurizeed the scheduled time;
Silica gel tube in described pressurization water vat is carried out reduced pressure treatment, takes out in described pressurization water vat to facilitate
Silica gel tube.
In a kind of detailed description of the invention of the present invention, described default pressure is 150-250MPa.
In a kind of detailed description of the invention of the present invention, the described biscuit by described long rod pottery is put into default
V-groove in carry out high temperature sintering process, the step obtaining long rod pottery includes:
The biscuit of described long rod pottery is put in default V-groove;
With high temperature block, the biscuit of the long rod pottery in described V-groove is corrected compaction treatment;
The biscuit of the long rod pottery after correction compacting is carried out high temperature sintering process, obtains long rod pottery.
In a kind of detailed description of the invention of the present invention, after obtaining described long rod pottery, also include:
Utilize centerless grinder that the diameter of described long rod pottery is processed.
In a kind of detailed description of the invention of the present invention, described ceramic powder is aluminium oxide or zirconium oxide.
In a kind of detailed description of the invention of the present invention, the D50 particle diameter of described ceramic powder is 300-700nm.
In a kind of detailed description of the invention of the present invention, the shore hardness of described silica gel tube is 15-20 degree.
In a kind of detailed description of the invention of the present invention, described preset length is 15-25mm.
The technical scheme that the embodiment of the present invention is provided, select predetermined inner diameter silica gel tube as mould,
Then ceramic powder it is circulated in silica gel tube and seals, and the silica gel tube after stretching preset length is put into cold
Cold isostatic compaction is carried out in the pressurization water vat of isostatic pressing machine, after cold isostatic compaction, further, will be long
The biscuit of rod pottery takes out from silica gel tube, and carries out high temperature burning in this biscuit is put into default V-groove
Knot processes, and obtains long rod pottery.In said process, ceramic powder is circulated in silica gel tube, and seal and
Tensile silicon sebific duct, then carries out cold isostatic compaction, eliminates the dispensing before molding and batch mixing process, i.e.
The present invention need not do binder removal and processes, and therefore makes the long rod ceramic time spent shorter, improves product
Production efficiency.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, below will be to enforcement
In example or description of the prior art, the required accompanying drawing used is briefly described, it should be apparent that, describe below
In accompanying drawing be only some embodiments of the present invention, for those of ordinary skill in the art, do not paying
On the premise of going out creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
The implementing procedure figure one of the manufacture method of a kind of long rod pottery that Fig. 1 provides for the embodiment of the present invention;
The implementing procedure figure two of the manufacture method of a kind of long rod pottery that Fig. 2 provides for the embodiment of the present invention.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clearly
Chu, be fully described by, it is clear that described embodiment be only a part of embodiment of the present invention rather than
Whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making creation
The every other embodiment obtained under property work premise, broadly falls into the scope of protection of the invention.
As it is shown in figure 1, a kind of long excellent ceramic manufacture method that the embodiment of the present invention provides, the method is permissible
Including:
Step S101, selects the silica gel tube of predetermined inner diameter as mould;
Implementation process to technical scheme does specific description below.First, select to preset
The silica gel tube of internal diameter is as mould.Wherein, the internal diameter of silica gel tube can be according to the long rod pottery that will make
The thickness of porcelain selects.Owing to shore hardness is elastic all in the pliability of the silica gel tube of 15-20 degree and absorption
Preferably, excellent performance, so in being embodied as, the shore hardness of the silica gel tube in the present invention can be
15-20 degree.It addition, the silica gel tube in the present invention can be the silica gel tube that only one end is closed, it is also possible to be
The silica gel tube that two ends are not closed.
Step S102, is circulated into ceramic powder in described silica gel tube, and described ceramic powder is carried out ram-jolt;
After choosing mould, further, ceramic powder is circulated in silica gel tube, and to pottery
Powder carries out ram-jolt.When silica gel tube is the silica gel tube that two ends are not closed, step S102 can include following
Step:
One end of described silica gel tube is sealed;
Described ceramic powder is poured into from the other end of described silica gel tube;
Described ceramic powder is carried out ram-jolt.
Wherein, the concrete grammar of ram-jolt ceramic powder can be the silica gel tube that teetertotters.It addition, it is apparent
Ground is: when silica gel tube is the silica gel tube that only one end is closed, directly can pour into pottery from the other end of silica gel tube
Ceramic powder, and the silica gel tube ram-jolt ceramic powder that teetertotters.Wherein, in a kind of specific embodiment party of the present invention
In formula, the ceramic powder in the present invention can be aluminium oxide or zirconium oxide.It addition, the ceramics in the present invention
The D50 particle diameter of material can be 300-700nm.
Step S103, is sealed in described ceramic powder in described silica gel tube;
After ram-jolt ceramic powder, further, ceramic powder is sealed in silica gel tube, specifically, will
The unencapsulated one end of silica gel tube carries out encapsulation process.
Step S104, is fixed to the pressure (hydraulic) water of cold isostatic press after the silica gel tube stretching preset length after sealing
Cold isostatic compaction is carried out in cylinder;
After being sealed in silica gel tube by ceramic powder, further, the silica gel tube stretching after sealing is preset
Cold isostatic compaction is carried out in being fixed to the pressurization water vat of cold isostatic press after length.A kind of tool in the present invention
In body embodiment, step S104 may include that
Silica gel tube after described sealing is stretched preset length;
Silica gel tube after stretching is fixed in the pressurization water vat of cold isostatic press;
It is pressurized to the silica gel tube in described pressurization water vat preset pressure;
Keep described default pressure that the silica gel tube in described pressurization water vat is pressurizeed the scheduled time;
Silica gel tube in described pressurization water vat is carried out reduced pressure treatment, takes out in described pressurization water vat to facilitate
Silica gel tube.
The bending of the excellent pottery of length in order to avoid producing, first, the silica gel tube stretching after sealing is default
Length, in being embodied as, the preset length in the present invention can be 15-25mm, specifically, presets long
The length of degree can be changed according to the length of silica gel tube.Further it will be understood that the length of silica gel tube
It is adaptive with the length of the long rod pottery made.Further, the silica gel tube after stretching is fixed to cold etc.
In the pressurization water vat of static pressure machine, and it is pressurized to preset pressure to the silica gel tube in pressurization water vat.It is being embodied as
In, above-mentioned default pressure can be 150-250MPa.It is pressurized to preset pressure to the silica gel tube in pressurization water vat
After, keep presetting pressure to the silica gel tube pressurization scheduled time in pressurization water vat.When being embodied as, this makes a reservation for
Time can be the 30-60 second.After to the silica gel tube pressurization scheduled time, further, in pressurization water vat
Silica gel tube carry out reduced pressure treatment, with facilitate from pressurization water vat in take out silica gel tube.
Owing to the forming process of rod pottery long in the present invention is carried out in cold isostatic press, it is i.e. by pressurization
Realize the molding of long rod pottery, so the present invention need not add slurry in ceramic powder, eliminate
Dispensing and batch mixing process.And the proportioning of the various slurry of blending process generally requires the longer exploration time, so
Technical scheme decreases the time of early stage when making long rod pottery.
Step S105, after cold isostatic compaction, takes out described silica gel tube in described pressurization water vat;
After cold isostatic compaction in step S104, silica gel tube is taken out in pressurization water vat, with convenient
The biscuit of long rod pottery is taken out from silica gel tube.
Step S106, takes out the biscuit of long rod pottery from described silica gel tube;
After silica gel tube takes out from pressurization water vat, further, from silica gel tube, take out the element of long rod pottery
Base.
Step S107, is carried out at high temperature sintering in the biscuit of described long rod pottery is put into default V-groove
Reason, obtains long rod pottery.
After taking out the biscuit of long rod pottery from silica gel tube, further, the biscuit of long rod pottery is put into
Carry out high temperature sintering process in the V-groove preset, obtain long rod pottery.In the present invention is embodied as, step
Rapid S107 may include that
The biscuit of described long rod pottery is put in default V-groove;
With high temperature block, the biscuit of the long rod pottery in described V-groove is corrected compaction treatment;
The biscuit of the long rod pottery after correction compacting is carried out high temperature sintering process, obtains long rod pottery.
When carrying out step S107, first, the biscuit of long rod pottery is put in default V-groove, and uses
High temperature block is corrected compaction treatment to the biscuit of the long rod pottery in V-groove, further, to correction pressure
The biscuit of the long rod pottery after reality carries out high temperature sintering process, obtains long rod pottery.Long rod pottery in the present invention
Biscuit be placed on V-groove in carry out high temperature sintering process, due to the structure of V-groove, the element of long rod pottery
When base is placed on V-groove, stability is preferable, thus technical scheme to be conducive to producing qualification rate high
Long rod pottery.It addition, after being put in default V-groove by the biscuit of long rod pottery, high temperature block can be used
The biscuit of the long rod pottery in V-groove is corrected compaction treatment.As such, it is possible to will not place
The biscuit of long rod pottery is corrected compaction treatment, carries out the biscuit of long rod pottery after correction compaction treatment again
High temperature sintering processes, and can further improve the qualification rate of the long rod pottery produced.
It is shown in Figure 2, in a kind of detailed description of the invention of the present invention, after step S107, it is also possible to
Including:
Step S108, utilizes centerless grinder to be processed the diameter of described long rod pottery.
After obtaining long rod pottery, in order to the quality making long rod pottery is more preferable, it is possible to further utilize nothing
The diameter of long rod pottery is processed by reduction bed.Owing to the diameter of long rod pottery can be carried out by centerless grinder
Retrofit, so the long rod pottery after centerless grinder is processed has more preferable quality, makes long rod pottery energy
Enough it is applied to the field higher to workpiece accuracy requirement.
The technical scheme that the embodiment of the present invention is provided, select predetermined inner diameter silica gel tube as mould,
Then ceramic powder it is circulated in silica gel tube and seals, and the silica gel tube after stretching preset length is put into cold
Cold isostatic compaction is carried out in the pressurization water vat of isostatic pressing machine, after cold isostatic compaction, further, will be long
The biscuit of rod pottery takes out from silica gel tube, and carries out high temperature burning in this biscuit is put into default V-groove
Knot processes, and obtains long rod pottery.In said process, ceramic powder is circulated in silica gel tube, and seal and
Tensile silicon sebific duct, then carries out cold isostatic compaction, eliminates the dispensing before molding and batch mixing process, i.e.
The present invention need not do binder removal and processes, and therefore makes the long rod ceramic time spent shorter, improves product
Production efficiency.
It should be noted that in this article, term " include ", " comprising " or its any other variant
It is intended to comprising of nonexcludability, so that include that the process of a series of key element, method not only include that
A little key elements, but also include other key elements being not expressly set out, or also include for this process, side
The key element that method is intrinsic.
Each embodiment in this specification all uses relevant mode to describe, phase homophase between each embodiment
As part see mutually, what each embodiment stressed is different from other embodiments it
Place.The foregoing is only presently preferred embodiments of the present invention, be not intended to limit protection scope of the present invention.
All any modification, equivalent substitution and improvement etc. made within the spirit and principles in the present invention, are all contained in
In protection scope of the present invention.
Claims (10)
1. the manufacture method of one kind long rod pottery, it is characterised in that including:
Select the silica gel tube of predetermined inner diameter as mould;
Ceramic powder is circulated in described silica gel tube, and described ceramic powder is carried out ram-jolt;
Described ceramic powder is sealed in described silica gel tube;
Carry out in being fixed to the pressurization water vat of cold isostatic press after silica gel tube stretching preset length after sealing
Cold isostatic compaction;
After cold isostatic compaction, described silica gel tube is taken out in described pressurization water vat;
The biscuit of long rod pottery is taken out from described silica gel tube;
Carry out high temperature sintering process in the biscuit of described long rod pottery is put into default V-groove, grown
Rod pottery.
Method the most according to claim 1, it is characterised in that described ceramic powder is circulated into described
In silica gel tube, and the step that described ceramic powder carries out ram-jolt includes:
One end of described silica gel tube is sealed;
Described ceramic powder is poured into from the other end of described silica gel tube;
Described ceramic powder is carried out ram-jolt.
Method the most according to claim 1, it is characterised in that described will seal after silica gel tube stretching
The step carrying out cold isostatic compaction in being fixed to the pressurization water vat of cold isostatic press after preset length includes:
Silica gel tube after described sealing is stretched preset length;
Silica gel tube after stretching is fixed in the pressurization water vat of cold isostatic press;
It is pressurized to the silica gel tube in described pressurization water vat preset pressure;
Keep described default pressure that the silica gel tube in described pressurization water vat is pressurizeed the scheduled time;
Silica gel tube in described pressurization water vat is carried out reduced pressure treatment, takes out in described pressurization water vat to facilitate
Silica gel tube.
Method the most according to claim 3, it is characterised in that described default pressure is 150-250MPa.
Method the most according to claim 1, it is characterised in that the described biscuit by described long rod pottery
Carrying out high temperature sintering process in putting into default V-groove, the step obtaining long rod pottery includes:
The biscuit of described long rod pottery is put in default V-groove;
With high temperature block, the biscuit of the long rod pottery in described V-groove is corrected compaction treatment;
The biscuit of the long rod pottery after correction compacting is carried out high temperature sintering process, obtains long rod pottery.
Method the most according to claim 1, it is characterised in that after obtaining described long rod pottery, also
Including:
Utilize centerless grinder that the diameter of described long rod pottery is processed.
7. according to the method described in any one of claim 1 to 6, it is characterised in that described ceramic powder is
Aluminium oxide or zirconium oxide.
8. according to the method described in any one of claim 1 to 6, it is characterised in that described ceramic powder
D50 particle diameter is 300-700nm.
9. according to the method described in any one of claim 1 to 6, it is characterised in that Shao of described silica gel tube
Family name's hardness is 15-20 degree.
10. according to the method described in any one of claim 1 to 6, it is characterised in that described preset length is
15-25mm。
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108372573A (en) * | 2018-03-20 | 2018-08-07 | 中国科学院上海硅酸盐研究所 | The cold isostatic compaction mould and forming method of ceramic tube |
CN108585820A (en) * | 2018-04-20 | 2018-09-28 | 横店集团东磁股份有限公司 | A kind of preparation method of speciality cylinder magnetic ferrite magnetic core |
CN113171210A (en) * | 2021-04-20 | 2021-07-27 | 江苏泰州麦迪医疗科技有限公司 | Manufacturing method and forming tool for ceramic sliding groove prosthesis |
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CN113171210A (en) * | 2021-04-20 | 2021-07-27 | 江苏泰州麦迪医疗科技有限公司 | Manufacturing method and forming tool for ceramic sliding groove prosthesis |
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