CN106212727A - A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect and preparation method thereof - Google Patents

A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect and preparation method thereof Download PDF

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Publication number
CN106212727A
CN106212727A CN201610593919.5A CN201610593919A CN106212727A CN 106212727 A CN106212727 A CN 106212727A CN 201610593919 A CN201610593919 A CN 201610593919A CN 106212727 A CN106212727 A CN 106212727A
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China
Prior art keywords
allii tuberosi
semen allii
gel
gel oil
erythritol
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CN201610593919.5A
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Chinese (zh)
Inventor
王根九
钱尼文
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Anhui Incense Grain And Oil Co Ltd
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Anhui Incense Grain And Oil Co Ltd
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Priority to CN201610593919.5A priority Critical patent/CN106212727A/en
Publication of CN106212727A publication Critical patent/CN106212727A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D7/00Edible oil or fat compositions containing an aqueous phase, e.g. margarines
    • A23D7/005Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by ingredients other than fatty acid triglycerides
    • A23D7/0056Spread compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D7/00Edible oil or fat compositions containing an aqueous phase, e.g. margarines
    • A23D7/02Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by the production or working-up
    • A23D7/04Working-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/335Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
    • A61K31/35Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom
    • A61K31/352Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom condensed with carbocyclic rings, e.g. methantheline 
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/02Inorganic compounds

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Epidemiology (AREA)
  • Polymers & Plastics (AREA)
  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Food Science & Technology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Inorganic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention discloses a kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect, including following parts by weight of component: Oleum Brassicae campestris 100 102, puerarin 67, pitaya peel total flavones 23, erythritol 56, yeast dextran 34, ethyl cellulose 1.1 1.2, lecithin 0.9 1, nano zeolite powder 45,12 hydroxyl castor oil acid 45, appropriate deionized water.The present invention prepares Semen Allii Tuberosi gel oil by functionalised dispersant, Oleum Brassicae campestris, gelator 12 hydroxyl castor oil acid and the erythritol built, there is good nutritive effect and treatment hypertension given efficacy, there is good non-oxidizability simultaneously, enrich the nutrition of Semen Allii Tuberosi gel oil.

Description

A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect and preparation method thereof
Technical field
The present invention relates to Semen Allii Tuberosi gel oil tech field, particularly relate to a kind of Semen Allii Tuberosi gel with treatment hypertensive effect Oil and preparation method thereof.
Background technology
Along with the change of people's dietary structure, China has become as in the world maximum food special fat country of consumption, food Product special fat not only gives local flavor, good mouthfeel and the moulding that food is unique, and has special merit in food processing Energy characteristic, such as, have the characteristics such as film, lubrication, shortening in bakery product.At present, food special fat is mainly with hydrogenated oil and fat It is main, trans fats, it is also called trans fatty acid, inverse state fatty acid, is that (unit is unsaturated or polynary for a kind of unsaturated fatty acid Unsaturated), its insalubrity, is the unnecessary nutrient of human body.Edible trans fats will improve the suffering from coronary heart The probability of disease of ZANG-organs.Research shows, containing a large amount of trans fatty acid in hydrogenated vegetable oil, mass fraction reaches 5%~11%, seriously surpasses Mark.In order to meet consumer to the healthy and demand of ticbit, reduce or eliminate in meals trans fatty acid and can not change Its special quality, is vast researcher and big problem that food production business faces and challenge.Therefore, low/zero trans is actively researched and developed Fatty acid food special fat has important practical significance.In recent years, the gel solid stateization of vegetable oil replaced hydrogenated vegetable oil Become study hotspot both domestic and external.Gel oil is memory fluid shape or the lipid mixtures of solid, shaped of a kind of thermal reversion, It is made up of the Low-molecular weight organogel factor of lipophilic liquid (generally vegetable oil) with a small amount of (< 10%), these organogels The factor has, trapping solution body oils can form the knot of variform (such as banding, threadiness) by the way of self assembly or crystallization Structure, forms three-dimensional net structure then, prevents the flowing of lipophilic liquid, so that whole system gelation.
Oleum Brassicae campestris is typically buff or brown, containing arachidic acid 0.4-1.0%, oleic acid 14-19%, linoleic acid 12-24%, mustard Acid 31-55%, linolenic acid 1-10%.From the perspective of nutritive value, human body may be up to 99% to Oleum Brassicae campestris digestibility, have function of gallbladder promoting, Certain vessel softening, slow down aging effect, and the cholesterol level in Oleum Brassicae campestris is with little or no containing, and is conducive to The people that cholesterol is high eats, and Oleum Brassicae campestris is the excellent edible oil that a kind of nutritive value is the highest.In the market about Semen Sesami gel The report of oil is little, the report of functional Semen Sesami gel oil especially almost without.
Develop nutritious Semen Allii Tuberosi gel oil, to improving its edible nourishing value, there is important value, it is possible to make consumption Person, while obtaining some functional characteristics being similar to hydrogenated vegetable oil, can take into account again its nutritive peculiarity.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of Semen Allii Tuberosi with treatment hypertensive effect Gel oil and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect, including following parts by weight of component: Oleum Brassicae campestris 100-102, Radix Puerariae Element 6-7, pitaya peel total flavones 2-3, erythritol 5-6, yeast dextran 3-4, ethyl cellulose 1.1-1.2, lecithin 0.9-1, nano zeolite powder 4-5,12-hydroxyl castor oil acid 4-5, appropriate deionized water.
A kind of Semen Allii Tuberosi gel oil preparation method with treatment hypertensive effect, comprises the following steps:
(1), first that the deionized water of lecithin, ethyl cellulose, yeast dextran and gross weight 2 times is mixed 70 DEG C of heating Close, by 30000r/min high shear treatment 3min, after-3 DEG C of lyophilizations process 20min, do again at liquid nitrogen quick freeze Dry 24h, obtains functionalised dispersant one standby;By puerarin, pitaya peel total flavones, nano zeolite powder and gross weight 2 times Deionized water add hot mixing at 70 DEG C, prepare aqueous solution ,-3 DEG C of lyophilizations by 30000r/min high shear treatment 3min After processing 20min, it is dried 24h again at liquid nitrogen quick freeze, obtains functionalised dispersant two standby;
(2), by Oleum Brassicae campestris, functionalised dispersant one, functionalised dispersant two, erythritol mixing, heat in steam bath and stir Mixing 50-60min, mixing speed is 150r/min to uniformly, adds 12-hydroxyl castor oil acid afterwards, changes infrared heating, first Processing from 100-140 DEG C of heated and stirred with the heating rate of 4 DEG C/min, mixing speed is 150r/min, then with 2 DEG C/min Rate of temperature fall process from 140-100 DEG C of cooling and stirring, mixing speed is 20r/min, then with the rate of temperature fall of 15 DEG C/min After continuing cool to room temperature, cold put 55-60h, to obtain final product.
The invention have the advantage that
The present invention is by the functionalised dispersant, Oleum Brassicae campestris, gelator 12-hydroxyl castor oil acid and the erythritol system that build Standby Semen Allii Tuberosi gel oil, has good nutritive effect and treatment hypertension given efficacy, has good non-oxidizability simultaneously, Enrich the nutrition of Semen Allii Tuberosi gel oil, in preparation process, use the heating of steam bath mix and blend, infrared intensification stirring to add successively Heat and alternating temperature stirring cooling and alternating temperature non-stirred cooling process, and can serve defencive function dispersion, promotion functions Property the dispersion uniform and stable distribution in Oleum Brassicae campestris and improve functionalised dispersant, Oleum Brassicae campestris, gelator, erythritol The uniformity of the gel of Diversity system, processes taken into account dish simultaneously in conjunction with alternating temperature stirring cooling and alternating temperature non-stirred cooling The uniformity of seed gel oil and hardness, viscosity and fragility.
Functionalised dispersant one serves the effect of nutrition oxidation, meanwhile, the coated fertilizer lecithin of employing, ethyl cellulose Element has the final system gelling of promotion;The puerarin that the nano zeolite powder that functionalised dispersant two uses loads is a kind of It is extracted from Chinese medicine Herba Gelsemii Elegantis or the isoflavone aglycone of Radix Puerariae rattan rhizome, has that lipotropy is strong, dissolubility is low, oral absorption is poor, biological profit The feature that expenditure is low, can be used for treating hypertension, has increase cerebral blood flow simultaneously, improves cerebral circulation effect;The Hylocereus undatus loaded Skin total flavones has the strongest oxidation resistance effect to Semen Allii Tuberosi gel oil;On the one hand the addition of nano zeolite powder improves lipophilic Sexual function material puerarin thermally-stabilised, on the other hand improves the compactness of the spacial framework of Semen Allii Tuberosi gel oil, increases The hardness of gel oil.
Detailed description of the invention
A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect, including following parts by weight of component: Oleum Brassicae campestris 100, Radix Puerariae Element 6, pitaya peel total flavones 2, erythritol 5, yeast dextran 3, ethyl cellulose 1.1, lecithin 0.9, nano zeolite powder 4,12 hydroxyl castor oil acids 4, appropriate deionized water.
A kind of Semen Allii Tuberosi gel oil preparation method with treatment hypertensive effect, comprises the following steps:
(1), first that the deionized water of lecithin, ethyl cellulose, yeast dextran and gross weight 2 times is mixed 70 DEG C of heating Close, by 30000r/min high shear treatment 3min, after DEG C lyophilization processes 20min, be dried again at liquid nitrogen quick freeze 24h, obtains functionalised dispersant one standby;By puerarin, pitaya peel total flavones, nano zeolite powder and gross weight 2 times Deionized water adds hot mixing at 70 DEG C, prepares aqueous solution by 30000r/min high shear treatment 3min, and DEG C lyophilization processes After 20min, it is dried 24h again at liquid nitrogen quick freeze, obtains functionalised dispersant two standby;
(2), by Oleum Brassicae campestris, functionalised dispersant one, functionalised dispersant two, erythritol mixing, heat in steam bath and stir Mixing 50min, mixing speed is 150r/min to uniformly, adds 12 hydroxyl castor oil acids afterwards, changes infrared heating, first with 4 DEG C/heating rate of min processes from 100 DEG C of heated and stirred, mixing speed is 150r/min, then in the cooling with 2 DEG C/min Speed processes from 140 DEG C of cooling and stirring, and mixing speed is 20r/min, then continues cool to the rate of temperature fall of 15 DEG C/min After room temperature, cold put 55h, to obtain final product.

Claims (2)

1. a Semen Allii Tuberosi gel oil with treatment hypertensive effect, it is characterised in that include following parts by weight of component: Oleum Brassicae campestris 100-102, puerarin 6-7, pitaya peel total flavones 2-3, erythritol 5-6, yeast dextran 3-4, ethyl cellulose 1.1- 1.2, lecithin 0.9-1, nano zeolite powder 4-5,12-hydroxyl castor oil acid 4-5, appropriate deionized water.
2. a Semen Allii Tuberosi gel oil preparation method with treatment hypertensive effect, it is characterised in that comprise the following steps:
(1), first that the deionized water of lecithin, ethyl cellulose, yeast dextran and gross weight 2 times is mixed 70 DEG C of heating Close, by 30000r/min high shear treatment 3min, after-3 DEG C of lyophilizations process 20min, do again at liquid nitrogen quick freeze Dry 24h, obtains functionalised dispersant one standby;By puerarin, pitaya peel total flavones, nano zeolite powder and gross weight 2 times Deionized water add hot mixing at 70 DEG C, prepare aqueous solution ,-3 DEG C of lyophilizations by 30000r/min high shear treatment 3min After processing 20min, it is dried 24h again at liquid nitrogen quick freeze, obtains functionalised dispersant two standby;
(2), by Oleum Brassicae campestris, functionalised dispersant one, functionalised dispersant two, erythritol mixing, heat in steam bath and stir Mixing 50-60min, mixing speed is 150r/min to uniformly, adds 12-hydroxyl castor oil acid afterwards, changes infrared heating, first Processing from 100-140 DEG C of heated and stirred with the heating rate of 4 DEG C/min, mixing speed is 150r/min, then with 2 DEG C/min Rate of temperature fall process from 140-100 DEG C of cooling and stirring, mixing speed is 20r/min, then with the rate of temperature fall of 15 DEG C/min After continuing cool to room temperature, cold put 55-60h, to obtain final product.
CN201610593919.5A 2016-07-27 2016-07-27 A kind of Semen Allii Tuberosi gel oil with treatment hypertensive effect and preparation method thereof Pending CN106212727A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108157525A (en) * 2018-01-29 2018-06-15 东北农业大学 A kind of method for preparing ricinoleic acid cold press rapeseed oil grease gel

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104582496A (en) * 2012-06-28 2015-04-29 陶氏环球技术有限责任公司 Method of preparing an edible oleogel
CN104855548A (en) * 2015-05-25 2015-08-26 华南理工大学 Preparation method of fat gel capable of loading carotene
CN105166916A (en) * 2015-10-30 2015-12-23 高萍 Food suitable for obese and overweight people and making method thereof and weight and health management method
CN105228461A (en) * 2013-05-31 2016-01-06 陶氏环球技术有限责任公司 Prepare the method for oleogel

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104582496A (en) * 2012-06-28 2015-04-29 陶氏环球技术有限责任公司 Method of preparing an edible oleogel
CN105228461A (en) * 2013-05-31 2016-01-06 陶氏环球技术有限责任公司 Prepare the method for oleogel
CN104855548A (en) * 2015-05-25 2015-08-26 华南理工大学 Preparation method of fat gel capable of loading carotene
CN105166916A (en) * 2015-10-30 2015-12-23 高萍 Food suitable for obese and overweight people and making method thereof and weight and health management method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
钟金锋等: "凝胶油及其在食品工业中的应用研究进展", 《食品科学》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108157525A (en) * 2018-01-29 2018-06-15 东北农业大学 A kind of method for preparing ricinoleic acid cold press rapeseed oil grease gel

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Application publication date: 20161214