CN106260100A - A kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil and preparation method thereof - Google Patents
A kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil and preparation method thereof Download PDFInfo
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- CN106260100A CN106260100A CN201610668256.9A CN201610668256A CN106260100A CN 106260100 A CN106260100 A CN 106260100A CN 201610668256 A CN201610668256 A CN 201610668256A CN 106260100 A CN106260100 A CN 106260100A
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- Prior art keywords
- semen
- herba rosmarini
- rosmarini officinalis
- corm eleocharitis
- refreshment
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
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- Medicines Containing Plant Substances (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, it is prepared by the raw materials in: Fructus Jujubae 22 25, apple flower 23, Semen Chaenomelis 67, Periostracum cicadae 34, fresh Corm Eleocharitis skin 15 20, Pleurotus geesteranus 35 36, VC1 2, citric acid 12, tartaric acid 12, Semen arachidis hypogaeae 200 250, Semen Brassicae campestris 100 150, Semen Sesami 20 30, lavandula angustifolia 1.7 2.3, Herba Rosmarini Officinalis 1.7 2, Usnea 1.2 2, phosphate buffer is appropriate;Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide all have certain inhibitory action to the oxidation of edible oil and fat, can delay the oxidation deterioration of oils and fats and goods thereof;Corm Eleocharitis skin is a kind of natural waste resource, has no side effect, and is expected to become the novel natural food antioxidant of great potential.
Description
Technical field
The present invention relates to mixed oil technical field, particularly relate to a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil and preparation side thereof
Method.
Background technology
Lipid peroxidation is the one of the main reasons of grease deterioration, and it can cause oils and fats and goods flavor variations, nutrition
It is worth and declines, and be eaten for a long time and can affect health, be possible to prevent the oxidizing acid of edible oil and fat by adding antioxidant
Lose.Therefore, from natural plants, screen high-efficiency low-toxicity and the strong Natural antioxidant of non-oxidizability becomes focus of concern.
Corm Eleocharitis skin is the by-product of Corm Eleocharitis processing, and its quality accounts for the 20%-25% of fresh Corm Eleocharitis, and stock number is the biggest.Corm Eleocharitis skin leads to
Often being dropped with form of waste, this not only wastes resource, and pollutes environment.At present, both at home and abroad Corm Eleocharitis skin is opened
Send out research on utilization and be concentrated mainly on the aspect such as bacteriostatic activity and pigment extraction.Additionally, also there is research to point out, Corm Eleocharitis peel extract exists
Free radical system has antioxidant activity, and Corm Eleocharitis peel extract is to the antioxidation of oils and fats, and there is not been reported.
Pleurotus geesteranus, has another name called Pleurotus geesteranus, and it is nutritious, rich in proteins, carbohydrate, vitamin and calcium, magnesium,
The mineral such as copper, zinc, can improve immune function of human body, has anticancer, blood fat reducing, intestine moistening stomach and beauty treatment etc. to human body and makees
With, Pleurotus geesteranus principle active component is polysaccharide.
Therefore, this research is intended to inquire into the polysaccharide extracted in Pleurotus geesteranus and the Corm Eleocharitis peel extract antioxygen to edible oil and fat
Change effect, provides theoretical foundation to the exploitation for Pleurotus geesteranus polysaccharide and Corm Eleocharitis skin resource.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil and
Preparation method.
The present invention is achieved by the following technical solutions:
A kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, is prepared by the raw materials in:
Fructus Jujubae 22-25, apple flower 2-3, Semen Chaenomelis 6-7, Periostracum cicadae 3-4, fresh Corm Eleocharitis skin 15-20, Pleurotus geesteranus 35-36, VC1-2,
Citric acid 1-2, tartaric acid 1-2, Semen arachidis hypogaeae 200-250, Semen Brassicae campestris 100-150, Semen Sesami 20-30, lavandula angustifolia 1.7-2.3, Herba Rosmarini Officinalis
1.7-2, Usnea 1.2-2, phosphate buffer is appropriate.
The preparation method of described a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, comprises the following steps:
(1) by lavandula angustifolia, Herba Rosmarini Officinalis, after the Usnea flooding by 6-9 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine
Powder;
(2) take extracting red date stone chopping, the material handled well is mixed with apple flower, Periostracum cicadae and pours in pot, with the water logging of 6-9 times amount
After carrying, then squeeze serosity in jointly pouring serum pressing machine into, by pouring step (1) gained Chinese medicine powder in gained serosity into, mix stand-by;
(3) take Semen Chaenomelis, after Semen arachidis hypogaeae, Semen Brassicae campestris, Semen Sesami clean roguing, stir-fry respectively in being placed in pot to surface checking shape, will at
The material managed and step (2) gained material mixing digestion 20-25 minute, take out drain away the water stand-by;By gained drying materials
It is placed on the intrinsic pressure expressed oil of pressafiner, obtains mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20-30 mesh sieve, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, be dried after cleaning
Pulverize, cross 40-45 mesh sieve, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring the mixing extraction of 60-70% ethanol into, meeting solid-liquid ratio is 1: 23-25, and holding temperature is 60-
70 DEG C, extraction time is 3-3.5h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2-3 time, takes out
Filter, merging filtrate, concentrated after lyophilization again, obtain Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4-0.45%, after mix homogeneously, pour mixed system weight into
Measure the phosphate buffer of 18-22 times, after mixing is mixed thoroughly, enzymolysis 2-3h at 40-45 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, freeze
Dry, obtain Pleurotus geesteranus polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
, a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil described in 2 and preparation method thereof, described phosphate buffer forms into
It is divided into: potassium dihydrogen phosphate 30-32g, 1-1.2mol/lNaOH solution 175-180ml, distilled water 800-850ml.
The invention have the advantage that Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide all have certain suppression to the oxidation of edible oil and fat
Effect, can delay the oxidation deterioration of oils and fats and goods thereof;Corm Eleocharitis skin is a kind of natural waste resource, has no side effect, is expected to into
Novel natural food antioxidant for great potential;
Meanwhile, Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide compound with VC, citric acid, tartaric acid can play synergistic function, compounding
Synergistic function, this potentiation is had to be owing to these synergists are to some gold in edible oil and fat the non-oxidizability of oil
Belonging to ion such as Cu 2+, Fe2+, Mn2+ etc. have sequestration effect, form slaine, enable and promote that the trace metal ion of oxidation is blunt
Change, no longer there is the ability of catalyzed oil lipid oxidation, thus add Corm Eleocharitis peel extract, the antioxidant effect of Pleurotus geesteranus polysaccharide;
Nutrition sweet-smelling of the present invention, long shelf-life, be also added with lavandula angustifolia, Herba Rosmarini Officinalis, the food medical material such as Usnea, it is clear that richness has given the present invention
Livering expectorant, elimination flatulence, memory reinforcing, the health-care effect of refreshment.
Detailed description of the invention
A kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, is prepared by the raw materials in:
Fructus Jujubae 22, apple flower 2, Semen Chaenomelis 6, Periostracum cicadae 3, fresh Corm Eleocharitis skin 15, Pleurotus geesteranus 35, VC1, citric acid 1, tartaric acid 1, flower
Life 200, Semen Brassicae campestris 100, Semen Sesami 20, lavandula angustifolia 1.7, Herba Rosmarini Officinalis 1.7, Usnea 1.2, phosphate buffer is appropriate.
The preparation method of described a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, comprises the following steps:
(1) by lavandula angustifolia, Herba Rosmarini Officinalis, after the Usnea flooding by 6 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine
Powder;
(2) take extracting red date stone chopping, the material handled well is mixed with apple flower, Periostracum cicadae and pours in pot, by the flooding of 6 times amount
After, then squeeze serosity in jointly pouring serum pressing machine into, by pouring step (1) gained Chinese medicine powder in gained serosity into, mix stand-by;
(3) take Semen Chaenomelis, after Semen arachidis hypogaeae, Semen Brassicae campestris, Semen Sesami clean roguing, stir-fry respectively in being placed in pot to surface checking shape, will at
The material managed and step (2) gained material mixing digestion 20 minutes, take out drain away the water stand-by;By rearmounted for gained drying materials
In the intrinsic pressure expressed oil of pressafiner, obtain mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20 mesh sieves, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, xeraphium after cleaning
Broken, cross 40 mesh sieves, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring 60% ethanol mixing extraction into, meeting solid-liquid ratio is 1: 23, and keeping temperature is 60 DEG C, extraction
Time is 3h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2 times, and sucking filtration, merging filtrate, through dense
Lyophilization again after contracting, obtains Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4%, after mix homogeneously, pour mixed system weight 18 into
Times phosphate buffer, after mixing is mixed thoroughly, enzymolysis 2h at 40 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, lyophilizing, obtain Pleurotus geesteranus
Polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
Described a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil and preparation method thereof, described phosphate buffer constituent
For: potassium dihydrogen phosphate 30g, 1mol/lNaOH solution 175ml, distilled water 800ml.
Claims (3)
1. a Herba Rosmarini Officinalis liver heat removing refreshment mixed oil, it is characterised in that be prepared by the raw materials in:
Fructus Jujubae 22-25, apple flower 2-3, Semen Chaenomelis 6-7, Periostracum cicadae 3-4, fresh Corm Eleocharitis skin 15-20, Pleurotus geesteranus 35-36, VC1-2,
Citric acid 1-2, tartaric acid 1-2, Semen arachidis hypogaeae 200-250, Semen Brassicae campestris 100-150, Semen Sesami 20-30, lavandula angustifolia 1.7-2.3, Herba Rosmarini Officinalis
1.7-2, Usnea 1.2-2, phosphate buffer is appropriate.
The preparation method of a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil the most as claimed in claim 1, it is characterised in that include following
Step:
(1) by lavandula angustifolia, Herba Rosmarini Officinalis, after the Usnea flooding by 6-9 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine
Powder;
(2) take extracting red date stone chopping, the material handled well is mixed with apple flower, Periostracum cicadae and pours in pot, with the water logging of 6-9 times amount
After carrying, then squeeze serosity in jointly pouring serum pressing machine into, by pouring step (1) gained Chinese medicine powder in gained serosity into, mix stand-by;
(3) take Semen Chaenomelis, after Semen arachidis hypogaeae, Semen Brassicae campestris, Semen Sesami clean roguing, stir-fry respectively in being placed in pot to surface checking shape, will at
The material managed and step (2) gained material mixing digestion 20-25 minute, take out drain away the water stand-by;By gained drying materials
It is placed on the intrinsic pressure expressed oil of pressafiner, obtains mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20-30 mesh sieve, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, be dried after cleaning
Pulverize, cross 40-45 mesh sieve, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring the mixing extraction of 60-70% ethanol into, meeting solid-liquid ratio is 1: 23-25, and holding temperature is 60-
70 DEG C, extraction time is 3-3.5h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2-3 time, takes out
Filter, merging filtrate, concentrated after lyophilization again, obtain Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4-0.45%, after mix homogeneously, pour mixed system weight into
Measure the phosphate buffer of 18-22 times, after mixing is mixed thoroughly, enzymolysis 2-3h at 40-45 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, freeze
Dry, obtain Pleurotus geesteranus polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
3. according to a kind of Herba Rosmarini Officinalis liver heat removing refreshment mixed oil described in claim 1,2 and preparation method thereof, it is characterised in that: institute
The phosphate buffer constituent stated is: potassium dihydrogen phosphate 30-32g, 1-1.2mol/lNaOH solution 175-180ml, distillation
Water 800-850ml.
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Citations (3)
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CN103493906A (en) * | 2013-08-29 | 2014-01-08 | 潘逸东 | Preparation method of heat-clearing dampness-draining health care edible oil |
CN103651965A (en) * | 2013-11-22 | 2014-03-26 | 安徽大平油脂有限公司 | Three-flower health care oil with blood-activating function |
CN105076495A (en) * | 2015-09-23 | 2015-11-25 | 成都艾比科生物科技有限公司 | Health-care blend oil and making method thereof |
-
2016
- 2016-08-16 CN CN201610668256.9A patent/CN106260100A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103493906A (en) * | 2013-08-29 | 2014-01-08 | 潘逸东 | Preparation method of heat-clearing dampness-draining health care edible oil |
CN103651965A (en) * | 2013-11-22 | 2014-03-26 | 安徽大平油脂有限公司 | Three-flower health care oil with blood-activating function |
CN105076495A (en) * | 2015-09-23 | 2015-11-25 | 成都艾比科生物科技有限公司 | Health-care blend oil and making method thereof |
Non-Patent Citations (2)
Title |
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张俐勤 等: "荸荠皮提取物对食用油脂抗氧化作用研究", 《中国油脂》 * |
耿中华 等: "秀珍菇多糖的抗花生油氧化活性研究", 《食品工业》 * |
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Application publication date: 20170104 |