CN106269506A - A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device - Google Patents
A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device Download PDFInfo
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- CN106269506A CN106269506A CN201610706973.6A CN201610706973A CN106269506A CN 106269506 A CN106269506 A CN 106269506A CN 201610706973 A CN201610706973 A CN 201610706973A CN 106269506 A CN106269506 A CN 106269506A
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- district
- catalyst
- hot blast
- guide portion
- air inducing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B7/00—Selective separation of solid materials carried by, or dispersed in, gas currents
- B07B7/01—Selective separation of solid materials carried by, or dispersed in, gas currents using gravity
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B11/00—Arrangement of accessories in apparatus for separating solids from solids using gas currents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B11/00—Arrangement of accessories in apparatus for separating solids from solids using gas currents
- B07B11/02—Arrangement of air or material conditioning accessories
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B11/00—Arrangement of accessories in apparatus for separating solids from solids using gas currents
- B07B11/06—Feeding or discharging arrangements
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- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
The invention discloses a kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device, including crane, classifying bunker, electromagnetism discharge valve, balance dispenser, electrical heating wind district, hot blast distribution guide portion, control zone, classification adjustable plate, the first air inducing district, the second air inducing district and the collecting region of multiple correspondence, described crane is connected with classifying bunker, described balance dispenser is arranged on the lower section of the discharging opening of top classifying bunker, described electromagnetism discharge valve is arranged on top classifying bunker discharge outlet, and described electrical heating wind district is arranged on the side below balance dispenser.Grading effect of the present invention is good, can reach more than 98%, classification process use hot blast as separating power, catalyst is nonhygroscopic, dust can be collected by sharp separation, safe and environment-friendly, classification process does not has catalyst shake broken phenomenon and catalyst abrasion loss phenomenon, and just can separate simply by the presence of density contrast.
Description
Technical field
The present invention relates to grading plant technical field, particularly relate to a kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physics
Grading plant.
Background technology
Continuous reformer is the device for the purpose of producing high-octane gasoline blending component and aromatic hydrocarbons.Its reaction exists
Carry out equipped with in the mobile bed radial reactor of catalyst made from platonic, during plant running, both can add in reactor
Add catalyst, it is also possible to from reactor, draw off catalyst.
Nearest period plant running within about 3 years, be one cycle, therebetween due to upstream raw material factor and behaviour in running
Factor of making has local run aways phenomenon to form dwarf's ball, owing to dwarf's the biggest catalyst of ball intensity produces mill in cyclic process sometimes
Damage, have partial catalyst wear and tear in cyclic process in the course of time and diminish, this part diminish catalyst be easy for blocking Johnson
Net and not circular regeneration, carbon deposition quantity of catalyst of long duration the most constantly rises and ultimately forms Johnson's selvage temperature runaway tympanites modification
(often occur in and bottom four anticentre pipes, heave horizontal strength fracture race agent phenomenon).
Catalyst the most constantly circulates, and makes the surfaces externally and internally of catalyst can produce knot carbon.Device is in general feelings
Under condition, the highest control of carbon deposition quantity can circular regeneration below 6%.
In catalyst recycle process, having partial catalyst that circulation is not fully achieved, the catalyst that this part does not flow claims
For " dead band catalyst ", for several times after circulation, the carbon deposition quantity of dead band catalyst may be up to 20~50%, when unloading catalyst, dead band
Catalyst can be entrained in low C catalyst outside outflow device, so forms catalyst contamination, and quantity depends on the scale of device, sets
The operating procedure that meter and catalyst draw off is relevant, and pollution rate reduces many, typically 5%~about 35%.
Existing experience have shown that, if in catalyst containing about 3% high C catalyst (phosphorus content > 8%), this catalyst
Should not use again, dead band agent or to accompany the agent of part dead band for the damage of equipment be during regenerator is turned " burning in vain " by " black burning "
Occur.Under " black burning " operating mode, the oxygen distribution of regenerator is: scorch region oxygen content is 0.5~1.3%, and oxychlorination district oxygen content is
0%;Under " in vain burn " operating mode, the oxygen distribution of regenerator is: scorch region oxygen content is 0.5~1.3%, oxychlorination district oxygen content be 4~
20%.The dead band catalyst of graphitization burns slowly under the environment of scorch region, " black burning ", after turning " burning in vain ", dead band agent is by burning
When Jiao Qu enters oxychlorination district, can burn rapidly under oxygen environment at 510 DEG C of high temperature, 4~20%, produce high temperature, sometimes temperature
Up to more than 1100 DEG C, the fusing of regenerator internals can be made, make sintering of catalyst.
Reformer unload during agent by dead band catalyst contamination catalyst medium high carbon catalyst total mass fraction about 5%~
35%, wherein 95~65% is the catalyst that can be continuing with.Therefore dress can not directly be returned, it is necessary to use windmill type classification skill
The catalyst that can return dress use is branched away by art, and in population in Zhenhai Refine-Chemical Company, five four reforming technique grading effects reach more than 98%.
At present, the shortcoming that the pellet type catalyst vibrating fluidized bed density classification technology of domestic use exists has (1) classification to imitate
Fruit is the highest;(2) there is abrasion that (3) in the classification process catalyst easy moisture absorption is lost;(4) density contrast catalyst below 3% can not divide
Level.
Summary of the invention
The invention aims to solve shortcoming present in prior art, and a kind of reforming catalyst negative pressure proposed
Fluidization windmill type physical fractionation device.
To achieve these goals, present invention employs following technical scheme:
A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device, unloads including crane, classifying bunker, electromagnetism
Material valve, balance dispenser, electrical heating wind district, hot blast distribution guide portion, control zone, classification adjustable plate, the first air inducing district, second draw
Wind district and the collecting region of multiple correspondence, described crane is connected with classifying bunker, and described balance dispenser is arranged on top classification
The lower section of the discharging opening of feed bin, described electromagnetism discharge valve is arranged on top classifying bunker discharge outlet, and described electrical heating wind district sets
Putting the side below balance dispenser, described hot blast distribution guide portion is arranged on the opposite side below balance dispenser, described
Control zone is arranged on the side away from electrical heating wind district, the hot blast distribution guide portion, and described classification adjustable plate is arranged on control zone, heat
Bottom between wind distribution guide portion, described control zone is provided with the first air inducing away from the upper end of the side of hot blast distribution guide portion
District, lower end is provided with the second air inducing district, and the plurality of collecting region is arranged on electrical heating wind district, hot blast distribution guide portion, control zone, divides
Level adjustable plate, the bottom in the second air inducing district.
Preferably, the quantity of described classification adjustable plate is 2.
Preferably, the plurality of collecting region includes coarse powder dirt collecting region, low-carbon (LC) catalyst collection district, the catalysis of little granule low-carbon (LC)
Agent collecting region, high-carbon catalyst collection district, dwarf's ball collecting region, described coarse powder dirt collecting region is positioned at control zone, the second air inducing district
Between bottom, described low-carbon (LC) catalyst collection district is positioned at the bottom between 2 classification adjustable plates, and described little granule low-carbon (LC) is catalyzed
Bottom between control zone and classification adjustable plate, the agent collecting region, described high-carbon catalyst collection district, dwarf's ball collecting region set
Put the bottom between hot blast distribution guide portion and classification adjustable plate, and high-carbon catalyst collection district is positioned close to hot blast distribution
The side of guide portion.
Preferably, described first air inducing district, the second air inducing district are respectively arranged with the first air-introduced machine, the second air-introduced machine.
Windmill type classification principle: using windmill ultimate principle is catalyst to be risen to certain eminence uniformly throw down, and
Make catalyst also make synchronous cross motion under the effect of horizontal hot wind, at this moment same volume, that density differs catalyst is the most front
After separate, owing to dividing into guiding adjustable plate, be adjusted according to the phosphorus content of catalyst, in classification process guide regulation
Plate, catalyst flow and classification air quantity three are mutually auxiliary to be connected, and in classification process, the random one that sets is as definite value, other two
Can regulate therewith.
In the present invention, grading effect is good, can reach more than 98%, uses hot blast as separating power, urge in classification process
Agent is nonhygroscopic, and dust can be collected by sharp separation, safe and environment-friendly, does not has catalyst to shake broken phenomenon and catalyst in classification process
Deterioration phenomenon, and just can separate simply by the presence of density contrast.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device that the present invention proposes
Figure.
In figure: 1 crane, 2 classifying bunkers, 3 electromagnetism discharge valves, 4 balance dispensers, 5 electrical heating wind districts, 6 hot blast distributions
Guide portion, 7 control zones, 8 classification adjustable plates, 9 first air inducing districts, 10 second air inducing districts, 11 coarse powder dirt collecting regions, 12 low-carbon (LC) catalysis
Agent collecting region, 13 little granule low-carbon (LC) catalyst collection districts, 14 high-carbon catalyst collection districts, 15 dwarf's ball collecting regions.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Describe, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments wholely.
With reference to Fig. 1, a kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device, including crane 1, classification material
Storehouse 2, electromagnetism discharge valve 3, balance dispenser 4, electrical heating wind district 5, hot blast distribution guide portion 6, control zone 7, classification adjustable plate 8,
First the 9, second air inducing district 10 of air inducing district and the collecting region of multiple correspondence, crane 1 is connected with classifying bunker 2, balances dispenser 4
Being arranged on the lower section of the discharging opening of top classifying bunker 2, electromagnetism discharge valve 3 is arranged on top classifying bunker 2 discharge outlet, and electricity adds
Hot blast district 5 is arranged on the side below balance dispenser 4, and hot blast distribution guide portion 6 is arranged on another below balance dispenser 4
Side, control zone 7 is arranged on the side away from electrical heating wind district 5, the hot blast distribution guide portion 6, and classification adjustable plate 8 is arranged on control zone
7, the bottom between hot blast distribution guide portion 6, the upper end of the side that control zone 7 is distributed guide portion 6 away from hot blast is provided with first and draws
Wind district 9, lower end is provided with the second air inducing district 10, and multiple collecting regions are arranged on electrical heating wind district 5, hot blast distribution guide portion 6, control zone
7, the bottom in classification adjustable plate the 8, second air inducing district 10.
The quantity of classification adjustable plate 8 is 2, and multiple collecting regions include coarse powder dirt collecting region 11, low-carbon (LC) catalyst collection district
12, little granule low-carbon (LC) catalyst collection district 13 (particle diameter≤1.2mm), high-carbon catalyst collection district 14, dwarf's ball collecting region 15, slightly
Bottom between the 7, second air inducing district 10, control zone, the dust collection district 11, low-carbon (LC) catalyst collection district 12 is positioned at 2 classifications
Bottom between adjustable plate 8, bottom between control zone 7 and classification adjustable plate 8, the little granule low-carbon (LC) catalyst collection district 13,
High-carbon catalyst collection district 14, dwarf's ball collecting region 15 are arranged on the end between hot blast distribution guide portion 6 and classification adjustable plate 8
Hold, and high-carbon catalyst collection district 14 is positioned close to the side of hot blast distribution guide portion 6, the 9, second air inducing district of the first air inducing district
10 are respectively arranged with the first air-introduced machine, the second air-introduced machine.
Technological process is: risen in top classifying bunker 2 by 1 bucket equipped with catalyst of crane, classifying bunker 2 times
Mouth is provided with electromagnetism discharge valve 3 and controls the deadweight flow of catalyst, and when certain gap opened by electromagnetism discharge valve 3, catalyst is from density current
Under on balance dispenser 4, catalyst is uniformly dished out exactly by the effect of balance dispenser 4.By the first air-introduced machine and second
Air-introduced machine carries out air inducing simultaneously, because it is unlimited that surrounding seals only electrical heating wind district 5, therefore during air-introduced machine work, hot blast passes
Catalyst leaves region, makes its transverse movement to power to the catalyst left,
When granular size is identical, the catalyst left is transported in the same direction under horizontal hot blast power by density compared with small catalyst
Action is fallen different positions and collects.
Grading effect is good, can reach more than 98%, uses hot blast as separating power in classification process, and catalyst is not inhaled
Tide, dust can sharp separation collect, safe and environment-friendly, classification process does not has catalyst shake broken phenomenon and catalyst abrasion loss
Phenomenon, and just can separate simply by the presence of density contrast.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (4)
1. a reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device, it is characterised in that: include crane, classification material
Storehouse, electromagnetism discharge valve, balance dispenser, electrical heating wind district, hot blast distribution guide portion, control zone, classification adjustable plate, the first air inducing
District, the second air inducing district and the collecting region of multiple correspondence, described crane is connected with classifying bunker, and described balance dispenser is arranged on
The lower section of the discharging opening of top classifying bunker, described electromagnetism discharge valve is arranged on top classifying bunker discharge outlet, and described electricity adds
Hot blast district is arranged on the side below balance dispenser, and described hot blast distribution guide portion is arranged on another below balance dispenser
Side, described control zone is arranged on the side away from electrical heating wind district, the hot blast distribution guide portion, and described classification adjustable plate is arranged on control
Bottom between district processed, hot blast distribution guide portion, described control zone is provided with the away from the upper end of side of hot blast distribution guide portion
One air inducing district, lower end is provided with the second air inducing district, and the plurality of collecting region is arranged on electrical heating wind district, hot blast distribution guide portion, control
District processed, classification adjustable plate, the bottom in the second air inducing district.
A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device the most according to claim 1, its feature exists
In: the quantity of described classification adjustable plate is 2.
A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device the most according to claim 2, its feature exists
In: the plurality of collecting region includes coarse powder dirt collecting region, low-carbon (LC) catalyst collection district, little granule low-carbon (LC) catalyst collection district, height
C catalyst collecting region, dwarf's ball collecting region, bottom between control zone, the second air inducing district, the described coarse powder dirt collecting region,
Described low-carbon (LC) catalyst collection district is positioned at the bottom between 2 classification adjustable plates, described little granule low-carbon (LC) catalyst collection position
Bottom between control zone and classification adjustable plate, described high-carbon catalyst collection district, dwarf's ball collecting region are arranged on hot blast point
Bottom between cloth guide portion and classification adjustable plate, and high-carbon catalyst collection district be positioned close to hot blast distribution guide portion one
Side.
A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device the most according to claim 1, its feature exists
In: described first air inducing district, the second air inducing district are respectively arranged with the first air-introduced machine, the second air-introduced machine.
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CN201610706973.6A CN106269506A (en) | 2016-08-23 | 2016-08-23 | A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device |
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CN201610706973.6A CN106269506A (en) | 2016-08-23 | 2016-08-23 | A kind of reforming catalyst negative pressure fluidised form wind-transformation vehicle type physical fractionation device |
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2016
- 2016-08-23 CN CN201610706973.6A patent/CN106269506A/en active Pending
Patent Citations (8)
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CN2036872U (en) * | 1988-06-20 | 1989-05-03 | 郭振勋 | Electric dual-purpose aerovane for air and screen classification |
CN2542349Y (en) * | 2001-09-27 | 2003-04-02 | 鲁选民 | Circulating fanning mill shutter adjuster |
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