CN106259496A - 一种协同增效的樱花树用杀虫剂及其制备方法 - Google Patents

一种协同增效的樱花树用杀虫剂及其制备方法 Download PDF

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CN106259496A
CN106259496A CN201610668198.XA CN201610668198A CN106259496A CN 106259496 A CN106259496 A CN 106259496A CN 201610668198 A CN201610668198 A CN 201610668198A CN 106259496 A CN106259496 A CN 106259496A
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Abstract

本发明提供了一种协同增效的樱花树用杀虫剂及其制备方法，该杀虫剂包括杀虫剂组分与增效组分，杀虫剂组分包括：氨基甲酸酯、八氯二丙醚、丁香油、啶虫脒、溴氰菊酯、氯氟氰虫酰、丙酮酸乙酯、乙酸酐、乙酸乙酯；增效组分包括：蓖麻油、油酸甘油酯、乳化硅油、2‑氨基‑2‑甲基‑1‑丙醇、乙酸乙酯、乙醇。其制备方法是先分别配制杀虫剂组分与增效组分，然后将其混合，即得。本发明提供的协同增效的樱花树用杀虫剂对樱花树上蚜虫、红蜘蛛和介壳虫具有显著的防治作用，喷洒樱花树后，并不影响樱花树新梢的生长，而且，使用本发明杀虫剂的樱花树，其叶色、叶片数量和质量明显优于空白。

Description

一种协同增效的樱花树用杀虫剂及其制备方法
技术领域
本发明属于杀虫剂技术领域，具体涉及一种协同增效的樱花树用杀虫剂及其制备方法。
背景技术
樱花又名山樱花、福岛樱、青肤樱等，蔷薇科李亚科落叶乔木。樱花是世界著名的花木，我国是樱花主要原产地之一。早在秦汉时期，樱花栽培就已经用于宫苑之中，唐朝时普遍出现在私家庭院。目前我国樱花树种植面积大，栽培面积一直呈持续增长的趋势，但樱花树虫害的发生率及防治方法一直未能较好解决。
长期以来，由于单剂的长期应用，室内外滞留喷洒防治卫生害虫如蚊、蝇、蜚蠊等出现了防效普遍降低的现象，这是由于单剂的长期使用导致卫生害虫对药剂的抗性增加。因此需要一种环保高效的农药复配品种来延缓卫生害虫抗药性的产生，通过多种农药药剂的复配，这样不仅能提高对卫生害虫的防治效果，而且经济方便，延缓卫生害虫抗药性的产生。
发明内容
本发明的目的是克服现有技术的不足而提供一种协同增效的樱花树用杀虫剂及其制备方法，该杀虫剂对樱花树上蚜虫、红蜘蛛和介壳虫具有显著的防治作用。
一种协同增效的樱花树用杀虫剂，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯5-8份，八氯二丙醚3-6份，丁香油2-4份，啶虫脒2-4份，溴氰菊酯1-3份，氯氟氰虫酰3-5份，丙酮酸乙酯5-8份，乙酸酐0.5-1份，乙酸乙酯40-60份；增效组分以重量份计包括：蓖麻油1-2份，油酸甘油酯2-4份，乳化硅油0.5-1份，2-氨基-2-甲基-1-丙醇1-3份，乙酸乙酯2-6份，乙醇5-8份。
所述协同增效的樱花树用杀虫剂的制备方法，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至50-60℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌40-60min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流15-20min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至30-40℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌30-50min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
进一步地，步骤1中真空条件的真空度为0.02-0.05MPa。
进一步地，步骤1中搅拌速度为180-200rpm。
进一步地，步骤2中加热温度为70-90℃。
进一步地，步骤3中搅拌速度为180-200rpm。
本发明提供的协同增效的樱花树用杀虫剂对樱花树上蚜虫、红蜘蛛和介壳虫具有显著的防治作用，喷洒樱花树后，并不影响樱花树新梢的生长，而且，使用本发明杀虫剂的樱花树，其叶色、叶片数量和质量明显优于空白。
具体实施方式
实施例1
一种协同增效的樱花树用杀虫剂，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯5份，八氯二丙醚3份，丁香油2份，啶虫脒2份，溴氰菊酯1份，氯氟氰虫酰3份，丙酮酸乙酯5份，乙酸酐0.5份，乙酸乙酯40份；增效组分以重量份计包括：蓖麻油1份，油酸甘油酯2份，乳化硅油0.5份，2-氨基-2-甲基-1-丙醇1份，乙酸乙酯2份，乙醇5份。
所述协同增效的樱花树用杀虫剂的制备方法，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至50℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌40min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流15min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至30℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌30min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
其中，步骤1中真空条件的真空度为0.02MPa，搅拌速度为180rpm；步骤2中加热温度为70℃，步骤3中搅拌速度为180rpm。
实施例2
一种协同增效的樱花树用杀虫剂，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯7份，八氯二丙醚4份，丁香油3份，啶虫脒3份，溴氰菊酯2份，氯氟氰虫酰4份，丙酮酸乙酯7份，乙酸酐0.8份，乙酸乙酯48份；增效组分以重量份计包括：蓖麻油1.7份，油酸甘油酯2.7份，乳化硅油0.9份，2-氨基-2-甲基-1-丙醇1.3份，乙酸乙酯3份，乙醇7份。
所述协同增效的樱花树用杀虫剂的制备方法，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至55℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌50min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流18min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至35℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌40min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
其中，步骤1中真空条件的真空度为0.04MPa，搅拌速度为190rpm；步骤2中加热温度为80℃，步骤3中搅拌速度为190rpm。
实施例3
一种协同增效的樱花树用杀虫剂，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯7份，八氯二丙醚5份，丁香油3.2份，啶虫脒3.5份，溴氰菊酯2.4份，氯氟氰虫酰4份，丙酮酸乙酯7份，乙酸酐0.8份，乙酸乙酯50份；增效组分以重量份计包括：蓖麻油1.8份，油酸甘油酯3.2份，乳化硅油0.8份，2-氨基-2-甲基-1-丙醇1.7份，乙酸乙酯4份，乙醇7份。
所述协同增效的樱花树用杀虫剂的制备方法，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至55℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌50min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流18min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至30℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌40min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
其中，步骤1中真空条件的真空度为0.07MPa，搅拌速度为190rpm；步骤2中加热温度为80℃，步骤3中搅拌速度为190rpm。
实施例4
一种协同增效的樱花树用杀虫剂，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯8份，八氯二丙醚6份，丁香油4份，啶虫脒4份，溴氰菊酯3份，氯氟氰虫酰5份，丙酮酸乙酯8份，乙酸酐1份，乙酸乙酯60份；增效组分以重量份计包括：蓖麻油2份，油酸甘油酯4份，乳化硅油1份，2-氨基-2-甲基-1-丙醇3份，乙酸乙酯6份，乙醇8份。
所述协同增效的樱花树用杀虫剂的制备方法，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至60℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌60min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流20min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至40℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌50min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
其中，步骤1中真空条件的真空度为0.05MPa，搅拌速度为200rpm；步骤2中加热温度为90℃，步骤3中搅拌速度为200rpm。
将本发明的杀虫剂以1：3的比例稀释为1000mL后喷洒处理试验树，每隔7d喷洒一次，连续使用2个月后观察樱花树上蚜虫、红蜘蛛和介壳虫的防治率，结果如下：
由上表可知，本发明的杀虫剂对樱花树上蚜虫、红蜘蛛和介壳虫具有显著的防治作用，喷洒樱花树后，并不影响樱花树新梢的生长，而且，使用本发明杀虫剂的樱花树，其叶色、叶片数量和质量明显优于空白。

Claims (6)

1.一种协同增效的樱花树用杀虫剂，其特征在于，包括杀虫剂组分与增效组分，杀虫剂组分以重量份计包括：氨基甲酸酯5-8份，八氯二丙醚3-6份，丁香油2-4份，啶虫脒2-4份，溴氰菊酯1-3份，氯氟氰虫酰3-5份，丙酮酸乙酯5-8份，乙酸酐0.5-1份，乙酸乙酯40-60份；增效组分以重量份计包括：蓖麻油1-2份，油酸甘油酯2-4份，乳化硅油0.5-1份，2-氨基-2-甲基-1-丙醇1-3份，乙酸乙酯2-6份，乙醇5-8份。
2.权利要求1所述的协同增效的樱花树用杀虫剂的制备方法，其特征在于，包括以下步骤：
步骤1，将氨基甲酸酯、八氯二丙醚和丁香油混合，搅拌，在真空条件下升温至50-60℃，再加入啶虫脒、溴氰菊酯和氯氟氰虫酰和乙酸酐，继续搅拌40-60min，降至室温，得到混合物料；
步骤2，将混合物料加至乙酸乙酯中，再加入丙酮酸乙酯，加热回流15-20min，降至室温，得到杀虫剂组分；
步骤3，将蓖麻油溶于乙醇中，升温至30-40℃，加入乙酸乙酯、油酸甘油酯、2-氨基-2-甲基-1-丙醇和乳化硅油，搅拌30-50min，得到增效组分；
步骤4，将杀虫剂组分与增效组分混合，即得。
3.根据权利要求2所述的协同增效的樱花树用杀虫剂的制备方法，其特征在于，步骤1中真空条件的真空度为0.02-0.05MPa。
4.根据权利要求2所述的协同增效的樱花树用杀虫剂的制备方法，其特征在于，步骤1中搅拌速度为180-200rpm。
5.根据权利要求2所述的协同增效的樱花树用杀虫剂的制备方法，其特征在于，步骤2中加热温度为70-90℃。
6.根据权利要求2所述的协同增效的樱花树用杀虫剂的制备方法，其特征在于，步骤3中搅拌速度为180-200rpm。
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