CN106243880A - A kind of environment-friendly type high life true mineral varnish of anti-soil - Google Patents

A kind of environment-friendly type high life true mineral varnish of anti-soil Download PDF

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Publication number
CN106243880A
CN106243880A CN201610724000.5A CN201610724000A CN106243880A CN 106243880 A CN106243880 A CN 106243880A CN 201610724000 A CN201610724000 A CN 201610724000A CN 106243880 A CN106243880 A CN 106243880A
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mineral varnish
true mineral
rotating speed
soil
environment
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CN106243880B (en
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刘清白
李建勇
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Anhui Furui snow chemical Polytron Technologies Inc
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FUYANG FURUIXUE CHEMICAL TECHNOLOGY Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/16Antifouling paints; Underwater paints
    • C09D5/1656Antifouling paints; Underwater paints characterised by the film-forming substance
    • C09D5/1662Synthetic film-forming substance
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/16Antifouling paints; Underwater paints
    • C09D5/1687Use of special additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16Fibres; Fibrils

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of environment-friendly type high life true mineral varnish of anti-soil, be made up of following component: pure-acrylic emulsion, silester, modified acacia, Oleum Ricini, activated silica ashes, dispersant, dodecyl sodium sulfate, tapioca, polyurethane thickener, coalescents, hollow glass microbead, defoamer, Folium Nelumbinis pulp-water, natural colour sand, modified wood fibre;Compared with prior art, the present invention true mineral varnish appearance colour is gorgeous, and the most attractive in appearance, environmental protection, adhesive force is extremely strong, water resistance is outstanding but also can effectively protect building not corroded by adverse circumstances, extends its service life;The true mineral varnish service life prepared through inventive formulation extends 2 2.5 times compared to common true mineral varnish, color sand makes true mineral varnish have colourful color, and can not fade, the present invention prepares the true mineral varnish of gained and has the effect of imitative stone, also there is certain heat insulation property, being a kind of novel building energy-saving material having many uses, market prospect is boundless.

Description

A kind of environment-friendly type high life true mineral varnish of anti-soil
Technical field
The present invention relates to decoration material field, particularly relate to a kind of environment-friendly type high life true mineral varnish of anti-soil.
Background technology
True mineral varnish is that a kind of decorative effect exactly likes marble, granite, the building after true mineral varnish decoration, have natural very Real natural colour, gives graceful harmonious, serious aesthetic feeling, is suitable for the interior/exterior decoration of various building, can receive Vividly, true to nature, effect of back to nature, existing true mineral varnish materials are that normal quartz sand makees smalt.Existing true mineral varnish glues Connecing property is poor, and adhesive force ratio is relatively low, the phenomenon that crackle comes off easily occurs, and its life-span is the highest, it is impossible to meet many fields on market The demand closed;And existing true mineral varnish has just painted complete, the true mineral varnish metope caused due to air reason, dust and granule Contamination phenomenon is serious, there is presently no and finds good solution, can only be that workmen adds construction is painted when Note and repeatedly repair, wanting thoroughly to solve such difficulty, it is necessary to finding one i.e. economy rational solution again.
Summary of the invention
In order to overcome above-mentioned deficiency, the invention provides a kind of environment-friendly type high life true mineral varnish of anti-soil.
The present invention is achieved through the following technical solutions:
A kind of environment-friendly type high life true mineral varnish of anti-soil, is made up of following component: pure-acrylic emulsion 35-38, silicic acid second by weight Ester 0.1-0.2, tapioca 0.4-0.6, modified acacia 1.0-1.2, Oleum Ricini 0.8-1.0, activated silica ashes 0.6- 0.8, dispersant 0.3-0.4, dodecyl sodium sulfate 0.7-0.9, polyurethane thickener 0.4-0.6, coalescents 1.2-1.5, Hollow glass microbead 0.6-1.0, defoamer 0.1-0.2, Folium Nelumbinis pulp-water 24-30, natural colour sand 65-68, modified wood fibre 0.6-0.8;
The preparation method of described modified wood fibre is: add the deionized water of its 10 times of quality in wood fibre, with 120r/ When min rotating speed stirs and is heated to 78 DEG C, add the ascorbic acid of wood fibre quality 0.2%, stir with 90r/min rotating speed Mix 10min, continue to be heated to 86 DEG C, then add the sodium hydroxide of wood fibre quality 1.2%, stir with 120r/min rotating speed After 20min, insulation, at 80-82 DEG C, drips the acrylic acid of wood fibre quality 1.8% in the 1h time, turns with 250r/min simultaneously Speed stirring 15min, then temperature is reduced to 72-74 DEG C, it is incubated 20min, then temperature is reduced to 42-44 DEG C, filters, Surface uses temperature to be that 12-15 DEG C of deionized water cleans 2-3 time, dries at 38-40 DEG C,;
The preparation method of described modified acacia powder is: add its quality 10% water and the methyl of 1% in Radix Acaciae senegalis Propane sulfonic acid, when stirring with 150r/min rotating speed and be heated to 66 DEG C, then adds the carboxylic of gum arabic powder quality 0.8% Sodium carboxymethylcellulose pyce, stirs 10min with 120r/min rotating speed, the most again it is used microwave treatment, and microwave power is 200W, place After the reason time is 45s, adds the flake zinc powder of Radix Acaciae senegalis quality 10%, temperature is adjusted to 78 DEG C, with 1200r/min Rotating speed stirring 20min,;
The preparation method of described Folium Nelumbinis pulp-water is: smashed to pieces by Folium Nelumbinis, and single Folium Nelumbinis granule is not less than 80 mesh, adds Folium Nelumbinis quality 50 Times water, after stirring 15 minutes with 800r/min rotating speed, then stirs 10r/min with 1800r/min rotating speed, to obtain final product.
Further, during described dispersant is anionic sodium polyacrylate, sodium tripolyphosphate any one.
Further, described coalescents is that alcohol ester 12, ethylene glycol monobutyl ether are mixed by 4:3 mass ratio.
Further, any during described defoamer is nonionic defoamer, molecular antifoaming agent, organic silicon defoamer Two kinds of mixed in equal amounts are made.The present invention is by using appointing in nonionic defoamer, molecular antifoaming agent, organic silicon defoamer Two kinds of mixed in equal amounts of anticipating make defoamer, and antifoam performance improves 1-1.5 times than single defoamer performance, reduces defoamer Usage amount, has saved the cost of defoamer greatly.
Further, described natural colour sand is that the natural colour sand of the natural colour sand of 100-140 mesh and 80-90 mesh is by 1:0.3 Mass ratio mix.
Further, described Oleum Ricini is through twice high-temperature heating treatment: be first heated to 1 DEG C/10s speed by Oleum Ricini 182 DEG C, it is incubated 4min, is then cooled to 12 DEG C with 1 DEG C/5s speed, be incubated 10min, then be heated to 200 with 1 DEG C/5s speed DEG C, it being incubated 2min, be then cooled to 10 DEG C with the speed of 1 DEG C/10s, after insulation 5min, clear-cutting forestland is to room temperature.Through twice Oleum Ricini after high-temperature heating treatment improves compared to without the water resistance of the Oleum Ricini true mineral varnish to making processed 2-3 times, add its temperature adaptation performance of true mineral varnish made without the Oleum Ricini processed and execute under conditions of-2-40 DEG C Work, and it is higher to add its thermal adaptability of true mineral varnish that Oleum Ricini after twice high-temperature heating treatment makes, can-8 DEG C- Construct under conditions of 65 DEG C, different regions and the demand of different building can be met, and use through twice high temperature The present invention true mineral varnish paint film hot strength that Oleum Ricini after heat treated is made and elongation at break compared to add without The true mineral varnish that the Oleum Ricini processed is made has been respectively increased 23% and 28%, the Oleum Ricini after twice high-temperature process and activated silica Ashes, the synergism of dodecyl sodium sulfate, it is possible to improve greatly the anti-pollution characteristic of the true mineral varnish of the present invention, it is to avoid construction The repairing repeatedly in personnel's later stage, has saved substantial amounts of man power and material.
A kind of preparation method of the environment-friendly type high life true mineral varnish of anti-soil, it comprises the following steps:
(1), Folium Nelumbinis pulp-water is added in dispersion cylinder, under 250-280r/min stirring, add pure-acrylic emulsion, stir 12- 15min;
(2), under the rotating speed of 250-280r/min, add silester, modified acacia powder, Oleum Ricini, then improve and turn Speed is to 380-400r/min, and stirs 15-18min under this rotating speed;
(3), stop addition activated silica ashes, modified wood fibre, dodecyl sodium sulfate after stirring, control rotating speed at 700- 12-15min is stirred under 750r/min stirring;
(4), stir after, continue to be slowly added into successively dispersant, tapioca, poly-under 700-750r/min stirring Urethane thickening agent, coalescents, hollow glass microbead, defoamer, obtain true mineral varnish base paste after being sufficiently stirred for 12-15min;
(5), finally by the above-mentioned true mineral varnish base paste prepared mix with natural colour sand, blowing after mix homogeneously, barrelling.
Wood fibre has excellent pliability and dispersibility, owing to wood fibre is organic fiber, so unavoidably It is added in true mineral varnish and can be affected, such as corrosion, cause the reduction of effect, the present invention is by wood fibre modification Reason, thus improves wood fibre surface corrosion resistance, and improves the surface compatability of wood fibre so that its with in the present invention Between other composition, concertedness is higher, thus improves the performance of true mineral varnish further, by adding modification wood fibre of the present invention, The true mineral varnish making preparation has the strongest antifreeze, a solar heat protection ability, and true mineral varnish paint film specific surface area reduces, and has high resistance to Dirty performance.
Radix Acaciae senegalis has gumminess and stability, the higher floating energy that flake zinc powder shows in water paint The advantages such as power, covering power and screening ability receive the concern of people, but flake zinc powder is used directly in water paint existence Wetting and dispersing is difficult, resistance to settling is poor, the problems such as reunion easily occur, thus affects the mechanical performance of coating, limits to a certain extent Make its application.The present invention is by being modified Radix Acaciae senegalis, by being carried out with Radix Acaciae senegalis by flake zinc powder In conjunction with, with Radix Acaciae senegalis as carrier such that it is able to overcome the problems such as flake zinc powder free settling, bad dispersibility, and flakey Zinc powder enables to again gum arabic-stabilized and gumminess is further enhanced, it is possible to improve the true stone of preparation further The adhesive force of paint, and the excellent stability of modified Radix Acaciae senegalis can improve the life-span of true mineral varnish further.
The invention has the beneficial effects as follows: compared with prior art, the present invention true mineral varnish appearance colour is gorgeous, the most attractive in appearance, Environmental protection, adhesive force is extremely strong, water resistance is outstanding and can effectively protect building not corroded by adverse circumstances, extends it and uses Life-span;The synergism of silester and tapioca can be effectively improved the adhesive force of true mineral varnish, and film forming is more uniform, natural, Thus improve coating quality and coating life further, this true mineral varnish product after film forming, dust appended by coating surface and dirt Can be clean after stain warp rain-out, easily exempt the trouble that labor cleaning is brought, saved human cost, through this True mineral varnish service life prepared by bright formula extends 2-2.5 times compared to common true mineral varnish, enhances the pliability of coating, adopts The Folium Nelumbinis pulp-water prepared by the present invention makes the weatherability of the true mineral varnish of the present invention, anti-pollution characteristic be greatly improved, and, dry The dry time is significantly shortened, and shortens more than 38% compared to the drying time of common true mineral varnish, thus reduces true stone Paint is dried the probability that period is the most damaged and pollutes.
Color sand makes true mineral varnish have colourful color, and can not fade, and the present invention prepares the true stone of gained Paint has the effect of imitative stone, also has certain heat insulation property, is a kind of novel building energy-saving material having many uses, market Prospect is boundless.
Detailed description of the invention
A kind of environment-friendly type high life true mineral varnish of anti-soil, is made up of following component: pure-acrylic emulsion 35-38, silicon by weight Acetoacetic ester 0.1-0.2, tapioca 0.4-0.6, modified acacia 1.0-1.2, Oleum Ricini 0.8-1.0, activated silica ashes 0.6-0.8, dispersant 0.3-0.4, dodecyl sodium sulfate 0.7-0.9, polyurethane thickener 0.4-0.6, coalescents 1.2- 1.5, hollow glass microbead 0.6-1.0, defoamer 0.1-0.2, Folium Nelumbinis pulp-water 24-30, natural colour sand 65-68, modified wooden fibre Dimension 0.6-0.8;
The preparation method of described modified wood fibre is: add the deionized water of its 10 times of quality in wood fibre, with 120r/ When min rotating speed stirs and is heated to 78 DEG C, add the ascorbic acid of wood fibre quality 0.2%, stir with 90r/min rotating speed Mix 10min, continue to be heated to 86 DEG C, then add the sodium hydroxide of wood fibre quality 1.2%, stir with 120r/min rotating speed After 20min, insulation, at 80-82 DEG C, drips the acrylic acid of wood fibre quality 1.8% in the 1h time, turns with 250r/min simultaneously Speed stirring 15min, then temperature is reduced to 72-74 DEG C, it is incubated 20min, then temperature is reduced to 42-44 DEG C, filters, Surface uses temperature to be that 12-15 DEG C of deionized water cleans 2-3 time, dries at 38-40 DEG C,;
The preparation method of described modified acacia powder is: add its quality 10% water and the methyl of 1% in Radix Acaciae senegalis Propane sulfonic acid, when stirring with 150r/min rotating speed and be heated to 66 DEG C, then adds the carboxylic of gum arabic powder quality 0.8% Sodium carboxymethylcellulose pyce, stirs 10min with 120r/min rotating speed, the most again it is used microwave treatment, and microwave power is 200W, place After the reason time is 45s, adds the flake zinc powder of Radix Acaciae senegalis quality 10%, temperature is adjusted to 78 DEG C, with 1200r/min Rotating speed stirring 20min,;
The preparation method of described Folium Nelumbinis pulp-water is: smashed to pieces by Folium Nelumbinis, and single Folium Nelumbinis granule is not less than 80 mesh, adds Folium Nelumbinis quality 50 Times water, after stirring 15 minutes with 800r/min rotating speed, then stirs 10r/min with 1800r/min rotating speed, to obtain final product.
Further, during described dispersant is anionic sodium polyacrylate, sodium tripolyphosphate any one.
Further, described coalescents is that alcohol ester 12, ethylene glycol monobutyl ether are mixed by 4:3 mass ratio.
Further, any during described defoamer is nonionic defoamer, molecular antifoaming agent, organic silicon defoamer Two kinds of mixed in equal amounts are made.
Further, described natural colour sand is that the natural colour sand of the natural colour sand of 100-140 mesh and 80-90 mesh is by 1:0.3 Mass ratio mix.
Further, described Oleum Ricini is through twice high-temperature heating treatment: be first heated to 1 DEG C/10s speed by Oleum Ricini 182 DEG C, it is incubated 4min, is then cooled to 12 DEG C with 1 DEG C/5s speed, be incubated 10min, then be heated to 200 with 1 DEG C/5s speed DEG C, it being incubated 2min, be then cooled to 10 DEG C with the speed of 1 DEG C/10s, after insulation 5min, clear-cutting forestland is to room temperature.
A kind of preparation method of the environment-friendly type high life true mineral varnish of anti-soil, it comprises the following steps:
(1), Folium Nelumbinis pulp-water is added in dispersion cylinder, under 250-280r/min stirring, add pure-acrylic emulsion, stir 12- 15min;
(2), under the rotating speed of 250-280r/min, add silester, modified acacia powder, Oleum Ricini, then improve and turn Speed is to 380-400r/min, and stirs 15-18min under this rotating speed;
(3), stop addition activated silica ashes, modified wood fibre, dodecyl sodium sulfate after stirring, control rotating speed at 700- 12-15min is stirred under 750r/min stirring;
(4), stir after, continue to be slowly added into successively dispersant, tapioca, poly-under 700-750r/min stirring Urethane thickening agent, coalescents, hollow glass microbead, defoamer, obtain true mineral varnish base paste after being sufficiently stirred for 12-15min;
(5), finally by the above-mentioned true mineral varnish base paste prepared mix with natural colour sand, blowing after mix homogeneously, barrelling.
The present invention true mineral varnish the performance test results:
Table 1
Wherein, comparative example 1 is: replace to without the Radix Acaciae senegalis processed by inventing modified acacia in true mineral varnish, Modification lignocellulose is replaced to common wood fibre, and other composition is identical with the present invention with preparation method.
As can be seen from Table 1, the present invention true mineral varnish various aspects of performance is more outstanding compared with common true mineral varnish, use without Cross the gum arabic powder processed and the true mineral varnish various aspects of performance prepared of common wood fibre has and to a certain degree reduces.

Claims (7)

1. the environment-friendly type high life true mineral varnish of anti-soil, it is characterised in that be made up of following component by weight: pure-acrylic emulsion 35-38, silester 0.1-0.2, tapioca 0.4-0.6, modified acacia 1.0-1.2, Oleum Ricini 0.8-1.0, work Property wollastonite powder 0.6-0.8, dispersant 0.3-0.4, dodecyl sodium sulfate 0.7-0.9, polyurethane thickener 0.4-0.6, film forming Auxiliary agent 1.2-1.5, hollow glass microbead 0.6-1.0, defoamer 0.1-0.2, Folium Nelumbinis pulp-water 24-30, natural colour sand 65-68, change Property wood fibre 0.6-0.8;
The preparation method of described modified wood fibre is: add the deionized water of its 10 times of quality in wood fibre, with 120r/ When min rotating speed stirs and is heated to 78 DEG C, add the ascorbic acid of wood fibre quality 0.2%, stir with 90r/min rotating speed Mix 10min, continue to be heated to 86 DEG C, then add the sodium hydroxide of wood fibre quality 1.2%, stir with 120r/min rotating speed After 20min, insulation, at 80-82 DEG C, drips the acrylic acid of wood fibre quality 1.8% in the 1h time, turns with 250r/min simultaneously Speed stirring 15min, then temperature is reduced to 72-74 DEG C, it is incubated 20min, then temperature is reduced to 42-44 DEG C, filters, Surface uses temperature to be that 12-15 DEG C of deionized water cleans 2-3 time, dries at 38-40 DEG C,;
The preparation method of described modified acacia powder is: add its quality 10% water and the methyl of 1% in Radix Acaciae senegalis Propane sulfonic acid, when stirring with 150r/min rotating speed and be heated to 66 DEG C, then adds the carboxylic of gum arabic powder quality 0.8% Sodium carboxymethylcellulose pyce, stirs 10min with 120r/min rotating speed, the most again it is used microwave treatment, and microwave power is 200W, place After the reason time is 45s, adds the flake zinc powder of Radix Acaciae senegalis quality 10%, temperature is adjusted to 78 DEG C, with 1200r/min Rotating speed stirring 20min,;
The preparation method of described Folium Nelumbinis pulp-water is: smashed to pieces by Folium Nelumbinis, and single Folium Nelumbinis granule is not less than 80 mesh, adds Folium Nelumbinis quality 50 Times water, after stirring 15 minutes with 800r/min rotating speed, then stirs 10r/min with 1800r/min rotating speed, to obtain final product.
A kind of environment-friendly type high life true mineral varnish of anti-soil the most according to claim 1, it is characterised in that described dispersant is cloudy In ion-type sodium polyacrylate, sodium tripolyphosphate any one.
A kind of environment-friendly type high life true mineral varnish of anti-soil the most according to claim 1, it is characterised in that described coalescents is Alcohol ester 12, ethylene glycol monobutyl ether are mixed by 4:3 mass ratio.
A kind of environment-friendly type high life true mineral varnish of anti-soil the most according to claim 1, it is characterised in that described defoamer is non- Any two kinds of mixed in equal amounts in ion-type defoamer, molecular antifoaming agent, organic silicon defoamer are made.
A kind of environment-friendly type high life true mineral varnish of anti-soil the most according to claim 1, it is characterised in that described natural colour sand is The natural colour sand of 100-140 mesh and the natural colour sand of 80-90 mesh are mixed by the mass ratio of 1:0.3.
A kind of environment-friendly type high life true mineral varnish of anti-soil the most according to claim 1, it is characterised in that described Oleum Ricini passes through Twice high-temperature heating treatment: first with 1 DEG C/10s speed, Oleum Ricini is heated to 182 DEG C, is incubated 4min, then with 1 DEG C/5s speed It is cooled to 12 DEG C, is incubated 10min, then is heated to 200 DEG C with 1 DEG C/5s speed, be incubated 2min, then drop with the speed of 1 DEG C/10s Temperature is to 10 DEG C, and after insulation 5min, clear-cutting forestland is to room temperature.
7., according to the preparation method of a kind of environment-friendly type high life true mineral varnish of anti-soil according to any one of claim 1-6, it is special Levying and be, it comprises the following steps:
(1), Folium Nelumbinis pulp-water is added in dispersion cylinder, under 250-280r/min stirring, add pure-acrylic emulsion, stir 12- 15min;
(2), under the rotating speed of 250-280r/min, add silester, modified acacia powder, Oleum Ricini, then improve and turn Speed is to 380-400r/min, and stirs 15-18min under this rotating speed;
(3), stop addition activated silica ashes, modified wood fibre, dodecyl sodium sulfate after stirring, control rotating speed at 700- 12-15min is stirred under 750r/min stirring;
(4), stir after, continue to be slowly added into successively dispersant, tapioca, poly-under 700-750r/min stirring Urethane thickening agent, coalescents, hollow glass microbead, defoamer, obtain true mineral varnish base paste after being sufficiently stirred for 12-15min;
(5), finally by the above-mentioned true mineral varnish base paste prepared mix with natural colour sand, blowing after mix homogeneously, barrelling.
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Cited By (5)

* Cited by examiner, † Cited by third party
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CN106590120A (en) * 2017-01-05 2017-04-26 安徽柏瑞特家居装饰品有限公司 Acid-alkali-resistant stone-like paint and preparation method thereof
CN111533492A (en) * 2020-04-29 2020-08-14 广东法兰迪涂料有限公司 Real stone paint and preparation method thereof
CN112974192A (en) * 2021-02-04 2021-06-18 杭州罗维标识系统工程有限公司 Preparation process of signboard
CN113429914A (en) * 2021-07-14 2021-09-24 广西美博新材料科技有限公司 Production process and application of nano micro silica powder stone waterproof back adhesive
CN114213952A (en) * 2021-12-28 2022-03-22 广东美涂士建材股份有限公司 Environment-friendly water-based paint and preparation method thereof

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CN104046182A (en) * 2014-05-23 2014-09-17 芜湖朗润新材料有限公司 Quick-drying lacquer
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CN111533492A (en) * 2020-04-29 2020-08-14 广东法兰迪涂料有限公司 Real stone paint and preparation method thereof
CN112974192A (en) * 2021-02-04 2021-06-18 杭州罗维标识系统工程有限公司 Preparation process of signboard
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CN114213952A (en) * 2021-12-28 2022-03-22 广东美涂士建材股份有限公司 Environment-friendly water-based paint and preparation method thereof

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