CN106278150A - A kind of preparation method of Maifanitum boccaro cooking device - Google Patents
A kind of preparation method of Maifanitum boccaro cooking device Download PDFInfo
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- CN106278150A CN106278150A CN201610657687.5A CN201610657687A CN106278150A CN 106278150 A CN106278150 A CN 106278150A CN 201610657687 A CN201610657687 A CN 201610657687A CN 106278150 A CN106278150 A CN 106278150A
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- Prior art keywords
- maifanitum
- base substrate
- mud
- biscuiting
- blank
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
Abstract
The invention provides the preparation method of a kind of Maifanitum boccaro cooking device, it is characterised in that comprise the following production steps that prepared by (1) blank;(2) Maifanitum slurrying;(3) product molding;(4) repaired biscuit;(5) high temperature biscuiting;(6) Maifanitum mud is used;(7) easy fired.The Maifanitum boccaro cooking device outward appearance that the present invention prepares is regular, and Maifanitum mud layer combines together with base substrate, surfacing, has some strength and wearability, it is adaptable to cooking food and cleaning.The quality of goods meets GB/T10816 " zisha earthenware " and QB/T2580 " fine ceramics cooking device " standard-required, the lead of goods, quantity of cadmium release meet GB12651 2003 " contact with food ceramic lead, quantity of cadmium release tolerance limit " standard-required, article topsheet has the activity of Maifanitum, useful trace element energy dissolution and energy ionizing.
Description
Technical field
The present invention relates to ceramic field, the preparation method of a kind of Maifanitum boccaro cooking device.
Background technology
According to " Maifanitum processing and application " book introduction: " Maifanitum is that Ancient Times in China physician is quite seemingly big according to its outward appearance
Rice dumpling that wheat rice cooks and gain the name, be China's application a kind of tradition natural minerals YAOSHI the earliest, be a kind of air slaking or half air slaking
The intermediate-felsic rock that shallow one-tenth becomes to an ultra shallow, it is a kind of grandidierite product.Maifanitum contains the multiple trace element useful to human body,
There is the dual regulation to constituent content in water and pH value, there is biological activity and nontoxic, innocuousness, be referred to as health care medicinal
Stone, health-care stone, long-lived stone.”
The effect of Maifanitum is unquestionable, is also widely used.And it is applied to pottery, it is i.e. and Ceramic bond to make Maifanitum
During ceramic, effect of Maifanitum the most significantly declines.Reason be pottery be to burn till through high temperature, when Maifanitum is former with pottery
Making product and when high temperature burns till after material mixing, Maifanitum can be with Ceramic Material association reaction form new crystal, wheat
Trace element in meal stone is difficult to disengage.
How to make the temperature that Maifanitum burns till without undergoing ceramic high temperature, can combine closely with pottery again and form one, system
One-tenth can contacting foodstuff and the Chinese medicine stone ceramic vessel of the cooking, make the trace element of Maifanitum be disengaged, and pottery keep original
Chemical stability, the sanitary index such as lead, quantity of cadmium release meets relevant criterion requirement, and this difficult problem is skill in current ceramic industry
Art innovation and the problem of research of technique.
Summary of the invention
For solving the problems referred to above, the invention provides the preparation method of a kind of Maifanitum boccaro cooking device.Through high temperature element
Use the mud layer with Maifanitum as main material on the base substrate of the boccaro ceramic cooking device burnt, and through easy fired, make ceramic
Base substrate combines together with mud, prepares Maifanitum boccaro cooking device.
The preparation method of the Maifanitum boccaro cooking device of the present invention, it is characterised in that comprise the following production steps that
(1) prepared by blank
By the preparation method of Production of Ceramics blank, take blank stock through ball milling, sieve, press filt, old, pugging, prepare pledge
Measure the blank that moisture content is 20 22% standby;
Described raw material is that purple clay, Kaolin, spodumene, Talcum, clay mix;
(2) Maifanitum slurrying
Take Maifanitum 78 82 weight portion, above-mentioned standby blank 18 22 weight portion as raw material;
Above-mentioned Maifanitum is 5 hours through 380 420 DEG C of calcinings, calcination time;
Adding clear water after being mixed by above-mentioned raw materials and carry out wet ball grinding, cross 325 mesh sieves through ball milling raw material, through sieving, storage deposited in by raw material
Stock tank is carried out old 24 36 hours, and adding clear water through old raw material, to be deployed into the Maifanitum mud that concentration is 32 36 Baume degrees standby
With;
(3) product molding
Take above-mentioned standby blank, use roller head machine to carry out roll forming, prepare shale base substrate;
(4) repaired biscuit
Use soft cloth and clear water, the above-mentioned shale billet surface through molding is carried out reconditioning, makes shale billet surface smooth, will repair
Shale base substrate after base is deposited at shady and cool ventilation, natural airing 8 10 hours;
(5) high temperature biscuiting
Shale base substrate through airing carrying out high temperature biscuiting, is i.e. to use conventional kiln to carry out biscuiting, biscuiting temperature is
1190 1210 DEG C, the biscuiting time is 12 14 hours, and biscuiting atmosphere is oxidizing atmosphere, becomes through the shale base substrate of biscuiting and has
The ceramic base substrate of some strength;
(6) Maifanitum mud is used
Above-mentioned standby Maifanitum mud is deposited in the stainless steel cask of opening;
Ceramic base substrate after above-mentioned biscuiting is heated, is i.e. to be positioned over ceramic base substrate in kiln to be heated to ceramic billet surface temperature
Degree is 70 80 DEG C;
Being soaked by heated ceramic base substrate in the Maifanitum mud of stainless steel cask inner face, the immersion time is 35 seconds, allows
Ceramic billet surface absorption mud, through absorption mud ceramic base substrate at pulp after, deposit in nature airing 3 at shady and cool ventilation
5 hours;
(7) easy fired
Use conventional Production of Ceramics kiln, to carrying out easy fired through using the ceramic base substrate of Maifanitum mud, burn till into
900 DEG C, firing time is 68 hours, prepares Maifanitum boccaro cooking device.
Composition of raw materials of the present invention described briefly below and the special role of technique: the present invention uses secondary method for cooking, heat-resisting purple
Chiltern base substrate uses high temperature biscuiting, uses the temperature close to 1200 DEG C, makes mineral material fully react the most biochemical and physics change
Changing, form new crystal, after high temperature biscuiting, no longer there is big change in base substrate in follow-up easy fired;Use
Easy fired, uses the temperature close to 900 DEG C, and Maifanitum mud layer produces with the billet surface through biscuiting and merges, and Maifanitum
Activity only have fraction impacted, overall activity is retained, and solves in the preparation method of routine, is added by Maifanitum
In blank, also high temperature burns till, the problem substantially destroying China medicinal stone active;Maifanitum first warp, close to the calcining of 400 DEG C, first removes
Removing the organic impurities in Maifanitum, this Temperature Treatment also makes Maifanitum fully activate;Before using Maifanitum mud, first to through height
The ceramic base substrate of temperature biscuiting carries out Temperature Treatment, makes ceramic base substrate enter in slurry liquid with temperature, makes ceramic base substrate energy preferably
Ground midge, solves a difficult problem for the more difficult midge of ceramic base substrate after high-temperature firing;Maifanitum mud is in preparation process, through 23
It old, can improve the absorption in ceramic billet surface of the viscosity of mud, beneficially mud layer.
The Maifanitum boccaro cooking device outward appearance that the present invention prepares is regular, and Maifanitum mud layer combines together with base substrate, table
Face is smooth, has some strength and wearability, it is adaptable to cooking food and cleaning.The quality of goods meets GB/T10816 " boccaro
Pottery " and QB/T2580 " fine ceramics cooking device " standard-required, the lead of goods, quantity of cadmium release meet GB12651 2003 " with
The ceramic lead of food contact, quantity of cadmium release tolerance limit " standard-required, article topsheet has the activity of Maifanitum, useful
Trace element energy dissolution and can ionizing.
Detailed description of the invention
Embodiment: the preparation method of Maifanitum boccaro cooking device, it is characterised in that comprise the following production steps that
(1) prepared by blank
By the preparation method of Production of Ceramics blank, take blank stock through ball milling, sieve, press filt, old, pugging, prepare pledge
Measure the blank that moisture content is 21% standby;
Described raw material is that purple clay, Kaolin, spodumene, Talcum, clay mix;
(2) Maifanitum slurrying
Take Maifanitum 80 weight portion, above-mentioned standby blank 20 weight portion as raw material;
Above-mentioned Maifanitum is 5 hours through 400 DEG C of calcinings, calcination time;
Adding clear water after being mixed by above-mentioned raw materials and carry out wet ball grinding, cross 325 mesh sieves through ball milling raw material, through sieving, storage deposited in by raw material
Stock tank is carried out old 30 hours, and adding clear water through old raw material, to be deployed into the Maifanitum mud that concentration is 35 Baume degrees standby;
(3) product molding
Take above-mentioned standby blank, use roller head machine to carry out roll forming, prepare shale base substrate;
(4) repaired biscuit
Use soft cloth and clear water, the above-mentioned shale billet surface through molding is carried out reconditioning, makes shale billet surface smooth, will repair
Shale base substrate after base is deposited at shady and cool ventilation, natural airing 9 hours;
(5) high temperature biscuiting
Shale base substrate through airing carrying out high temperature biscuiting, is i.e. to use conventional kiln to carry out biscuiting, biscuiting temperature is 1200
DEG C, the biscuiting time is 13 hours, and biscuiting atmosphere is oxidizing atmosphere;
(6) Maifanitum mud is used
Above-mentioned standby Maifanitum mud is deposited in the stainless steel cask of opening;
Ceramic base substrate after above-mentioned biscuiting is heated, is i.e. to be positioned over ceramic base substrate in kiln to be heated to ceramic billet surface temperature
Degree is 75 DEG C;
Being soaked by heated ceramic base substrate in the Maifanitum mud of stainless steel cask inner face, the immersion time is 4 seconds, allows ceramic
Billet surface absorption mud, through absorption mud ceramic base substrate at pulp after, deposit in nature airing 4 hours at shady and cool ventilation;
(7) easy fired
Use conventional Production of Ceramics kiln, to carrying out easy fired through using the ceramic base substrate of Maifanitum mud, burn till into
900 DEG C, firing time is 7 hours, prepares Maifanitum boccaro cooking device.
The Maifanitum boccaro cooking device outward appearance that the present embodiment prepares is regular, and Maifanitum mud layer combines together with base substrate,
Surfacing, has some strength and wearability, it is adaptable to cooking food and cleaning.It is " purple that the quality of goods meets GB/T10816
Sand pottery " and QB/T2580 " fine ceramics cooking device " standard-required, the lead of goods, quantity of cadmium release meet GB12651 2003
" contact with food ceramic lead, quantity of cadmium release tolerance limit " standard-required, article topsheet has the activity of Maifanitum, has
The trace element energy dissolution of benefit and energy ionizing.
Comparative example 1: unlike embodiment, Maifanitum makes blank with blank stock after mixing, goods only with
1200 DEG C of high temperature burn till, and the activity of Maifanitum is destroyed, and the beneficial element of Maifanitum cannot dissolution.
Comparative example 2: unlike embodiment, Maifanitum makes blank with blank stock after mixing, goods are only with 900
DEG C easy fired, product strength is poor, it is easy to damaged, and the quality of goods is loosened, not up to vitrification, and impact uses.
Comparative example 3: unlike embodiment, the temperature of goods easy fired brings up to 1100 DEG C, the activity of Maifanitum
The most destroyed.
Comparative example 4: unlike embodiment, ceramic base substrate does not carry out Temperature Treatment before using Maifanitum mud, pottery
The midge ability of matter base substrate, mud absorption is uneven, does not reaches the thickness of requirement.
Comparative example 5: unlike embodiment, Maifanitum mud in preparation without old, the differences in viscosity of mud, shadow
Ring mud application effect.
Comparative example 6: unlike embodiment, is added without blank in the preparation of Maifanitum mud, goods are at easy fired
In, it is poor that mud layer is combined with ceramic base substrate, it is easy to produces delamination.
Claims (2)
1. the preparation method of Maifanitum boccaro cooking device, it is characterised in that comprise the following production steps that
(1) prepared by blank
By the preparation method of Production of Ceramics blank, take blank stock through ball milling, sieve, press filt, old, pugging, prepare pledge
Measure the blank that moisture content is 20 22% standby;
(2) Maifanitum slurrying
Take Maifanitum 78 82 weight portion, above-mentioned standby blank 18 22 weight portion as raw material;
Above-mentioned Maifanitum is 5 hours through 380 420 DEG C of calcinings, calcination time;
Adding clear water after being mixed by above-mentioned raw materials and carry out wet ball grinding, cross 325 mesh sieves through ball milling raw material, through sieving, storage deposited in by raw material
Stock tank is carried out old 24 36 hours, and adding clear water through old raw material, to be deployed into the Maifanitum mud that concentration is 32 36 Baume degrees standby
With;
(3) product molding
Take above-mentioned standby blank, use roller head machine to carry out roll forming, prepare shale base substrate;
(4) repaired biscuit
Use soft cloth and clear water, the above-mentioned shale billet surface through molding is carried out reconditioning, makes shale billet surface smooth, will repair
Shale base substrate after base is deposited at shady and cool ventilation, natural airing 8 10 hours;
(5) high temperature biscuiting
Shale base substrate through airing carrying out high temperature biscuiting, is i.e. to use conventional kiln to carry out biscuiting, biscuiting temperature is
1190 1210 DEG C, the biscuiting time is 12 14 hours, and biscuiting atmosphere is oxidizing atmosphere, becomes through the shale base substrate of biscuiting and has
The ceramic base substrate of some strength;
(6) Maifanitum mud is used
Above-mentioned standby Maifanitum mud is deposited in the stainless steel cask of opening;
Ceramic base substrate after above-mentioned biscuiting is heated, is i.e. to be positioned over ceramic base substrate in kiln to be heated to ceramic billet surface temperature
Degree is 70 80 DEG C;
Being soaked by heated ceramic base substrate in the Maifanitum mud of stainless steel cask inner face, the immersion time is 35 seconds, allows
Ceramic billet surface absorption mud, through absorption mud ceramic base substrate at pulp after, deposit in nature airing 3 at shady and cool ventilation
5 hours;
(7) easy fired
Use conventional Production of Ceramics kiln, to carrying out easy fired through using the ceramic base substrate of Maifanitum mud, burn till into
900 DEG C, firing time is 68 hours, prepares Maifanitum boccaro cooking device.
2. method described in claim 1, it is characterised in that described in step (1), raw material is purple clay, Kaolin, spodumene, cunning
Stone, clay.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109431192A (en) * | 2018-12-22 | 2019-03-08 | 洛阳脉渡文化传播有限公司 | A kind of production method of medical stone teapot |
CN115433002A (en) * | 2022-08-23 | 2022-12-06 | 秦皇岛日福陶瓷有限公司 | Medical stone ceramic product and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109431192A (en) * | 2018-12-22 | 2019-03-08 | 洛阳脉渡文化传播有限公司 | A kind of production method of medical stone teapot |
CN115433002A (en) * | 2022-08-23 | 2022-12-06 | 秦皇岛日福陶瓷有限公司 | Medical stone ceramic product and preparation method thereof |
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