CN106260094A - A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation method thereof - Google Patents

A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation method thereof Download PDF

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Publication number
CN106260094A
CN106260094A CN201610668207.5A CN201610668207A CN106260094A CN 106260094 A CN106260094 A CN 106260094A CN 201610668207 A CN201610668207 A CN 201610668207A CN 106260094 A CN106260094 A CN 106260094A
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China
Prior art keywords
semen
rhizoma phragmitis
herba centellae
corm eleocharitis
pleurotus geesteranus
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CN201610668207.5A
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Chinese (zh)
Inventor
张涛
张�廷
张永霞
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Anhui Tian Jian Food Technology Co Ltd
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Anhui Tian Jian Food Technology Co Ltd
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Priority to CN201610668207.5A priority Critical patent/CN106260094A/en
Publication of CN106260094A publication Critical patent/CN106260094A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil, it is prepared by the raw materials in: Flos Eriobotryae 89, Flos Jasmini Sambac 8 10, Folium Cinnamomi porrecti 46, Fericarpium Citri Limoniae 56, fresh Corm Eleocharitis skin 15 20, Pleurotus geesteranus 35 36, VC1 2, citric acid 12, tartaric acid 12, Semen arachidis hypogaeae 200 250, Semen Brassicae campestris 100 150, Semen Sesami 20 30, Rhizoma Phragmitis 1.1 2, Semen Allii Tuberosi 1.1 3.2, Herba Centellae 1.5 3, phosphate buffer is appropriate;Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide all have certain inhibitory action to the oxidation of edible oil and fat, can delay the oxidation deterioration of oils and fats and goods thereof;Corm Eleocharitis skin is a kind of natural waste resource, has no side effect, and is expected to become the novel natural food antioxidant of great potential.

Description

A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation method thereof
Technical field
The present invention relates to mixed oil technical field, particularly relate to a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation side thereof Method.
Background technology
Lipid peroxidation is the one of the main reasons of grease deterioration, and it can cause oils and fats and goods flavor variations, nutrition It is worth and declines, and be eaten for a long time and can affect health, be possible to prevent the oxidizing acid of edible oil and fat by adding antioxidant Lose.Therefore, from natural plants, screen high-efficiency low-toxicity and the strong Natural antioxidant of non-oxidizability becomes focus of concern.
Corm Eleocharitis skin is the by-product of Corm Eleocharitis processing, and its quality accounts for the 20%-25% of fresh Corm Eleocharitis, and stock number is the biggest.Corm Eleocharitis skin leads to Often being dropped with form of waste, this not only wastes resource, and pollutes environment.At present, both at home and abroad Corm Eleocharitis skin is opened Send out research on utilization and be concentrated mainly on the aspect such as bacteriostatic activity and pigment extraction.Additionally, also there is research to point out, Corm Eleocharitis peel extract exists Free radical system has antioxidant activity, and Corm Eleocharitis peel extract is to the antioxidation of oils and fats, and there is not been reported.
Pleurotus geesteranus, has another name called Pleurotus geesteranus, and it is nutritious, rich in proteins, carbohydrate, vitamin and calcium, magnesium, The mineral such as copper, zinc, can improve immune function of human body, has anticancer, blood fat reducing, intestine moistening stomach and beauty treatment etc. to human body and makees With, Pleurotus geesteranus principle active component is polysaccharide.
Therefore, this research is intended to inquire into the polysaccharide extracted in Pleurotus geesteranus and the Corm Eleocharitis peel extract antioxygen to edible oil and fat Change effect, provides theoretical foundation to the exploitation for Pleurotus geesteranus polysaccharide and Corm Eleocharitis skin resource.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and Preparation method.
The present invention is achieved by the following technical solutions:
A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil, is prepared by the raw materials in:
Flos Eriobotryae 8-9, Flos Jasmini Sambac 8-10, Folium Cinnamomi porrecti 4-6, Fericarpium Citri Limoniae 5-6, fresh Corm Eleocharitis skin 15-20, Pleurotus geesteranus 35-36, VC1- 2, citric acid 1-2, tartaric acid 1-2, Semen arachidis hypogaeae 200-250, Semen Brassicae campestris 100-150, Semen Sesami 20-30, Rhizoma Phragmitis 1.1-2, Semen Allii Tuberosi 1.1-3.2, Herba Centellae 1.5-3, phosphate buffer is appropriate.
The preparation method of described a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil, comprises the following steps:
(1) by after Rhizoma Phragmitis, Semen Allii Tuberosi, the Herba Centellae flooding by 6-9 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine Powder;Take Flos Eriobotryae, Flos Jasmini Sambac, Folium Cinnamomi porrecti, the clean chopping of Fericarpium Citri Limoniae, and mix with Chinese medicine powder;
(2) take Semen arachidis hypogaeae, after Semen Brassicae campestris, Semen Sesami clean roguing, mix homogeneously with step (1) gained material, more jointly send into steamer Interior water proof fumigates 22-25 minute;
(3) the most jointly poured in frying pan by step (2) gained material, to stir-fry to surface be polygon in mixing, then will handle well Material is placed in the intrinsic pressure expressed oil of pressafiner, obtains mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20-30 mesh sieve, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, be dried after cleaning Pulverize, cross 40-45 mesh sieve, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring the mixing extraction of 60-70% ethanol into, meeting solid-liquid ratio is 1: 23-25, and holding temperature is 60- 70 DEG C, extraction time is 3-3.5h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2-3 time, takes out Filter, merging filtrate, concentrated after lyophilization again, obtain Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4-0.45%, after mix homogeneously, pour mixed system weight into Measure the phosphate buffer of 18-22 times, after mixing is mixed thoroughly, enzymolysis 2-3h at 40-45 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, freeze Dry, obtain Pleurotus geesteranus polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
, a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil described in 2 and preparation method thereof, described phosphate buffer forms into It is divided into: potassium dihydrogen phosphate 30-32g, 1-1.2mol/lNaOH solution 175-180ml, distilled water 800-850ml.
The invention have the advantage that Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide all have certain suppression to the oxidation of edible oil and fat Effect, can delay the oxidation deterioration of oils and fats and goods thereof;Corm Eleocharitis skin is a kind of natural waste resource, has no side effect, is expected to into Novel natural food antioxidant for great potential;
Meanwhile, Corm Eleocharitis peel extract, Pleurotus geesteranus polysaccharide compound with VC, citric acid, tartaric acid can play synergistic function, compounding Synergistic function, this potentiation is had to be owing to these synergists are to some gold in edible oil and fat the non-oxidizability of oil Belonging to ion such as Cu 2+, Fe2+, Mn2+ etc. have sequestration effect, form slaine, enable and promote that the trace metal ion of oxidation is blunt Change, no longer there is the ability of catalyzed oil lipid oxidation, thus add Corm Eleocharitis peel extract, the antioxidant effect of Pleurotus geesteranus polysaccharide;
Nutrition sweet-smelling of the present invention, long shelf-life, it is also added with the food medical materials such as Rhizoma Phragmitis, Semen Allii Tuberosi, Herba Centellae, it is clear that richness has given the present invention Heat is promoted the production of body fluid relieving restlessness, liver and kidney tonifying, the health-care effect of tonifying YANG controlling nocturnal emission with astringent drugs.
Detailed description of the invention
A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil, is prepared by the raw materials in:
Flos Eriobotryae 8, Flos Jasmini Sambac 8, Folium Cinnamomi porrecti 4, Fericarpium Citri Limoniae 5, fresh Corm Eleocharitis skin 15, Pleurotus geesteranus 35, VC1, citric acid 1, tartaric acid 1, Semen arachidis hypogaeae 200, Semen Brassicae campestris 100, Semen Sesami 20, Rhizoma Phragmitis 1.1, Semen Allii Tuberosi 1.1, Herba Centellae 1.5, phosphate buffer is appropriate.
The preparation method of described a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil, comprises the following steps:
(1) by after Rhizoma Phragmitis, Semen Allii Tuberosi, the Herba Centellae flooding by 6 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine Powder;Take Flos Eriobotryae, Flos Jasmini Sambac, Folium Cinnamomi porrecti, the clean chopping of Fericarpium Citri Limoniae, and mix with Chinese medicine powder;
(2) take Semen arachidis hypogaeae, after Semen Brassicae campestris, Semen Sesami clean roguing, mix homogeneously with step (1) gained material, more jointly send into steamer Interior water proof fumigates 22 minutes;
(3) the most jointly poured in frying pan by step (2) gained material, to stir-fry to surface be polygon in mixing, then will handle well Material is placed in the intrinsic pressure expressed oil of pressafiner, obtains mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20 mesh sieves, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, xeraphium after cleaning Broken, cross 40 mesh sieves, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring 60% ethanol mixing extraction into, meeting solid-liquid ratio is 1: 23, and keeping temperature is 60 DEG C, extraction Time is 3h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2 times, and sucking filtration, merging filtrate, through dense Lyophilization again after contracting, obtains Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4%, after mix homogeneously, pour mixed system weight 18 into Times phosphate buffer, after mixing is mixed thoroughly, enzymolysis 2h at 40 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, lyophilizing, obtain Pleurotus geesteranus Polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
Described a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation method thereof, described phosphate buffer constituent For: potassium dihydrogen phosphate 30g, 1mol/lNaOH solution 175ml, distilled water 800ml.

Claims (3)

1. a Herba Centellae Rhizoma Phragmitis draft mixed oil, it is characterised in that be prepared by the raw materials in:
Flos Eriobotryae 8-9, Flos Jasmini Sambac 8-10, Folium Cinnamomi porrecti 4-6, Fericarpium Citri Limoniae 5-6, fresh Corm Eleocharitis skin 15-20, Pleurotus geesteranus 35-36, VC1- 2, citric acid 1-2, tartaric acid 1-2, Semen arachidis hypogaeae 200-250, Semen Brassicae campestris 100-150, Semen Sesami 20-30, Rhizoma Phragmitis 1.1-2, Semen Allii Tuberosi 1.1-3.2, Herba Centellae 1.5-3, phosphate buffer is appropriate.
The preparation method of a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil the most as claimed in claim 1, it is characterised in that include following Step:
(1) by after Rhizoma Phragmitis, Semen Allii Tuberosi, the Herba Centellae flooding by 6-9 times amount, medicine juice is filtered to obtain, more spray-dried, obtain Chinese medicine Powder;Take Flos Eriobotryae, Flos Jasmini Sambac, Folium Cinnamomi porrecti, the clean chopping of Fericarpium Citri Limoniae, and mix with Chinese medicine powder;
(2) take Semen arachidis hypogaeae, after Semen Brassicae campestris, Semen Sesami clean roguing, mix homogeneously with step (1) gained material, more jointly send into steamer Interior water proof fumigates 22-25 minute;
(3) the most jointly poured in frying pan by step (2) gained material, to stir-fry to surface be polygon in mixing, then will handle well Material is placed in the intrinsic pressure expressed oil of pressafiner, obtains mixing oil plant;
(4) take fresh Corm Eleocharitis skin to dry, then after pulverizing, cross 20-30 mesh sieve, obtain Corm Eleocharitis skin coarse powder;Take Pleurotus geesteranus, be dried after cleaning Pulverize, cross 40-45 mesh sieve, obtain pleurotusgeesteranuspowder powder, collect standby;
(5) by Corm Eleocharitis skin coarse powder, pouring the mixing extraction of 60-70% ethanol into, meeting solid-liquid ratio is 1: 23-25, and holding temperature is 60- 70 DEG C, extraction time is 3-3.5h;Extracting solution after vacuum filtration, collects filtrate;Filtering residue same method extracts 2-3 time, takes out Filter, merging filtrate, concentrated after lyophilization again, obtain Corm Eleocharitis corium farinosum;
(6) take Pleurotus geesteranus sample, add the cellulase of its quality 0.4-0.45%, after mix homogeneously, pour mixed system weight into Measure the phosphate buffer of 18-22 times, after mixing is mixed thoroughly, enzymolysis 2-3h at 40-45 DEG C, then through enzyme denaturing, centrifugal, sucking filtration, freeze Dry, obtain Pleurotus geesteranus polysaccharide;
(7) by above-mentioned steps gained mixing oil plant and remain each material mix homogeneously, then sterilization filling, to obtain final product.
3. according to a kind of Herba Centellae Rhizoma Phragmitis draft mixed oil described in claim 1,2 and preparation method thereof, it is characterised in that: institute The phosphate buffer constituent stated is: potassium dihydrogen phosphate 30-32g, 1-1.2mol/lNaOH solution 175-180ml, distillation Water 800-850ml.
CN201610668207.5A 2016-08-16 2016-08-16 A kind of Herba Centellae Rhizoma Phragmitis draft mixed oil and preparation method thereof Pending CN106260094A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108102777A (en) * 2018-01-12 2018-06-01 张艳雪 A kind of cold pressing sesame oil full of nutrition and preparation method thereof
CN108157526A (en) * 2018-01-12 2018-06-15 张艳雪 A kind of cold pressing sesame oil and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103493906A (en) * 2013-08-29 2014-01-08 潘逸东 Preparation method of heat-clearing dampness-draining health care edible oil
CN103651965A (en) * 2013-11-22 2014-03-26 安徽大平油脂有限公司 Three-flower health care oil with blood-activating function

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103493906A (en) * 2013-08-29 2014-01-08 潘逸东 Preparation method of heat-clearing dampness-draining health care edible oil
CN103651965A (en) * 2013-11-22 2014-03-26 安徽大平油脂有限公司 Three-flower health care oil with blood-activating function

Non-Patent Citations (2)

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Title
张俐勤等: "荸荠皮提取物对食用油脂抗氧化作用研究", 《中国油脂》 *
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108102777A (en) * 2018-01-12 2018-06-01 张艳雪 A kind of cold pressing sesame oil full of nutrition and preparation method thereof
CN108157526A (en) * 2018-01-12 2018-06-15 张艳雪 A kind of cold pressing sesame oil and preparation method thereof

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Application publication date: 20170104