CN106167838A - A kind of processing method of the rich functional nigecose of polyphenol - Google Patents

A kind of processing method of the rich functional nigecose of polyphenol Download PDF

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CN106167838A
CN106167838A CN201610670593.1A CN201610670593A CN106167838A CN 106167838 A CN106167838 A CN 106167838A CN 201610670593 A CN201610670593 A CN 201610670593A CN 106167838 A CN106167838 A CN 106167838A
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juice
nigecose
polyphenol
membrane
functional
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CN106167838B (en
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史昌蓉
李凯
杭方学
陆海勤
李红
谢彩锋
刘继栋
邓立高
李文
蒙丽丹
曲睿晶
兰梅娟
李�一
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Guangxi University
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Guangxi University
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    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00Purification of sugar juices
    • C13B20/16Purification of sugar juices by physical means, e.g. osmosis or filtration
    • C13B20/165Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration
    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B10/00Production of sugar juices
    • C13B10/02Expressing juice from sugar cane or similar material, e.g. sorghum saccharatum
    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B50/00Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
    • C13B50/002Addition of chemicals or other foodstuffs

Abstract

The processing method of a kind of rich functional nigecose of polyphenol, step is as follows: sugar cane crushing obtains material liquid, first adds lime cream, reheats and obtains heating material liquid;Primary ceramic membrane is used to be filtrated to get one-level film clear juice and one-level membrance concentration juice;Secondary membrane is used to obtain secondary membrane clear juice and the secondary membrane concentrated juice of aldehydes matter enrichment;Secondary membrane concentrated juice is used for producing the rich functional nigecose of polyphenol, method is as follows: choose at least one in Colla Corii Asini, Fructus Jujubae, Arillus Longan, Radix Angelicae Sinensis, Radix Codonopsis, Fructus Lycii, Bulbus Lilii, Herba Leonuri and Rhizoma Zingiberis Recens or several as functional components, boiling taking juice or be dried and crushed into powder, after secondary membrane concentrated juice evaporation and concentration, add above-mentioned juice or powder, sugar cook, graining, molding, be packaged to be the rich functional nigecose of polyphenol.Polyphenols of the present invention has obtained effective enrichment, and adds the functional components of multiple integration of edible and medicinal herbs, and relatively conventional production technology improves 4~8 times, improves quality and the nutritive value of nigecose.

Description

A kind of processing method of the rich functional nigecose of polyphenol
Technical field
The present invention relates to sugar refining technology field, the processing method of a kind of rich functional nigecose of polyphenol.
Background technology
Sugar Industry is Guangxi mainstay of the national economy industry, relates to the comprehensive industry of secondary and tertiary industries, near in district The productive life of half population is closely bound up with Sugarcane Industry, the fiscal revenues of Shi Wo district and minority area, border area agriculture The main support that people's employment increases income.In recent years, owing to being affected by international sugar valency, sugar valency constantly dropped.In addition production cost is high, Agriculture as the foundation of the economy is weaker, mechanization degree is low, and the varities of industrial products is single, lack the problems such as the market competitiveness, makes Guangxi Sugar industry has gone to life-and-death crossroad.Having put into effect a series of policy for this Guangxi District government promotes Chinese Sugar Industry to rise transition Level, " overall plan about promoting Chinese Sugar Industry starting new undertaking ", clearly propose " with Caulis Sacchari sinensis multiformity industry as handgrip, to accelerate The development non-sugar product of Caulis Sacchari sinensis, strengthens the industry ability to ward off risks ", conscientiously improve the Chinese Sugar Industry capability of sustainable development and international competition Power.
It is the deeper brown sugar of color in nigecose original idea, owing to color approximates black, thus is referred to as by Japan and Taiwan Nigecose, China's Mainland claims brown sugar.Nigecose is not through highly refined, the sucrose of decolouring.In addition to providing heat energy, possibly together with few Amount polyphenols and multiple essential amino acid, growth in humans grow indispensable malic acid, riboflavin, carotene, Nicotinic acid and trace element, such as calcium, potassium, ferrum, magnesium and folic acid and other mineral etc., have the highest nutritive value, Er Qieyou It is beneficial to acid-base balance in human body.
After traditional nigecose production method is mainly sugar cane crushing, heating sugarcane juice is to boiling, and now impurity can be along with bubble Producing and float, skim upper strata scum silica frost, and carry out stepped evaporation concentration, after being concentrated to certain brix, cooling down and stirring stimulates Crystalline substance, forms lamellar sugar or powdered sugar.But tradition nigecose production technology is because clarifying efficiency is relatively low, and causes the impurity of nigecose product Content is higher, is dissolved in the water and occurs turbid phenomenon afterwards;And this is conventionally produced inefficient, it is difficult to realize industry metaplasia Produce.
Polyphenol compound, refers to the general name having the plant component of several phenolic hydroxyl group in molecular structure, including phenol Acid and flavone compound.Polyphenol compound has certain oxidation resistance, has listed Natural antioxidant category in, is excellent Good hydrogen or the donor of electronics, the superoxide anion causing 26S Proteasome Structure and Function to damage to producing peroxidation and hydroxyl are certainly Obvious scavenging action is had by free radicals such as bases.Oxidative damage is to cause many chronic diseases, such as cardiovascular diseases, cancer and aging Major reason.These chronic diseases can be played preventive effect by the anti-oxidation function of polyphenol.Containing a large amount of pigment things in Caulis Sacchari sinensis Matter, these materials belong to polyphenol compound and flavonoids, and the content of polyphenols is compared with many fruit or vegetable Go even farther.Polyphenols extract in Caulis Sacchari sinensis has stronger removing free radical, antioxidant activity, the battalion to the mankind Support, healthy and diseases prevention and treatment are significant.There are some researches show, the polyphenols contained in Caulis Sacchari sinensis, belong to water solublity color Element, for the carbon skeleton of C6-C3-C6, all has plural hydroxyl on phenyl ring simultaneously, common are 3 classes: i.e. anthocyanidin, Xanthin (flavonoid), catechin.Research according to Haier's base Ovshinsky and Clarke measures: the polyphenol compound in Caulis Sacchari sinensis is many Concentrate on the sugarcane taper near growing point to divide.The high molecular polyphenol compound of molecular weight more than 5000 full bar Caulis Sacchari sinensis point Cloth is: sugarcane leaf accounts for 33%, the sugarcane tip (0 one 11 joint) accounts for 37%, and the sugarcane stem after topping only accounts for 30%, it is seen that though the sugarcane tip is only sugarcane stem Fraction, but Polyphenols thing is then more than sugarcane stem, and Relatively centralized.Caulis Sacchari sinensis in juice-extracting process, these water-soluble polyphenols chemical combination Thing major part enters in Caulis Sacchari sinensis juice.
Therefore, when using band belt leaf Caulis Sacchari sinensis as raw material, for producing nigecose product after squeezing the juice, process uses efficient The peace and quiet sugarcane juice of membrane separation technique, it is possible to the effective quality improving nigecose;Multistage Membranes parallel processing sugarcane juice enrichment polyphenols Produce nigecose technique, it is possible to the effective nutritive value improving nigecose and functional importance.Meet modern people to functional Nutraceutical demand;Also comply with the requirement that development cane products is diversified, high-valued simultaneously, be that developing Sugarcane Industry develops new road The embodiment in footpath.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, it is provided that the processing method of a kind of rich functional nigecose of polyphenol.
To achieve these goals, present invention employs techniques below scheme:
The processing method of a kind of rich functional nigecose of polyphenol, comprises the steps:
(1) take sugarcane slightly with the Caulis Sacchari sinensis of sugarcane leaf as raw material, squeeze the juice and tentatively go the removal of impurity, obtaining material liquid;
(2) material liquid first adds lime cream regulation pH to 7.0~7.5, is again heated to 80~90 DEG C, obtains heating material liquid;
(3) use the primary ceramic membrane filtering and heating material liquid in aperture 50~200nm, obtain one-level film clear juice and one-level film Concentrated juice;
(4) use the secondary membrane one-level film clear juice of molecular cut off 1~5kDa, obtain secondary membrane clear juice and phenolic material The secondary membrane concentrated juice of matter enrichment;
(5) secondary membrane concentrated juice is used for producing the rich functional nigecose of polyphenol, and concrete grammar is as follows:
First, at least one in Colla Corii Asini, Fructus Jujubae, Arillus Longan, Radix Angelicae Sinensis, Radix Codonopsis, Fructus Lycii, Bulbus Lilii, Herba Leonuri and Rhizoma Zingiberis Recens is chosen Or several as functional components, boiling taking juice or be dried and crushed into powder,
Then, secondary membrane concentrated juice evaporation and concentration to 60~65 ° of BX, add juice or the powder of above-mentioned functions composition End, stirs, and stirs off at ambient pressure to sweet cake brix 94~96 ° of BX, pours in mould, natural cooling after sweet cake stirring graining After molding, it is packaged to be the rich functional nigecose of polyphenol.
Secondary membrane clear juice produces for white sugar.
One-level membrance concentration juice is pumped in material liquid after carbonation, filter press.
Step (3) transmembrane pressure 0.25~0.45Mpa, crossflow velocity 4~5m/s, volume concentration is 8~12 again.
Step (4) transmembrane pressure is 0.6~1.0Mpa, crossflow velocity 4.5~5.5m/s, and volume concentration multiple is 8~10.
In step (5), count by weight, 2 parts of Colla Corii Asini, Fructus Jujubae 10 parts, Arillus Longan 5 parts, Radix Angelicae Sinensis 1 part, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 2 parts, Herba Leonuri 1 part and 1 part of Rhizoma Zingiberis Recens.
In step (5), count by weight, 10 parts of Colla Corii Asini, Fructus Jujubae 5 parts, Arillus Longan 2 parts, Radix Angelicae Sinensis 2 parts, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 3 parts, Herba Leonuri 2 parts and 3 parts of Rhizoma Zingiberis Recens.
In step (5), the gross weight adding functional components is that secondary membrane concentrated juice evaporation and concentration weighs to 60~65 ° of BX The 5~15% of amount.
Colla Corii Asini, for tonifying blood and arresting bleeding, moistens dry good medicine, and clinical practice is unable in blood deficiency and yellow complexion, dizziness cardiopalmus, flesh flaccidity, the heart Tired insomnia, stirring-up of pathogenic wind in the interior resulting from deficiency, xeropulmonary cough, phthisical cough are spat blood, are spitted blood, the aspects such as metrorrhagia of having blood in stool have significant curative effect.Colla Corii Asini has life Blood effect, the anemia that can be used for losing blood, iron deficiency anemia, aplastic anemia and old, child, the nourishing of women.And to youngster Growth promoter virgin, teen-age has an improvement result, long-term taking Colla Corii Asini, also can skin nutrition, make skin bright and clean lubricious and have Elastic.
Fructus Jujubae, has another name called Fructus Jujubae, and Fructus Jujubae sweet in the mouth is warm in nature, return taste warp, has invigorating the spleen and replenishing QI, nourishing blood to tranquillize the mind, the merit of the mitigation property of medicine Energy;The pharmacology in modern times then finds, containing protein, fat, saccharide, organic acid, vitamin A, vitamin C, many in Fructus Jujubae Planting the nutrition that micro-calcium and aminoacid etc. are abundant, particularly vitamin content is the highest, has " natural complex ball " Good reputation, has nourishing YIN and invigorating YANG, the effect enriched blood.
Arillus Longan is also known as Arillus Longan, sweet in the mouth warm in nature, heart-spleen boosting, fills blood;There is good nourishing benefiting action.Can be used for heart spleen The diseases such as insomnia caused by deficient, insufficiency of vital energy and blood, forgetful, palpitation with fear, dizziness.Also can treat the most weak or mental deterioration.Women exists Adjust puerperal benefit the most suitable.Li Shizhen (1518-1593 A.D.) is described in Compendium of Material Medica: " food is with Fructus Litchi for expensive, and it is good for providing benefit then Arillus Longan ". Arillus Longan is extraordinarily praised highly.Confirming according to pharmacological research, Arillus Longan is containing glucose, sucrose and the various nutrients such as vitamin A, B.Wherein contain Having more is protein, fat and several mineral materials.These nutrients are all the most required to human body.Especially for working with one's mind People, consume sad temper blood, more effectively.Because containing the trace element of a large amount of useful healths, Arillus Longan becomes one already Taste good medicine.
Radix Angelicae Sinensis: call dry return, the Qin which, western Radix Angelicae Sinensis, Min Radix Angelicae Sinensis, Radix Angelicae Sinensis, Radix Angelicae Sinensis body, contain that Radix Angelicae Sinensis, Radix Angelicae Sinensis be bent, Radix Angelicae Gigatis, Perennial herb, high 0.4-1 rice.The month at florescence 6-7, really the phase 7-9 month.Radix Angelicae Sinensis sweet in the mouth, pungent, bitter, warm in nature.Radix Angelicae Sinensis has work of enriching blood Blood, menstruction regulating and pain relieving, effect of relaxing bowel, can be used for blood deficiency and yellow complexion,
The treatment of dizziness cardiopalmus, menoxenia, amenorrhea dysmenorrhea, asthenia cold abdominalgia, dryness of the intestine constipation, rheumatic arthralgia etc..In Radix Angelicae Sinensis Effective ingredient Radix Angelicae Sinensis polysaccharide has immunocompetence, and treatment tumor, radiation damage etc. have good therapeutic effect.Radix Angelicae Sinensis polysaccharide can affect to be made Blood system, promotes hemopoietic.
Radix Codonopsis: Chinese medicine Radix Codonopsis is Radix Platycodonis perennial grass wood plant Radix Codonopsis, element flower Radix Codonopsis, radix codonpsis tangshen and belongs to various plants together Dry root.Radix Codonopsis sweet in the mouth warm in nature, major function invigorating the spleen and replenishing QI, strengthening spleen and tonifying lung.Weak for splitting the deficiency of the lung, cardiopalmus of breathing hard, lack of appetite is just Half congealed, dyspnea due to deficiency is coughed, and interior-heat is quenched one's thirst.Chemical composition Radix Codonopsis polysaccharide in Radix Codonopsis has well immunity rise effect, scalable machine Body immunity, removes free radical, hemopoietic and antineoplastic action.
Fructus Lycii is the liver and the kidney tonifying Chinese medicine commonly used simply, and its color is scarlet, and its taste is fragrant and sweet.Modern medicine study confirms that it contains Betaine, polysaccharide, crude fat, crude protein, carotene, vitamin A, vitamin C, vitamin B1, vitamin B2 and calcium, phosphorus, The nutritional labelings such as ferrum, zinc, manganese, linoleic acid, have facilitation to hemopoietic function.
Bulbus Lilii has the highest medical value.The merits such as removing toxic substances, reason spleen stomach invigorating, dampness removing removing food stagnancy, mind tranquilizing and the heart calming, blood circulation promoting Effect.Cure mainly the diseases such as chronic cough, hemoptysis, fidgets due to deficiency palpitation with fear, treatment lung network disease and health-care antisenile are had special effect.According to pharmacological research Showing, dried lily bulb has the effect of leukocyte increasing, therefore has preferable curative effect to kinds cancer.
Herba Leonuri, has promoting blood flow to regulate menstruation, stasis-dispelling and pain-killing, inducing diuresis to remove edema, heat-clearing toxin-expelling functions, cure mainly menoxenia, dysmenorrhea, Amenorrhea, Hypomenorrhea, puerperal blood faints, abdominalgia with blood stasis, nephralgia edema, dysuria, hematuria etc..It contains various trace elements, Selenium has enhancing immunocyte vigor, relaxes atherosclerotic effect, manganese energy antioxidation, the effect of waiting for a long time of resisting fatigue, health care. Herba Leonuri also has beauty functions.
CORTEX ZINGIBERIS RHIZOMAE is pungent cool, controls skin edema, the row severe edema due to hypofunction of the spleen;The pungent temperature of Rhizoma Zingiberis Recens juice, pungent scattered cold syndrome of the stomach strength is strong, is used for vomiting; The pungent temperature of Rhizoma Zingiberis, warming middle-JIAO is instigated cold, and recuperating depleted YANG is promoted blood circulation, and warming the spleen strength of trembling with fear is big, and Rhizoma Zingiberis Preparatum acrid in the mouth hardship does not walk table in walking, the temperature part of the body cavity below the umbilicus, housing the bladder, kidneys and bowels is cold;Big gun Rhizoma Zingiberis Recens charcoal is warm in nature, and relatively homoiothermy divides cold;Roast Rhizoma Zingiberis Recens hardship temperature, relatively warming intestines and stomach is cold.Pungent and the scattered temperature of Rhizoma Zingiberis Recens, strengthening the spleen stomach, kind warming middle-JIAO fall Check is vomitted, and dehumidify the painful abdominal mass that disappears, and eliminating phlegm and stopping cough, with stopping nausea and vomiting by lowering the adverse flow of QI as length.Rhizoma Zingiberis Recens have in Chinese medicine and pharmacy dissipate, preventing or arresting vomiting, cough-relieving etc. Effect.Can be used to suppress tumor, appetite promoting and the spleen strengthening, reducing swelling and alleviating pain.
Compared with prior art, the beneficial effect that the present invention possesses:
The present invention uses the ceramic membrane filter Caulis Sacchari sinensis juice of two-stage difference membrane aperture size, uses secondary membrane concentrated juice raw Producing the rich functional nigecose of polyphenol, the functional components polyphenols in secondary membrane concentrated juice has obtained effective enrichment, relatively Traditional processing technology improves 4~8 times, thus improves quality and the nutritive value of nigecose.The eutrophy nigecose of gained is molten Turbidity after solution to 12 ° Bx is at below 1NTU, and the product nigecose fragrance of gained is strong, and in sepia, indices all reaches The national standard requirement of one-level nigecose (brown sugar).
Color value of clear juice obtained by two grades of nanofiltration membrane reduces by 40%~60% relative to mixed juice, haze reduction 99.99%, purity improves 1%~3%, and secondary membrane filtered juice can be used for white sugar and produces.
After obtaining heating material liquid, use the ceramic membrane of different membrane aperture size to carry out twice filtration, first use larger aperture Ceramic membrane filter remove most of non-sugar impurity such as the ash in mixed juice, colloid, little granule sugarcane marrow, then use smaller aperture due Membrane filtration one-level clear juice, the polyphenols etc. in effectively catching one-level film clear juice, obtain polyphenols enrichment two grades Membrance concentration juice produces for the rich functional nigecose of polyphenol, obtains colour, turbidity relatively low simultaneously, and the secondary membrane clear juice that purity is higher can Produce for white sugar.And in the prior art, the technique not yet occurring syrup is passed through twice filtration treatment.
The primary ceramic membrane in aperture 50~200nm, two grades of NF membrane of molecular cut off 1~5kDa, only utilize above-mentioned The film in aperture carries out double-filtration could reduce other influences nigecose product while ensureing polyphenols enrichment as far as possible The invalid impurity of matter.
The present invention with the addition of the functional components of multiple integration of edible and medicinal herbs in nigecose, enriches nigecose taste, meets not With the selection of consumer, also further increase the nutritional labeling of nigecose simultaneously.
Detailed description of the invention
Below by embodiment, technical scheme is further elaborated.
Embodiment 1
The processing method of a kind of rich functional nigecose of polyphenol, comprises the steps:
(1) take sugarcane slightly with the Caulis Sacchari sinensis of sugarcane leaf as raw material;
(2) crushing sugar cane obtains mixed juice, utilizes 100 mesh vibrosieves to remove the large granular impurities such as bagasse, then revolves with 200 mesh The sieve that shakes removes little granule foreign, obtains material liquid;
(3) material liquid first adds lime cream regulation pH to 7.5, then is heated to 60 DEG C by pipe heat exchanger, pump to baffle-box, With being steam heated to 85 DEG C, obtain heating material liquid;
(4) carrying out clarification filtration, transmembrane pressure 0.45Mpa, crossflow velocity 4m/s by 50nm primary ceramic membrane, volume is dense Demagnification number is 10, to remove most of non-sugar impurity such as antibacterial in mixed juice, ash, colloid, obtain one-level film clear juice and One-level film-filter concentration liquid, one-level membrance concentration liquid is pumped in material liquid after membrance concentration liquid clarifying treatment system;
(5) one-level film evaporator supplypump is delivered to and in secondary membrane material liquid tank, by two grades of NF membrane that molecular cut off is 1kDa Filtering, transmembrane pressure 1.0Mpa, crossflow velocity 5.5m/s, filter temperature 70 DEG C, volume concentration multiple is 8, secondary membrane effectively catching Polyphenols etc. in one-level clear juice, respectively obtains colour, turbidity is relatively low, purity is higher secondary membrane clear juice and rich in polyphenol The secondary membrane concentrated juice of class material;Secondary membrane evaporator supplypump is delivered to sugar refinery clear juice case and is produced for white sugar, and secondary membrane concentrated juice is used In producing the rich functional nigecose of polyphenol, concrete grammar is as follows:
First, count by weight, weigh 2 parts of Colla Corii Asini, Fructus Jujubae 10 parts, Arillus Longan 5 parts, Radix Angelicae Sinensis 1 part, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 2 parts, Herba Leonuri 1 part and 1 part of Rhizoma Zingiberis Recens, add 8~10 times of weight water, decocts 60min, waste taking juice,
Then, secondary membrane concentrated juice passes through falling film type vacuum vaporation system, is concentrated into 65 ° of BX, adds above-mentioned decoction and obtains Juice, after stirring, stir off under atmospheric pressure state to sweet cake brix 94~95 ° of BX with interlayer iron pan, move to help by sweet cake Brilliant case, pour into after stirring graining be covered with through strict sterilization sterilization food paper using wood mold coupled in, allow its natural cooling become Type, is packaged to be the rich functional nigecose of polyphenol after removing paper.
The quality of the present embodiment gained one-level film clear juice, secondary membrane clear juice and secondary membrane concentrated juice is as shown in table 1, and finished product is black Sugar products matter is as shown in table 2.
The quality of sugarcane juice before and after table 1. film excessively
The indices contrast of table 2. finished product nigecose
Note: total sugar is divided into reducing sugar content+Sucrose
Embodiment 2
The processing method of a kind of rich functional nigecose of polyphenol, comprises the steps:
(1) take sugarcane slightly with the Caulis Sacchari sinensis of sugarcane leaf as raw material;
(2) cane milling obtains mixed juice, utilizes 50 mesh vibrosieves to remove the bulky grain sugarcane marrows etc. such as bagasse, then uses 250 mesh Spin vibration sieve filters, and removes short grained impurity, obtains material liquid;
(2) material liquid first adds lime cream regulation pH to 7.0, then is heated to 55 DEG C by pipe heat exchanger, and pump is to head tank Baffle-box, with being steam heated to 80 DEG C, obtains heating material liquid;
(3) clarification filtration, transmembrane pressure 0.35Mpa, crossflow velocity 4.5m/s, body are carried out by 100nm primary ceramic membrane Long-pending cycles of concentration is 10, to remove the major part impurity such as antibacterial in mixed juice, ash, colloid, obtains one-level film clear juice and Level film-filter concentration liquid, one-level membrance concentration liquid is pumped in material liquid after membrance concentration liquid clarifying treatment system;
(4) one-level film evaporator supplypump is delivered to and in secondary membrane material liquid tank, by two grades of NF membrane that molecular cut off is 5kDa Filtering, transmembrane pressure is 0.6Mpa, crossflow velocity 5m/s, filters temperature 75 DEG C, and volume concentration multiple is 10, effectively catching one-level film The polyphenols etc. of clear juice, respectively obtains colour, turbidity is relatively low, purity is higher secondary membrane clear juice and rich in polyphenols Secondary membrane concentrated juice;Secondary membrane evaporator supplypump is delivered to sugar refinery clear juice case and is produced for white sugar, and secondary membrane concentrated juice is used for producing The rich functional nigecose of polyphenol, concrete grammar is as follows:
First, count by weight, weigh 10 parts of Colla Corii Asini, Fructus Jujubae 5 parts, Arillus Longan 2 parts, Radix Angelicae Sinensis 2 parts, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 3 parts, Herba Leonuri 2 parts and 3 parts of Rhizoma Zingiberis Recens, clean enucleation of shelling by above-mentioned raw materials component, and drying to water content is less than After 5 percent, pulverize in the lump, cross 80~100 mesh sieves, obtain powder;
Then, secondary membrane concentrated juice passes through falling film type vacuum vaporation system, is concentrated into 65 ° of BX, adds above-mentioned powder, powder Addition is secondary membrane concentrated juice evaporation and concentration to after 60~65 ° of BX the 10% of weight, after stirring, with interlayer iron pan often Stir off under pressure condition to sweet cake brix 94~95 ° of BX, sweet cake is moved to crystallization in motion case, pour into after stirring graining and be covered with through strictly disappearing The food paper using of sterilization wood mold coupled in, allow its natural cooling molding, after removing paper, be packaged to be the rich functional nigecose of polyphenol.
Embodiment 3
The processing method of a kind of rich functional nigecose of polyphenol, comprises the steps:
(1) cane milling obtains mixed juice, utilizes 80 mesh vibrosieves to remove the large granular impurities such as bagasse, then uses 300 mesh Spin vibration sieve removes little granule foreign, obtains material liquid;
(2) material liquid first adds lime cream regulation pH to 7.2, then is heated to 65 DEG C by pipe heat exchanger, and pump is to head tank Baffle-box, with being steam heated to 90 DEG C, obtains heating material liquid;
(3) clarification filtration, transmembrane pressure 0.25Mpa, crossflow velocity 5m/s, volume are carried out by 200nm primary ceramic membrane Cycles of concentration is 10, to remove the major part impurity such as antibacterial in mixed juice, ash, colloid, obtains one-level film clear juice and one-level film Filter concentration liquid, one-level membrance concentration liquid is pumped in material liquid after membrance concentration liquid clarifying treatment system;
(4) one-level film evaporator supplypump is delivered to and in secondary membrane material liquid tank, by the secondary membrane of molecular cut off 2kDa, across Mould difference is 0.8Mpa, crossflow velocity 4.5m/s, filters temperature 70 DEG C, and volume concentration multiple is 8, many in effectively catching one-level clear juice Aldehydes matters etc., respectively obtain colour, turbidity is relatively low, purity is higher secondary membrane clear juice and the secondary membrane rich in polyphenols Concentrated juice;Secondary membrane evaporator supplypump is delivered to sugar refinery clear juice case and is produced for white sugar, and secondary membrane concentrated juice is used for producing rich polyphenol merit Energy property nigecose, concrete grammar is as follows:
First, arbitrarily weighing Colla Corii Asini, Fructus Jujubae, Arillus Longan, Radix Angelicae Sinensis, Radix Codonopsis, Fructus Lycii, Bulbus Lilii, Herba Leonuri and Rhizoma Zingiberis Recens, weight is two Level membrance concentration juice evaporation and concentration, to after 60~65 ° of BX the 5% of weight, adds 8~10 times of weight water, decoction 60min, waste extracting juice Liquid;Or pulverize, cross 80~100 mesh sieves, obtain powder;
Then, secondary membrane concentrated juice passes through falling film type vacuum vaporation system, is concentrated into 65 ° of BX, adds above-mentioned decoction and obtains Juice or powder, after stirring, stir off under atmospheric pressure state to sweet cake brix 94~95 ° of BX with interlayer iron pan, by sugar Cake moves to crystallization in motion case, pour into after stirring graining be covered with through strict sterilization sterilization food paper using wood mold coupled in, allow its from So cool down molding, after removing paper, be packaged to be the rich functional nigecose of polyphenol.

Claims (8)

1. the processing method of the functional nigecose of rich polyphenol, it is characterised in that comprise the steps:
(1) take sugarcane slightly with the Caulis Sacchari sinensis of sugarcane leaf as raw material, squeeze the juice and tentatively go the removal of impurity, obtaining material liquid;
(2) material liquid first adds lime cream regulation pH to 7.0~7.5, is again heated to 80~90 DEG C, obtains heating material liquid;
(3) use the primary ceramic membrane filtering and heating material liquid in aperture 50~200nm, obtain one-level film clear juice and one-level membrance concentration Juice;
(4) use the secondary membrane one-level film clear juice of molecular cut off 1~5kDa, obtain secondary membrane clear juice and aldehydes matter is rich The secondary membrane concentrated juice of collection;
(5) secondary membrane concentrated juice is used for producing the rich functional nigecose of polyphenol, and concrete grammar is as follows:
First, choose at least one in Colla Corii Asini, Fructus Jujubae, Arillus Longan, Radix Angelicae Sinensis, Radix Codonopsis, Fructus Lycii, Bulbus Lilii, Herba Leonuri and Rhizoma Zingiberis Recens or Several as functional components, boiling taking juice or be dried and crushed into powder,
Then, secondary membrane concentrated juice evaporation and concentration to 60~65 ° of BX, add juice or the powder of above-mentioned functions composition, stir Mix uniformly, stir off at ambient pressure to sweet cake brix 94~96 ° of BX, pour in mould after sweet cake stirring graining, natural cooling molding After, it is packaged to be the rich functional nigecose of polyphenol.
2. the processing method of the rich functional nigecose of polyphenol as claimed in claim 1, it is characterised in that secondary membrane clear juice is for white Saccharum Sinensis Roxb. produces.
3. the processing method of the functional nigecose of rich polyphenol as described in claim 1 is any, it is characterised in that one-level membrance concentration juice It is pumped in material liquid after carbonation, filter press.
4. the processing method of the functional nigecose of rich polyphenol as described in claims 1 to 3 any one, it is characterised in that step (3) transmembrane pressure 0.25~0.45Mpa, crossflow velocity 4~5m/s, volume concentration is 8~12 again.
5. the processing method of the functional nigecose of rich polyphenol as described in claims 1 to 3 any one, it is characterised in that step (4) transmembrane pressure is 0.6~1.0Mpa, crossflow velocity 4.5~5.5m/s, and volume concentration multiple is 8~10.
6. the processing method of the functional nigecose of rich polyphenol as described in claims 1 to 3 any one, it is characterised in that step (5) in, count by weight, 2 parts of Colla Corii Asini, Fructus Jujubae 10 parts, Arillus Longan 5 parts, Radix Angelicae Sinensis 1 part, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 2 Part, Herba Leonuri 1 part and 1 part of Rhizoma Zingiberis Recens.
7. the processing method of the functional nigecose of rich polyphenol as described in claims 1 to 3 any one, it is characterised in that step (5) in, count by weight, 10 parts of Colla Corii Asini, Fructus Jujubae 5 parts, Arillus Longan 2 parts, Radix Angelicae Sinensis 2 parts, Radix Codonopsis 1 part, Fructus Lycii 0.5 part, Bulbus Lilii 3 Part, Herba Leonuri 2 parts and 3 parts of Rhizoma Zingiberis Recens.
8. the processing method of the functional nigecose of rich polyphenol as described in claims 1 to 3 any one, it is characterised in that step (5), in, adding the gross weight of functional components is secondary membrane concentrated juice evaporation and concentration to after 60~65 ° of BX the 5~15% of weight.
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CN106819332A (en) * 2017-02-09 2017-06-13 合肥原素坊食品有限公司 A kind of green tea brown sugar and preparation method thereof
CN107149021A (en) * 2017-04-26 2017-09-12 广西怡神糖业有限公司 A kind of production method of longan-jujube brown sugar block
CN107788504A (en) * 2017-09-22 2018-03-13 广州天惠食品股份有限公司 A kind of brown sugar syrup and preparation method thereof

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