CN106182269A - A kind for the treatment of fluid for fragility purple willow and preparation method thereof - Google Patents
A kind for the treatment of fluid for fragility purple willow and preparation method thereof Download PDFInfo
- Publication number
- CN106182269A CN106182269A CN201610574923.7A CN201610574923A CN106182269A CN 106182269 A CN106182269 A CN 106182269A CN 201610574923 A CN201610574923 A CN 201610574923A CN 106182269 A CN106182269 A CN 106182269A
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- China
- Prior art keywords
- parts
- purple willow
- fragility
- weight portion
- water
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
Abstract
The invention discloses a kind for the treatment of fluid for fragility purple willow and preparation method thereof, it is made up of the raw material of following weight portion: 15 18 parts of bran wax, dialkyl diphenylamine 8 12 parts, BBP(Butyl Benzyl Phthalate 10 15 parts, 46 parts of SA sodium, vinyl silicone oil 8 10 parts, ternary carboxyl vinyl chloride-vinyl acetate resin 47 parts, ferrocene 46 parts, 35 parts of tert-butylbenzene formic acid, white carbon 10 16 parts, antibacterial additive 22 28 parts.The present invention has the advantage that inorganic agent film property prepared in the present invention is preferable compared to existing technology, there is preferable emulsion property, adhesive force is strong, by processing under the Ultrasonic Conditions of corresponding frequencies, a certain amount of colloid can be filled inside purple willow, strengthen the toughness of purple willow, simultaneously can also effectively insect protected, mildew-resistant, stability is preferable, has stronger weatherability, improves the economic worth of fragility purple willow.
Description
Technical field
The invention belongs to wicker plaiting article product treatment technical field, be specifically related to a kind for the treatment of fluid for fragility purple willow and system thereof
Preparation Method.
Background technology
The kind of purple willow is a lot, wherein Clausena lansium (Lour.) Skeels purple willow quality better, and pliable and tough uniformly but yield is less, Pericarpium Citri Reticulatae Viride purple willow poor quality,
But yield is more, gained wicker is more crisp, matter is soft, poor toughness, and the only purple willow of small part high-quality can be widely applied to knitting, shadow
Ring certain economic benefit, generally all can have been processed by soak before purple willow uses so that it is more toughness, or play one
Fixed insect protected, anti-mold effect, but for the most relevant processing method of fragility purple willow, limit the application of purple willow.
Summary of the invention
It is an object of the invention to for existing problem, it is provided that a kind for the treatment of fluid for fragility purple willow and preparation side thereof
Method.
The present invention is achieved by the following technical solutions: a kind for the treatment of fluid for fragility purple willow, by following weight portion
Raw material make: bran wax 15-18 part, dialkyl diphenylamine 8-12 part, BBP(Butyl Benzyl Phthalate 10-15 part, SA sodium 4-6
Part, vinyl silicone oil 8-10 part, ternary carboxyl vinyl chloride-vinyl acetate resin 4-7 part, ferrocene 4-6 part, tert-butylbenzene formic acid 3-5 part, Linesless charcoal
Black 10-16 part, antibacterial additive 22-28 part；
Wherein, antibacterial additive is made up of the raw material of following weight portion: bitter youth's rattan 20-25 part, Cortex Meliae 8-15 part, Wuyi 5-8
Part, Herba Schizonepetae 3-6 part, Rhizoma Paridis 7-12 part, Herba Aristolochiae Mollissimae 17-22 part, Herba Scutellariae Barbatae 8-12 part, Semen Arecae 3-5 part, cortex toonae 6-10 part.
A kind of preparation method for fragility purple willow treatment fluid, comprises the following steps:
(1) weigh the material of corresponding deal according to the raw material of antibacterial additive, pulverize the ground product being less than 3mm for particle diameter respectively,
Being dried to moisture is 8-14%, with being equivalent to soak by water 4-5 hour of its weight portion 10 times, takes filtrate, be concentrated into after filtration
/ 10th of original volume, obtain concentrated solution and are antibacterial additive；
(2) weigh after the bran wax of corresponding weight portion, BBP(Butyl Benzyl Phthalate and ternary carboxyl vinyl chloride-vinyl acetate resin mix at 75-85 DEG C
Under conditions of stir 30-40 minute, obtain compound；
(3), after weighing surplus stock mixing, the water being equivalent to its weight portion 1.5-2 times is added, at 35-40 DEG C, 1200-1500r/
Stir 15-20 minute under conditions of min, obtain mixed serum；
(4) antibacterial additive obtained as above, compound and mixed slurry are mixed, under conditions of 50-55 DEG C, stir 2-3 little
Time, obtain homogeneous serosity, particle sice in serosity ＜ 30 μm, after filtration, obtain finished product, seal and preserve.
Wherein, step (1) filters gained medicinal residues dry to moisture less than 10% after reusable 4-6 time；For the second time
Using amount of water is 8 times of water, concentrates 1/8th for its volume after decoction；Amount of water and enrichment factor proportionally reduce afterwards.
The using method of present treatment agent is: purple willow is put into submergence in treatment fluid, installs ultrasound wave frequency on its chamber wall
Rate is the supersonic generator of 28KHZ, processes 10-15 hour, naturally dries after taking-up under normal temperature condition.
The present invention has the advantage that inorganic agent film property prepared in the present invention is preferable compared to existing technology, has
Preferably emulsion property, adhesive force is strong, by processing under the Ultrasonic Conditions of corresponding frequencies, can fill out inside purple willow
Fill a certain amount of colloid, strengthen the toughness of purple willow, simultaneously can also effectively insect protected, mildew-resistant, stability preferably, has stronger weather-proof
Property, improve the economic worth of fragility purple willow.
Detailed description of the invention
Embodiment 1
A kind for the treatment of fluid for fragility purple willow, is made up of the raw material of following weight portion: 16 parts of bran wax, dialkyl diphenylamine 12
Part, BBP(Butyl Benzyl Phthalate 12 parts, 5 parts of SA sodium, vinyl silicone oil 8 parts, ternary carboxyl vinyl chloride-vinyl acetate resin 6 parts, ferrocene 5
Part, 4 parts of tert-butylbenzene formic acid, white carbon 10 parts, antibacterial additive 22 parts；
Wherein, antibacterial additive is made up of the raw material of following weight portion: bitter 24 parts of youth rattan, Cortex Meliae 9 parts, 8 parts, Wuyi, Herba Schizonepetae 5
Part, Rhizoma Paridis 10 parts, Herba Aristolochiae Mollissimae 21 parts, Herba Scutellariae Barbatae 12 parts, Semen Arecae 3 parts, cortex toonae 8 parts.
A kind of preparation method for fragility purple willow treatment fluid, comprises the following steps:
(1) weigh the material of corresponding deal according to the raw material of antibacterial additive, pulverize the ground product being less than 3mm for particle diameter respectively,
Being dried to moisture is 8-14%, with being equivalent to soak by water 4-5 hour of its weight portion 10 times, takes filtrate, be concentrated into after filtration
/ 10th of original volume, obtain concentrated solution and are antibacterial additive；
(2) weigh after the bran wax of corresponding weight portion, BBP(Butyl Benzyl Phthalate and ternary carboxyl vinyl chloride-vinyl acetate resin mix at 75-85 DEG C
Under conditions of stir 30-40 minute, obtain compound；
(3), after weighing surplus stock mixing, the water being equivalent to its weight portion 1.5-2 times is added, at 35-40 DEG C, 1200-1500r/
Stir 15-20 minute under conditions of min, obtain mixed serum；
(4) antibacterial additive obtained as above, compound and mixed slurry are mixed, under conditions of 50-55 DEG C, stir 2-3 little
Time, obtain homogeneous serosity, particle sice in serosity ＜ 30 μm, after filtration, obtain finished product, seal and preserve.
Wherein, step (1) filters gained medicinal residues dry to moisture less than 10% after reusable 4-6 time；For the second time
Using amount of water is 8 times of water, concentrates 1/8th for its volume after decoction；Amount of water and enrichment factor proportionally reduce afterwards.
The using method of present treatment agent is: purple willow is put into submergence in treatment fluid, installs ultrasound wave frequency on its chamber wall
Rate is the supersonic generator of 28KHZ, processes 10-15 hour, naturally dries after taking-up under normal temperature condition.
Fragility purple willow is after said method processes in the present embodiment, can be dried, do not return under normal temperature condition in 4 hours
Viscous, hardness reaches 3H, and after using 1 year, without going mouldy or moth, epidermis, without the phenomenon split, keeps preferable pliability and load
Ability, the scope of application is wider.
Claims (4)
1. the treatment fluid for fragility purple willow, it is characterised in that be made up of the raw material of following weight portion: bran wax 15-18 part,
Dialkyl diphenylamine 8-12 part, BBP(Butyl Benzyl Phthalate 10-15 part, SA sodium 4-6 part, vinyl silicone oil 8-10 part, three
Unit's carboxyl vinyl chloride-vinyl acetate resin 4-7 part, ferrocene 4-6 part, tert-butylbenzene formic acid 3-5 part, white carbon 10-16 part, antibacterial additive 22-
28 parts；
Wherein, antibacterial additive is made up of the raw material of following weight portion: bitter youth's rattan 20-25 part, Cortex Meliae 8-15 part, Wuyi 5-8
Part, Herba Schizonepetae 3-6 part, Rhizoma Paridis 7-12 part, Herba Aristolochiae Mollissimae 17-22 part, Herba Scutellariae Barbatae 8-12 part, Semen Arecae 3-5 part, cortex toonae 6-10 part.
2. the preparation method being used for fragility purple willow treatment fluid as claimed in claim 1, it is characterised in that include following step
Rapid:
(1) weigh the material of corresponding deal according to the raw material of antibacterial additive, pulverize the ground product being less than 3mm for particle diameter respectively,
Being dried to moisture is 8-14%, with being equivalent to soak by water 4-5 hour of its weight portion 10 times, takes filtrate, be concentrated into after filtration
/ 10th of original volume, obtain concentrated solution and are antibacterial additive；
(2) weigh after the bran wax of corresponding weight portion, BBP(Butyl Benzyl Phthalate and ternary carboxyl vinyl chloride-vinyl acetate resin mix at 75-85 DEG C
Under conditions of stir 30-40 minute, obtain compound；
(3), after weighing surplus stock mixing, the water being equivalent to its weight portion 1.5-2 times is added, at 35-40 DEG C, 1200-1500r/
Stir 15-20 minute under conditions of min, obtain mixed serum；
(4) antibacterial additive obtained as above, compound and mixed slurry are mixed, under conditions of 50-55 DEG C, stir 2-3 little
Time, obtain homogeneous serosity, particle sice in serosity ＜ 30 μm, after filtration, obtain finished product, seal and preserve.
A kind of preparation method for fragility purple willow treatment fluid, it is characterised in that wherein step (1)
Middle filtration gained medicinal residues are being dried to moisture less than after 10% reusable 4-6 time；Second time uses amount of water to be 8 times of water, decocts
/ 8th for its volume are concentrated after boiling；Amount of water and enrichment factor proportionally reduce afterwards.
A kind for the treatment of fluid for fragility purple willow, it is characterised in that using method is: put by purple willow
Entering submergence in treatment fluid, installing ultrasonic frequency on its chamber wall is the supersonic generator of 28KHZ, processes 10-15 hour,
Naturally dry under normal temperature condition after taking-up.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610574923.7A CN106182269A (en) | 2016-07-21 | 2016-07-21 | A kind for the treatment of fluid for fragility purple willow and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610574923.7A CN106182269A (en) | 2016-07-21 | 2016-07-21 | A kind for the treatment of fluid for fragility purple willow and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106182269A true CN106182269A (en) | 2016-12-07 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610574923.7A Pending CN106182269A (en) | 2016-07-21 | 2016-07-21 | A kind for the treatment of fluid for fragility purple willow and preparation method thereof |
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| CN (1) | CN106182269A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108705632A (en) * | 2018-06-08 | 2018-10-26 | 阜南县宏达工艺品厂 | A method of promoting wicker products weatherability |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104365693A (en) * | 2014-10-29 | 2015-02-25 | 阜南县宏泰工艺品有限公司 | Treatment agent for white willow |
| CN104441155A (en) * | 2014-09-25 | 2015-03-25 | 阜南县猛发工艺品有限公司 | Rattan treatment method |
-
2016
- 2016-07-21 CN CN201610574923.7A patent/CN106182269A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104441155A (en) * | 2014-09-25 | 2015-03-25 | 阜南县猛发工艺品有限公司 | Rattan treatment method |
| CN104365693A (en) * | 2014-10-29 | 2015-02-25 | 阜南县宏泰工艺品有限公司 | Treatment agent for white willow |
Non-Patent Citations (4)
| Title |
|---|
| 国家食品药品监督管理局执业药师资格认证中心: "《中药学专业知识（一）》", 31 January 2014 * |
| 李晓平等: "《木材胶黏剂》", 31 January 2003 * |
| 陆启玉等: "《油脂化工产品生产技术》", 31 March 2004 * |
| 高俊刚等: "《改性聚氯乙烯新材料》", 30 October 2002 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108705632A (en) * | 2018-06-08 | 2018-10-26 | 阜南县宏达工艺品厂 | A method of promoting wicker products weatherability |
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20161207 |