CN106214593A - A kind of moisturizing liquid containing nano active carbon and preparation method thereof - Google Patents
A kind of moisturizing liquid containing nano active carbon and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of moisturizing liquid containing nano active carbon, component meter by weight, mainly consists of the following composition: nano active carbon 0.01 0.1 parts, little molecule hyaluronic acid 3.2 5 parts, lecithin liposome 0.3 2 parts, coenzyme Q10 0.6 1.2 parts, glycerol 4 16 parts, propylene glycol 58 parts, rose extract 0.2 1.5 parts, allantoin 0.3 1.5 parts, amino acid humectant 0.3 0.8 parts, VE0.1 0.5 part, wheat malt germ extract 0.05 1 parts, oleum lini 0.05 0.1 parts, PEG 40 0.1 0.3 parts, purified water 30 80 parts.The moisturizing liquid of the present invention is applicable to all types of skin, it is particularly well-suited to the skin repair after micropin, phototherapy, all kinds of instrument treatment, moisturizing, moisturizing use, utilize high-end liposome technology, nutrient substance is made to be more easy to enter skin, reach quickly to repair, moisturizing, the effect of long-acting moisturizing, thus improve coarse, microgroove, be dried.
Description
Technical field
The present invention relates to technical field of skin care, be specifically related to a kind of moisturizing liquid containing nano active carbon and preparation thereof
Method.
Background technology
Along with economy, the improvement day by day of living standard, the basis maintenance of skin has become a part for daily life.Well
Skin be mainly manifested in the various aspects of the colour of skin, elasticity, gloss, texture and physiological function, and these are played crucial effect and make
Be exactly the water content of skin.The generally water content of epidermis and corium is about 75%, and outmost horny layer typically should not
Less than 10%, water content of stratum corneum is that the skin of 10-20% then shows as soft and moist, smooth, flexible, if less than 10%, then and skin
Skin horny layer can excessively be dried even to be there is squama or ruptures.Therefore, the deep water supplement for skin is only the U.S. that secures good health
The basic guarantee of beautiful skin.Although the most different total classes of moisturizing product is various, but most moisturizing skin care item are only capable of supplementary table
Moisture outside skin, increases water, the content of oil at skin surface, and cannot deeply improve the moisture of cortex, and this is not
Can fundamentally improve being dried of skin.
Secondly, for the skin after micropin, phototherapy, all kinds of instrument treatment, including invasive, Wicresoft, noinvasive etc., be required for into
The postoperative reparation of row, on the one hand antibacterial to be killed, prevent scar hyperplasia, is on the other hand also performed to skin wound epidermis and skin corium
Reparation, suppression melanin is formed, and does not has the most quick-acting skin-protection products at present, it is possible to collect reparation, moisturizing, moisturizing in one
Body, is exclusively used in the skin reparation after all kinds of instrument treatment.
Although it addition, have the multiple skin-protection product becoming " multi-efficiency " at present, but the research effect of reality shows, it
Many the effects possessing simple superposition, multiple skin problems are not obviously improved effect.Except this, more there are some skin protections
Product, in order to reach whitening effect for the moment, with the addition of the harmful materials such as heavy metal.
Therefore, this invention address that a kind of moisturizing liquid containing nano active carbon of development, while deep water supplement, have close
The effect that collection is repaired.
Summary of the invention
Present invention solves the technical problem that and be to provide a kind of moisturizing liquid containing nano active carbon and preparation method thereof, institute
State moisturizing liquid while deep water supplement, there is the effect of intensive reparation.
The technical scheme is that
A kind of moisturizing liquid containing nano active carbon, it is characterised in that component meter by weight, mainly by following component group
Become: nano active carbon 0.01-0.1 part, little molecule hyaluronic acid 3.2-5 part, lecithin liposome 0.3-2 part, coenzyme Q10 0.6-
1.2 parts, glycerol 4-16 part, propylene glycol 5-8 part, rose extract 0.2-1.5 part, allantoin 0.3-1.5 part, amino acid humectant
0.3-0.8 part, VE0.1-0.5 part, wheat malt germ extract 0.05-1 part, oleum lini 0.05-0.1 part, PEG-40 0.1-0.3
Part, purified water 30-80 part.
Further, described nano active carbon is nano level activated carbon, and its particle diameter is 1-100nm.
Further, described nano active carbon is modified with hydroxy functional group.
Further, the method for modifying described nano active carbon being modified hydroxy functional group is: by nano active carbon with
Mass concentration is that the ethanol solution of 20-30% is by 1:(50～1000) part by weight be mixed and sonicated for, obtain dispersion all
Even nano active carbon suspension；It is the HNO of 15% by mass concentration3Solution carry out oxidation processes, keep 84-90 DEG C of constant temperature
Processing 20-35min, then be placed in ultrasonic processor and carry out supersound process, the power of supersound process is 1.05KW～1.15KW, super
The sound time is 5min～18min, and controlling temperature range is 68～72 DEG C；Finally filter PH to 7～7.5 with deionized water drip washing,
Place into dried in vacuum drying oven, i.e. obtain the nano active carbon of hydroxy functional groups.
Further, the molecular weight ranges of described little molecule hyaluronic acid is between 400000～800000.
A kind of moisturizing liquid containing nano active carbon, its preparation method is:
Step one: weigh nano active carbon, little molecule hyaluronic acid, lecithin liposome, coenzyme Q10, sweet by described proportioning
Oil, propylene glycol, rose extract, allantoin, amino acid humectant, VE, wheat malt germ extract, oleum lini, PEG-40, purification
Water, stand-by；
Step 2: by described nano active carbon deionized water dissolving so that it is become suspension, nanometer in described suspension
The mass concentration of activated carbon is less than or equal to 10 ‰；
Step 3: the part by weight that described little molecule hyaluronic acid is pressed 1:2 adds purified water, and stirring obtains little molecule glass urine
Acid solution, stand-by；
Step 4: mix swelling with purified water according to the weight ratio of 1:3 by described carbomer, obtains swelling carbomer molten
Liquid, stand-by；
Step 5: by described lecithin liposome, coenzyme Q10, glycerol, propylene glycol, allantoin, amino acid humectant, VE,
Wheat malt germ extract, oleum lini, PEG-40 mixing and stirring, obtain mixture stand-by；
Step 6: in the swelling carbomer solution that step 5 gained mixture addition to step 3 is obtained, add
The hyaluronic acid solution that step 2 obtains, after standing 30～60 minutes, more firmly rocks, until hyaluronic acid stock solution is dissolved completely in mixed
In compound；It is further continued for adding suspension, rose extract and the residue purified water that step one obtains, is placed in homogenizer, open
Homogenizer, controls temperature and is 50-62 DEG C, and mixing speed is 12000-20000r/min, carries out emulsifying homogeneous, and the time is 20-
30min, while hot with ultrasonic cleaner ultrasonic disperse 2-15min, temperature when controlling ultrasonic disperse is 55-70 DEG C, then exists
Quickly cooling under condition of ice bath, and carry out mechanical defoaming, froth breaking is naturally cooling to 35 DEG C after completing, i.e. obtain described moisturizing
Liquid.
The invention has the beneficial effects as follows: the moisturizing liquid of the present invention is applicable to all types of skin, be particularly well-suited to micropin,
Skin repair after phototherapy, all kinds of instrument treatment, moisturizing, moisturizing use, and utilize high-end liposome technology, make nutrient substance be more easy to
Enter skin, reach quickly to repair, moisturizing, the effect of long-acting moisturizing, thus improve coarse, microgroove, be dried.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is further limited, but claimed
Scope is not only limited to description.
Embodiment 1:
A kind of moisturizing liquid containing nano active carbon, component meter by weight, mainly consist of the following composition: nano active
0.01 part of carbon, little molecule hyaluronic acid 3.2 parts, lecithin liposome 0.3 part, coenzyme Q10 0.6 part, glycerol 4 parts, propylene glycol 5 parts,
Rose extract 0.2 part, allantoin 0.3 part, amino acid humectant 0.3 part, VE 0.1 part, wheat malt germ extract 0.05 part,
Oleum lini 0.05 part, PEG-40 0.1 part, purified water 30 parts.
Wherein, described nano active carbon is nano level activated carbon, and its particle diameter is 1nm.Modify on described nano active carbon
Having hydroxy functional group, method of modifying is: be that the ethanol solution of 20% is by the weight ratio of 1:50 by nano active carbon and mass concentration
Example is mixed and sonicated for, and obtains finely dispersed nano active carbon suspension；It is the HNO of 15% by mass concentration3Solution
Carry out oxidation processes, keep 84 DEG C of constant temperature to process 20min, then be placed in ultrasonic processor and carry out supersound process, supersound process
Power is 1.05KW, and ultrasonic time is 5min, and controlling temperature range is 68 DEG C；Finally filter PH to 7 with deionized water drip washing, then
Put into dried in vacuum drying oven, i.e. obtain the nano active carbon of hydroxy functional groups.Dividing of described little molecule hyaluronic acid
Sub-weight range is between 400000.
The preparation method of the moisturizing liquid that should contain nano active carbon is:
Step one: weigh nano active carbon, little molecule hyaluronic acid, lecithin liposome, coenzyme Q10, sweet by described proportioning
Oil, propylene glycol, rose extract, allantoin, amino acid humectant, VE, wheat malt germ extract, oleum lini, PEG-40, purification
Water, stand-by；
Step 2: by described nano active carbon deionized water dissolving so that it is become suspension, nanometer in described suspension
The mass concentration of activated carbon is 2 ‰；
Step 3: the part by weight that described little molecule hyaluronic acid is pressed 1:2 adds purified water, and stirring obtains little molecule glass urine
Acid solution, stand-by；
Step 4: mix swelling with purified water according to the weight ratio of 1:3 by described carbomer, obtains swelling carbomer molten
Liquid, stand-by；
Step 5: by described lecithin liposome, coenzyme Q10, glycerol, propylene glycol, allantoin, amino acid humectant, VE,
Wheat malt germ extract, oleum lini, PEG-40 mixing and stirring, obtain mixture stand-by；
Step 6: in the swelling carbomer solution that step 5 gained mixture addition to step 3 is obtained, add
The hyaluronic acid solution that step 2 obtains, after standing 30 minutes, more firmly rocks, until hyaluronic acid stock solution is dissolved completely in mixture
In；It is further continued for adding suspension, rose extract and the residue purified water that step one obtains, is placed in homogenizer, open homogenizing
Machine, controlling temperature is 50 DEG C, and mixing speed is 12000r/min, carries out emulsifying homogeneous, and the time is 20min, uses ultrasound wave while hot
Washer ultrasonic disperse 2min, temperature when controlling ultrasonic disperse is 55 DEG C, then quickly cools under condition of ice bath, and
Carrying out mechanical defoaming, froth breaking is naturally cooling to 35 DEG C after completing, and i.e. obtains described moisturizing liquid.
Embodiment 2:
A kind of moisturizing liquid containing nano active carbon, component meter by weight, mainly consist of the following composition: nano active
0.055 part of carbon, little molecule hyaluronic acid 4.1 parts, lecithin liposome 1.15 parts, coenzyme Q10 0.9, glycerol 10 parts, propylene glycol 6.5
Part, rose extract 0.85 part, allantoin 0.9 part, amino acid humectant 0.65 part, VE 0.3 part, wheat malt germ extract
0.525 part, oleum lini 0.075 part, PEG-40 0.2 part, purified water 55 parts.
Wherein, described nano active carbon is nano level activated carbon, and its particle diameter is 50nm.Modify on described nano active carbon
Having hydroxy functional group, method of modifying is: be that the ethanol solution of 25% is by the weight ratio of 1:525 by nano active carbon and mass concentration
Example is mixed and sonicated for, and obtains finely dispersed nano active carbon suspension；It is the HNO of 15% by mass concentration3Solution
Carry out oxidation processes, keep 87 DEG C of constant temperature to process 27.min, then be placed in ultrasonic processor and carry out supersound process, supersound process
Power is 1.1KW, and ultrasonic time is 11.5min, and controlling temperature range is 70 DEG C；Finally filter PH to 7 with deionized water drip washing,
Place into dried in vacuum drying oven, i.e. obtain the nano active carbon of hydroxy functional groups.Described little molecule hyaluronic acid
Molecular weight ranges is between 600000.
The preparation method of the moisturizing liquid that should contain nano active carbon is:
Step one: weigh nano active carbon, little molecule hyaluronic acid, lecithin liposome, coenzyme Q10, sweet by described proportioning
Oil, propylene glycol, rose extract, allantoin, amino acid humectant, VE, wheat malt germ extract, oleum lini, PEG-40, purification
Water, stand-by；
Step 2: by described nano active carbon deionized water dissolving so that it is become suspension, nanometer in described suspension
The mass concentration of activated carbon is 6 ‰；
Step 3: the part by weight that described little molecule hyaluronic acid is pressed 1:2 adds purified water, and stirring obtains little molecule glass urine
Acid solution, stand-by；
Step 4: mix swelling with purified water according to the weight ratio of 1:3 by described carbomer, obtains swelling carbomer molten
Liquid, stand-by；
Step 5: by described lecithin liposome, coenzyme Q10, glycerol, propylene glycol, allantoin, amino acid humectant, VE,
Wheat malt germ extract, oleum lini, PEG-40 mixing and stirring, obtain mixture stand-by；
Step 6: in the swelling carbomer solution that step 5 gained mixture addition to step 3 is obtained, add
The hyaluronic acid solution that step 2 obtains, after standing 45 minutes, more firmly rocks, until hyaluronic acid stock solution is dissolved completely in mixture
In；It is further continued for adding suspension, rose extract and the residue purified water that step one obtains, is placed in homogenizer, open homogenizing
Machine, controlling temperature is 56 DEG C, and mixing speed is 16000r/min, carries out emulsifying homogeneous, and the time is 25min, uses ultrasound wave while hot
Washer ultrasonic disperse 5.8min, temperature when controlling ultrasonic disperse is 62.5 DEG C, then quickly cools down fall under condition of ice bath
Temperature, and carry out mechanical defoaming, froth breaking is naturally cooling to 35 DEG C after completing, i.e. obtain described moisturizing liquid.
Embodiment 3:
A kind of moisturizing liquid containing nano active carbon, component meter by weight, mainly consist of the following composition: nano active
0.1 part of carbon, little molecule hyaluronic acid 5 parts, lecithin liposome 2 parts, coenzyme Q10 1.2 parts, glycerol 16 parts, propylene glycol 8 parts, Flos Rosae Rugosae
Extract 1.5 parts, allantoin 1.5 parts, amino acid humectant 0.8 part, VE 0.5 part, wheat malt germ extract 1 part, oleum lini
0.1 part, PEG-40 0.3 part, purified water 80 parts.
Wherein, described nano active carbon is nano level activated carbon, and its particle diameter is 100nm.Repair on described nano active carbon
Being decorated with hydroxy functional group, method of modifying is: be that the ethanol solution of 30% is by the weight of 1:1000 by nano active carbon and mass concentration
Amount ratio is mixed and sonicated for, and obtains finely dispersed nano active carbon suspension；It is the HNO of 15% by mass concentration3's
Solution carries out oxidation processes, keeps 90 DEG C of constant temperature to process 35min, then is placed in ultrasonic processor and carries out supersound process, ultrasonic place
The power of reason is 1.15KW, and ultrasonic time is 18min, and controlling temperature range is 72 DEG C；Finally filter PH with deionized water drip washing
To 7.5, place into dried in vacuum drying oven, i.e. obtain the nano active carbon of hydroxy functional groups.Described little molecule glass
The molecular weight ranges of uric acid is between 800000.
The preparation method of the moisturizing liquid that should contain nano active carbon is:
Step one: weigh nano active carbon, little molecule hyaluronic acid, lecithin liposome, coenzyme Q10, sweet by described proportioning
Oil, propylene glycol, rose extract, allantoin, amino acid humectant, VE, wheat malt germ extract, oleum lini, PEG-40, purification
Water, stand-by；
Step 2: by described nano active carbon deionized water dissolving so that it is become suspension, nanometer in described suspension
The mass concentration of activated carbon is 10 ‰；
Step 3: the part by weight that described little molecule hyaluronic acid is pressed 1:2 adds purified water, and stirring obtains little molecule glass urine
Acid solution, stand-by；
Step 4: mix swelling with purified water according to the weight ratio of 1:3 by described carbomer, obtains swelling carbomer molten
Liquid, stand-by；
Step 5: by described lecithin liposome, coenzyme Q10, glycerol, propylene glycol, allantoin, amino acid humectant, VE,
Wheat malt germ extract, oleum lini, PEG-40 mixing and stirring, obtain mixture stand-by；
Step 6: in the swelling carbomer solution that step 5 gained mixture addition to step 3 is obtained, add
The hyaluronic acid solution that step 2 obtains, after standing 60 minutes, more firmly rocks, until hyaluronic acid stock solution is dissolved completely in mixture
In；It is further continued for adding suspension, rose extract and the residue purified water that step one obtains, is placed in homogenizer, open homogenizing
Machine, controlling temperature is 62 DEG C, and mixing speed is 20000r/min, carries out emulsifying homogeneous, and the time is 30min, uses ultrasound wave while hot
Washer ultrasonic disperse 15min, temperature when controlling ultrasonic disperse is 70 DEG C, then quickly cools under condition of ice bath,
And carrying out mechanical defoaming, froth breaking is naturally cooling to 35 DEG C after completing, i.e. obtain described moisturizing liquid.
Moisturizing liquid is tested
1, test sample
(1) laboratory sample: above-described embodiment 1, embodiment 2 and the moisturizing liquid prepared by embodiment 3；
(2) with reference to sample: commercially available Ai Shike is because repairing peptide (production of Jia Bo bio tech ltd, Shanghai).
2, test object
60 33 years old～healthy without dermopathic women between 56 years old, 60 test objects are randomly divided into four groups, respectively
Named A group, B group, C group and D group, often organize 15 people.
3, method of testing
(1) four groups test objects left and right forearm on determine test zone, the area of test zone be 6cm ×
6cm；
(2) with SKICON 200 type keratodermatitis water content measuring instrument, four groups are tested the skin beauty water of object test zones
Cooperation, with testing, is surveyed inspection instrument by SEM575 type skin elasticity and is surveyed the skin elasticity of four groups of test object test zones
Examination, this test result is referred to as initial value.
(3) A group test object uses the moisturizing liquid prepared by above-described embodiment 1, B group test object to use above-described embodiment
Moisturizing liquid prepared by 2, C group test object uses the moisturizing liquid prepared by above-described embodiment 3, and D group test object uses described
With reference to sample, using seven days continuously, every day respectively uses once, and each consumption is 0.5 gram.
(4) A, after B, C, D group test object uses test sample seven days continuously, with SKICON 200 type keratodermatitis water
The skin hydration effect of each group of test object test zone is tested by content measuring instrument, surveys inspection by SEM575 type skin elasticity
The skin elasticity of each group of test object test zone is tested by instrument, and this test result is referred to as test value.
4, result of the test
(1) result of the test of A group: test value is compared with initial value, and subjects skin's average capacitance increases by 39%, experimenter
Skin average elasticity increases by 18.2%, and the average compactibility of subjects skin increases by 13.5%.
The result of the test of B group: test value is compared with initial value, and subjects skin's average capacitance increases by 38.3%, experimenter
Skin average elasticity increases by 20.1%, and the average compactibility of subjects skin increases by 16.2%.
The result of the test of C group: test value is compared with initial value, and subjects skin's average capacitance increases by 40.5%, experimenter
Skin average elasticity increases by 23.7%, and the average compactibility of subjects skin increases by 17.4%.
(2) result of the test of D group: test value compared with initial value, subjects skin's average capacitance increase by 17.3%, tested
Person's skin average elasticity increases by 14.6%, and the average compactibility of subjects skin increases by 10.1%.
From above experimental result, the moisturizing excellent effect of moisturizing liquid of the present invention.
Claims (6)
1. the moisturizing liquid containing nano active carbon, it is characterised in that component meter by weight, mainly by following component group
Become: nano active carbon 0.01-0.1 part, little molecule hyaluronic acid 3.2-5 part, lecithin liposome 0.3-2 part, coenzyme Q10 0.6-
1.2 parts, glycerol 4-16 part, propylene glycol 5-8 part, rose extract 0.2-1.5 part, allantoin 0.3-1.5 part, amino acid humectant
0.3-0.8 part, VE0.1-0.5 part, wheat malt germ extract 0.05-1 part, oleum lini 0.05-0.1 part, PEG-40 0.1-0.3
Part, purified water 30-80 part.
A kind of moisturizing liquid containing nano active carbon, it is characterised in that described nano active carbon is
Nano level activated carbon, its particle diameter is 1-100nm.
A kind of moisturizing liquid containing nano active carbon, it is characterised in that on described nano active carbon
It is modified with hydroxy functional group.
A kind of moisturizing liquid containing nano active carbon, it is characterised in that on described nano active carbon
The method of modifying modifying hydroxy functional group is: by ethanol solution that nano active carbon and mass concentration are 20-30% by 1:(50～
1000) part by weight is mixed and sonicated for, and obtains finely dispersed nano active carbon suspension；It is 15% by mass concentration
HNO3Solution carry out oxidation processes, keep 84-90 DEG C of constant temperature to process 20-35min, then be placed in ultrasonic processor and surpass
Sonication；Finally filter PH to 7～7.5 with deionized water drip washing, place into dried in vacuum drying oven, i.e. obtain containing hydroxyl
The nano active carbon of base functional group.
A kind of moisturizing liquid containing nano active carbon, it is characterised in that described little molecule hyaluronic acid
Molecular weight ranges between 400000～800000.
6. a kind of moisturizing liquid containing nano active carbon as described in claim 1-5, it is characterised in that preparation method is:
Step one: by described proportioning weigh nano active carbon, little molecule hyaluronic acid, lecithin liposome, coenzyme Q10, glycerol, third
Glycol, rose extract, allantoin, amino acid humectant, VE, wheat malt germ extract, oleum lini, PEG-40, purified water, treat
With；
Step 2: by described nano active carbon deionized water dissolving so that it is become suspension, nano active in described suspension
The mass concentration of carbon is less than or equal to 10 ‰；
Step 3: the part by weight that described little molecule hyaluronic acid is pressed 1:2 adds purified water, and it is molten that stirring obtains little molecule hyaluronic acid
Liquid, stand-by；
Step 4: mix swelling with purified water according to the weight ratio of 1:3 by described carbomer, obtains swelling carbomer solution,
Stand-by；
Step 5: by described lecithin liposome, coenzyme Q10, glycerol, propylene glycol, allantoin, amino acid humectant, VE, Semen Tritici aestivi
Embryo extract, oleum lini, PEG-40 mixing and stirring, obtain mixture stand-by；
Step 6: in the swelling carbomer solution obtain step 5 gained mixture addition to step 3, add step
The hyaluronic acid solution that two obtain, after standing 30～60 minutes, more firmly rocks, until hyaluronic acid stock solution is dissolved completely in mixture
In；It is further continued for adding suspension, rose extract and the residue purified water that step one obtains, is placed in homogenizer, open homogenizing
Machine, controls temperature and is 50-62 DEG C, and mixing speed is 12000-20000r/min, carries out emulsifying homogeneous, and the time is 20-30min,
Using ultrasonic cleaner ultrasonic disperse while hot, then quickly cool under condition of ice bath, and carry out mechanical defoaming, froth breaking is complete
It is naturally cooling to 35 DEG C after one-tenth, i.e. obtains described moisturizing liquid.
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