CN106278114A - A kind of rotor magnetic steel rotor material and preparation method thereof - Google Patents
A kind of rotor magnetic steel rotor material and preparation method thereof Download PDFInfo
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- CN106278114A CN106278114A CN201610668244.6A CN201610668244A CN106278114A CN 106278114 A CN106278114 A CN 106278114A CN 201610668244 A CN201610668244 A CN 201610668244A CN 106278114 A CN106278114 A CN 106278114A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B20/00—Use of materials as fillers for mortars, concrete or artificial stone according to more than one of groups C04B14/00 - C04B18/00 and characterised by shape or grain distribution; Treatment of materials according to more than one of the groups C04B14/00 - C04B18/00 specially adapted to enhance their filling properties in mortars, concrete or artificial stone; Expanding or defibrillating materials
- C04B20/02—Treatment
- C04B20/023—Chemical treatment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00008—Obtaining or using nanotechnology related materials
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- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
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- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Hard Magnetic Materials (AREA)
Abstract
The invention discloses a kind of rotor magnetic steel rotor material and preparation method thereof, described rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 20 30 parts, aluminium oxide 20 30 parts, zinc oxide 10 20 parts, calcium oxide 10 15 parts, nylon fiber 10 15 parts, ammonium chloride 8 10 parts, 24 parts of silica gel, glycerol 24 parts；Rotor magnetic steel rotor material prepared by the present invention has higher wear-resistant, antioxidant resistance to elevated temperatures.
Description
Technical field
The present invention relates to a kind of field of material technology, specifically a kind of rotor magnetic steel rotor material and preparation method thereof.
Background technology
Traditional rotor magnetic steel rotor material generally uses SiO 2 powder uniformly to mix with resin material, is pressed into
Rotor, owing to silicon dioxide mixes with resin material, easily forms the mixture that quality is uneven, and in use, quality is uneven
Even rotor material easily causes the abrasion of rotor；Therefore research and develop novel rotor magnetic steel rotor material, be the most urgent appointing
Business.
Summary of the invention
It is an object of the invention to provide a kind of rotor magnetic steel rotor material and preparation method thereof, to solve above-mentioned background
The problem proposed in technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 20-30
Part, aluminium oxide 20-30 part, zinc oxide 10-20 part, calcium oxide 10-15 part, nylon fiber 10-15 part, ammonium chloride 8-10 part, silicon
Glue 2-4 part, glycerol 2-4 part；The preparation method of described nano modification silicon dioxide: first by sodium carboxymethyl cellulose, polyethylene
Alcohol, dicyclohexylcarbodiimide mix and carry out vacuum filtration process obtain mixture, then by mixture and silicon dioxide powder
End carries out reacting i.e. obtaining nano modification silicon dioxide under microwave.
As the further scheme of the present invention: described rotor magnetic steel rotor material, according to the primary raw material of weight portion it is:
Nano modification silicon dioxide 24-28 part, aluminium oxide 26-27 part, zinc oxide 12-17 part, calcium oxide 10-15 part, nylon fiber 10-
15 parts, ammonium chloride 8-10 part, silica gel 2-4 part, glycerol 2-4 part；The preparation method of described nano modification silicon dioxide: first by carboxylic
Sodium carboxymethylcellulose pyce, polyvinyl alcohol, dicyclohexylcarbodiimide mix and carry out vacuum filtration process obtain mixture, then will
Mixture and SiO 2 powder carry out reacting i.e. obtaining nano modification silicon dioxide under microwave.
As the further scheme of the present invention: described rotor magnetic steel rotor material, according to the primary raw material of weight portion it is:
Nano modification silicon dioxide 27 parts, aluminium oxide 27 parts, zinc oxide 14 parts, calcium oxide 13 parts, nylon fiber 14 parts, ammonium chloride 9 parts,
3 parts of silica gel, glycerol 3 parts；The preparation method of described nano modification silicon dioxide: first by sodium carboxymethyl cellulose, polyvinyl alcohol,
Dicyclohexylcarbodiimide mixes and carries out vacuum filtration and processes and obtain mixture, then mixture and SiO 2 powder is existed
Carry out under microwave reacting i.e. obtaining nano modification silicon dioxide.
As the further scheme of the present invention: the particle diameter of described aluminium oxide is 178 μm.
As the further scheme of the present invention: the mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1245-1500 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 300-600W, and the time is 50-60 minute, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
As the further scheme of the present invention: in step (1), fusion temperature is 1378 DEG C.
Compared with prior art, the invention has the beneficial effects as follows:
Rotor magnetic steel rotor material prepared by the present invention has higher wear-resistant, antioxidant resistance to elevated temperatures.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 20 parts, oxygen
Change 20 parts of aluminum, zinc oxide 10 parts, calcium oxide 10 parts, nylon fiber 10 parts, ammonium chloride 8 parts, 2 parts of silica gel, glycerol 2 parts；Described receive
The preparation method of rice improved silica: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed also
Carry out vacuum filtration process and obtain mixture, then carry out reacting i.e. being received under microwave by mixture and SiO 2 powder
Rice improved silica；The particle diameter of described aluminium oxide is 178 μm；The mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1245 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 300W, and the time is 50 minutes, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
Embodiment 2
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 24 parts, oxygen
Change 26 parts of aluminum, zinc oxide 12 parts, calcium oxide 10 parts, nylon fiber 10 parts, ammonium chloride 8 parts, 2 parts of silica gel, glycerol 2 parts；Described receive
The preparation method of rice improved silica: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed also
Carry out vacuum filtration process and obtain mixture, then carry out reacting i.e. being received under microwave by mixture and SiO 2 powder
Rice improved silica；The particle diameter of described aluminium oxide is 178 μm；The mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1245 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 300W, and the time is 50 minutes, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
Embodiment 3
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 27 parts, oxygen
Change 27 parts of aluminum, zinc oxide 14 parts, calcium oxide 13 parts, nylon fiber 14 parts, ammonium chloride 9 parts, 3 parts of silica gel, glycerol 3 parts；Described receive
The preparation method of rice improved silica: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed also
Carry out vacuum filtration process and obtain mixture, then carry out reacting i.e. being received under microwave by mixture and SiO 2 powder
Rice improved silica；The particle diameter of described aluminium oxide is 178 μm；The mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1378 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 450W, and the time is 55 minutes, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
Embodiment 4
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 28 parts, oxygen
Change 27 parts of aluminum, zinc oxide 17 parts, calcium oxide 15 parts, nylon fiber 15 parts, ammonium chloride 10 parts, 4 parts of silica gel, glycerol 4 parts；Described receive
The preparation method of rice improved silica: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed also
Carry out vacuum filtration process and obtain mixture, then carry out reacting i.e. being received under microwave by mixture and SiO 2 powder
Rice improved silica；The particle diameter of described aluminium oxide is 178 μm；The mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1500 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 600W, and the time is 60 minutes, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
Embodiment 5
A kind of rotor magnetic steel rotor material, according to the primary raw material of weight portion be: nano modification silicon dioxide 30 parts, oxygen
Change 30 parts of aluminum, zinc oxide 20 parts, calcium oxide 15 parts, nylon fiber 15 parts, ammonium chloride 10 parts, 4 parts of silica gel, glycerol 4 parts；Described receive
The preparation method of rice improved silica: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed also
Carry out vacuum filtration process and obtain mixture, then carry out reacting i.e. being received under microwave by mixture and SiO 2 powder
Rice improved silica；The particle diameter of described aluminium oxide is 178 μm；The mesh number of described zinc oxide is 600 mesh.
The preparation method of a kind of rotor magnetic steel rotor material, concretely comprises the following steps:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, processes in agitator
90min, melts subsequently, and fusion temperature is 1500 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carry out sonic oscillation subsequently
Processing, the power that sonic oscillation processes is 600W, and the time is 60 minutes, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (7)
1. a rotor magnetic steel rotor material, it is characterised in that according to the primary raw material of weight portion be: nano modification titanium dioxide
Silicon 20-30 part, aluminium oxide 20-30 part, zinc oxide 10-20 part, calcium oxide 10-15 part, nylon fiber 10-15 part, ammonium chloride 8-
10 parts, silica gel 2-4 part, glycerol 2-4 part；The preparation method of described nano modification silicon dioxide: first by sodium carboxymethyl cellulose,
Polyvinyl alcohol, dicyclohexylcarbodiimide mix and carry out vacuum filtration process obtain mixture, then by mixture and dioxy
SiClx powder carries out reacting i.e. obtaining nano modification silicon dioxide under microwave.
Rotor magnetic steel rotor material the most according to claim 1, it is characterised in that described rotor magnetic steel rotor material
Material, according to the primary raw material of weight portion be: nano modification silicon dioxide 24-28 part, aluminium oxide 26-27 part, zinc oxide 12-17
Part, calcium oxide 10-15 part, nylon fiber 10-15 part, ammonium chloride 8-10 part, silica gel 2-4 part, glycerol 2-4 part；Described nanometer changes
The preparation method of property silicon dioxide: first sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed and carry out
Vacuum filtration processes and obtains mixture, then carries out reacting under microwave by mixture and SiO 2 powder and i.e. obtains nanometer and change
Property silicon dioxide.
Rotor magnetic steel rotor material the most according to claim 1 and 2, it is characterised in that described rotor magnetic steel rotor
Material, according to the primary raw material of weight portion be: nano modification silicon dioxide 27 parts, aluminium oxide 27 parts, zinc oxide 14 parts, calcium oxide
13 parts, nylon fiber 14 parts, ammonium chloride 9 parts, 3 parts of silica gel, glycerol 3 parts；The preparation method of described nano modification silicon dioxide: first
First sodium carboxymethyl cellulose, polyvinyl alcohol, dicyclohexylcarbodiimide are mixed and carry out vacuum filtration and process and obtain mixture,
Then carry out reacting under microwave i.e. obtaining nano modification silicon dioxide by mixture and SiO 2 powder.
Rotor magnetic steel rotor material the most according to claim 3, it is characterised in that the particle diameter of described aluminium oxide is 178 μ
m。
Rotor magnetic steel rotor material the most according to claim 3, it is characterised in that the mesh number of described zinc oxide is 600
Mesh.
6. the preparation method of the rotor magnetic steel rotor material as described in claim 1-5 is arbitrary, it is characterised in that concrete
Step is:
(1) first, nano modification silicon dioxide puts into aluminium oxide, zinc oxide, calcium oxide, agitator processes 90min,
Melting subsequently, fusion temperature is 1245-1500 DEG C, obtains melting solid；
(2) then, melting solid is mixed homogeneously with nylon fiber, ammonium chloride, silica gel, glycerol, carries out sonic oscillation process subsequently,
The power that sonic oscillation processes is 300-600W, and the time is 50-60 minute, obtains mixture I；
(3) last, mixture I is carried out oven drying at low temperature pelletize, obtains rotor magnetic steel rotor material.
The preparation method of rotor magnetic steel rotor material the most according to claim 6, it is characterised in that molten in step (1)
Changing temperature is 1378 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610668244.6A CN106278114A (en) | 2016-08-11 | 2016-08-11 | A kind of rotor magnetic steel rotor material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610668244.6A CN106278114A (en) | 2016-08-11 | 2016-08-11 | A kind of rotor magnetic steel rotor material and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54102220A (en) * | 1978-01-31 | 1979-08-11 | Toshiba Corp | Tarbine rotor material |
| US20110076410A1 (en) * | 2009-09-30 | 2011-03-31 | Andrew Jay Skoog | Method for making strain tolerant corrosion protective coating compositions and coated articles |
| CN104258737A (en) * | 2014-09-10 | 2015-01-07 | 山东工业陶瓷研究设计院有限公司 | Preparation method of large-size thin-wall hollow flat-plate ceramic film |
| CN103758746B (en) * | 2014-01-17 | 2015-10-28 | 钢铁研究总院 | A kind of steel-bimetal copper-steel rotor and manufacture method thereof |
| CN105152638A (en) * | 2015-09-02 | 2015-12-16 | 安徽万年针织有限公司 | Aluminum oxide ceramic hole containing coal residues |
-
2016
- 2016-08-11 CN CN201610668244.6A patent/CN106278114A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54102220A (en) * | 1978-01-31 | 1979-08-11 | Toshiba Corp | Tarbine rotor material |
| US20110076410A1 (en) * | 2009-09-30 | 2011-03-31 | Andrew Jay Skoog | Method for making strain tolerant corrosion protective coating compositions and coated articles |
| CN103758746B (en) * | 2014-01-17 | 2015-10-28 | 钢铁研究总院 | A kind of steel-bimetal copper-steel rotor and manufacture method thereof |
| CN104258737A (en) * | 2014-09-10 | 2015-01-07 | 山东工业陶瓷研究设计院有限公司 | Preparation method of large-size thin-wall hollow flat-plate ceramic film |
| CN105152638A (en) * | 2015-09-02 | 2015-12-16 | 安徽万年针织有限公司 | Aluminum oxide ceramic hole containing coal residues |
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Application publication date: 20170104 |