CN106120408A - A kind of digit printing technique of silk fabric - Google Patents
A kind of digit printing technique of silk fabric Download PDFInfo
- Publication number
- CN106120408A CN106120408A CN201610504359.1A CN201610504359A CN106120408A CN 106120408 A CN106120408 A CN 106120408A CN 201610504359 A CN201610504359 A CN 201610504359A CN 106120408 A CN106120408 A CN 106120408A
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- CN
- China
- Prior art keywords
- corn starch
- silk fabric
- printing technique
- brucite
- friendly type
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
- D06P1/6491—(Thio)urea or (cyclic) derivatives
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/10—Material containing basic nitrogen containing amide groups using reactive dyes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Coloring (AREA)
Abstract
A kind of digit printing technique of silk fabric, the thickener used is on the basis of tradition thickener, add brucite, utilize the architectural characteristic that it is special, it is only necessary to add a small amount of sodium hydroxide and ethanol and under citric acid effect, common ball milling, i.e. can reach the modification to corn starch, whole course of reaction is simple, without harmful Organic substance, is the preparation method of the dyeing paste of a kind of environment-friendly type.
Description
Technical field
The present invention relates to digital printing technology field, particularly relate to the digit printing technique of a kind of silk fabric.
Background technology
Digital ink-jet printed technology is that inkjet printing is expanded greatly in the one of industrial application.Modern computer inkjet printing
Technology, can be with various input mediums such as scanner, digital camera, digital camera etc. when printing in textiles, needing
The pattern wanted is with digital input computer, after various mapping software color separation in printing systems process, then through computer control
The digital inkjet printing machine of system, is directly ejected into printing ink on various fabric, prints out required various patterns, this
Plant printing technique and be referred to as digital inking printing.
In recent years, digital printing technology has obtained rapid development.Compared with Conventional decal, digit printing technique cleans,
Production process is flexible, can remotely order goods, include supply chain network in, is the direction of following printing in textiles technology development.
But due to the characteristic of mulberry silk, its fabric face is relatively smooth, ink-jet printed the most but do not reach intended effect
Really, there is a lot of problem, the most ink-jet printed color depth on the textile is inadequate, bigger etc. with the aberration of electronics pattern,
Thus limit the development of textile inkjet printing.
In printing with reactive dye, thickener is commonly used as thickening agent to regulate the rheological property of mill base.Sodium alginate is because of it not
React with reactive dye, the advantage such as tinctorial yield is high, chromatograph is complete, easily wash away from fabric, fabrics feel soft, the most active
The first-selection of reactive dye printing paste.But it is expensive, stamp cost is of a relatively high, therefore finds a kind of with low cost, it is possible to should
For digital printing technology, the thickener printing fine chemical wastewater has become as the task of top priority.
Summary of the invention
In order to solve the problem in background technology, the present invention provides the digit printing technique of a kind of silk fabric.
The digit printing technique of a kind of silk fabric, comprises the following steps: textile sizing → drying → spray printing → decatize →
Cold water washes → and hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 5-7%, carbamide 1-
2%, water surplus.
Preferably, described spray printing operation uses reactive dye.
The effect of carbamide is moisture absorption in steaming procedure, makes fiber swelling, helps dyestuff to permeate in fiber and upper dye fibre
Dimension, but amount of urea is crossed conference and is made pretreating fabrics a large amount of moisture absorptions during depositing, and the process of soaping after stamp will make waste water
In urea content be greatly increased, cause environment oxygen-enriched, therefore should strictly control the consumption of carbamide.Along with amount of urea increases,
The tinctorial yield printing fabric face has the trend of increase, but increasing degree is little, and amount of urea tinctorial yield when 1-2% is preferable.
The preparation method of described environment-friendly type dyeing paste, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product.
Preferably, the particle diameter of the described brucite described in step A is 200-500 μm；
Preferably, the particle diameter of the described corn starch described in step A is 80-200 μm；
Preferably, the particle diameter of the described modified corn starch described in step B is 10-30 μm.
Preferably, described environment-friendly type dyeing paste, including following main component:
Corn starch 60-75%
Sodium alginate 5-8%
Brucite 3-5%
Sodium hydroxide 1-2%
Galactomannan 10-15%
Ethanol 1-2%
Citric acid surplus.
Hydrotalcite material belongs to anion type laminated compound.Lamellar compound refers to have layer structure, interlayer ion
There is a compounds of interchangeability, utilize the intercalation that lamellar compound main body is had under highly polar molecular action
With the interchangeability of interlayer ion, some functional guest species are introduced bedding void and laminate distance is strutted thus is formed
Layer-pillared compound.Hydrotalcite-based compound (LDHs) is the novel inorganic functional material that a class has layer structure, the master of LDHs
Body laminate chemical composition and its laminate cationic characteristic, laminate charge density or anion exchange capacity, supermolecular intercalation structure
Closely related etc. factor.
The digit printing technique of the silk fabric of the present invention, adds environment-friendly type dyeing paste, thus in sizing process
Without adding Matrii Sulfas Exsiccatus, inorganic salt, decrease salt pollute, if simultaneously because environment-friendly type dyeing paste be added to the water after in alkalescence,
Therefore without adding alkaline matter regulation pH value.Described environment-friendly type dyeing paste is on the basis of tradition thickener, adds water
Talcum, utilizes the architectural characteristic that brucite is special, it is only necessary to add a small amount of sodium hydroxide and ethanol and under citric acid effect, altogether
Same ball milling, i.e. can reach the modification to corn starch, and whole course of reaction is simple, without harmful Organic substance.
Specific implementation method
Embodiment 1
The digit printing technique of a kind of silk fabric, comprises the following steps: textile sizing → drying → spray printing → decatize → cold water
Wash → hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 6%, carbamide
1.5%, water surplus；
Described spray printing operation uses reactive dye；
Described environment-friendly type dyeing paste, including following main component:
Corn starch 70%
Sodium alginate 7%
Brucite 3.5%
Sodium hydroxide 1.5%
Galactomannan 12.5%
Ethanol 1.5%
Citric acid surplus.
The preparation method of described environment-friendly type dyeing paste, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product.
The particle diameter of the described brucite described in step A is 200-500 μm；
The particle diameter of the described corn starch described in step A is 80-200 μm；
The particle diameter of the described modified corn starch described in step B is 10-30 μm.
Embodiment 2
The digit printing technique of a kind of silk fabric, comprises the following steps: textile sizing → drying → spray printing → decatize → cold water
Wash → hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 7%, carbamide 1%,
Water surplus；
Described spray printing operation uses reactive dye；
Described environment-friendly type dyeing paste, including following main component:
Corn starch 60%
Sodium alginate 8%
Brucite 5%
Sodium hydroxide 2%
Galactomannan 15%
Ethanol 2%
Citric acid surplus.
The preparation method of described environment-friendly type dyeing paste, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product.
The particle diameter of the described brucite described in step A is 200-500 μm；
The particle diameter of the described corn starch described in step A is 80-200 μm；
The particle diameter of the described modified corn starch described in step B is 10-30 μm.
Embodiment 3
The digit printing technique of a kind of silk fabric, comprises the following steps: textile sizing → drying → spray printing → decatize → cold water
Wash → hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 5%, carbamide 2%,
Water surplus；
Described spray printing operation uses reactive dye；
Described environment-friendly type dyeing paste, including following main component:
Corn starch 75%
Sodium alginate 5%
Brucite 3%
Sodium hydroxide 1%
Galactomannan 10%
Ethanol 1%
Citric acid surplus.
The preparation method of described environment-friendly type dyeing paste, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product.
The particle diameter of the described brucite described in step A is 200-500 μm；
The particle diameter of the described corn starch described in step A is 80-200 μm；
The particle diameter of the described modified corn starch described in step B is 10-30 μm.
The digit printing technique of the silk fabric of embodiment 1-3 is carried out spray printing, respectively to C (blue or green), M (pinkish red), Y
(yellow), the color fastness of K (black) 4 kinds of colored fabrics are tested, and the results are shown in Table 1.
Table 1:
| 50 WASHING COLOR FASTNESSs | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Blue or green | 4 grades | 4 grades | 4 grades |
| Pinkish red | 4 grades | 4 grades | 4 grades |
| Yellow | 4 grades | 4 grades | 4 grades |
| Black | 4 grades | 4 grades | 4 grades |
By test data it is recognised that the product made of the present invention, color fastness is high, even across being cleaned multiple times, remain to colour-fast,
Fade, keep original color and vividness.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (8)
1. the digit printing technique of a silk fabric, it is characterised in that comprise the following steps: textile sizing → drying → spray printing
→ decatize → cold water washes → and hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 5-7%, carbamide 1-
2%, water surplus.
The digit printing technique of silk fabric the most according to claim 1, it is characterised in that make in described spray printing operation
Use reactive dye.
The digit printing technique of silk fabric the most according to claim 1, it is characterised in that described environment-friendly type printing and dyeing are stuck with paste
Material, including following main component:
Corn starch 60-75%
Sodium alginate 5-8%
Brucite 3-5%
Sodium hydroxide 1-2%
Galactomannan 10-15%
Ethanol 1-2%
Citric acid surplus.
The digit printing technique of silk fabric the most according to claim 1, it is characterised in that described environment-friendly type printing and dyeing are stuck with paste
The preparation method of material, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product.
The digit printing technique of silk fabric the most according to claim 4, it is characterised in that described in described step A
The particle diameter of brucite be 200-500 μm.
The digit printing technique of silk fabric the most according to claim 4, it is characterised in that described in described step A
The particle diameter of corn starch be 80-200 μm.
The digit printing technique of silk fabric the most according to claim 4, it is characterised in that described in described step B
The particle diameter of modified corn starch be 10-30 μm.
The digit printing technique of silk fabric the most according to claim 1, it is characterised in that comprise the following steps:
Textile sizing → drying → spray printing → decatize → cold water washes → and hot water wash → soap → hot water wash → cold water washes → dries；
In described textile sizing operation, slurry therewith percentage composition by weight is as follows: environment-friendly type dyeing paste 6%, carbamide 1.5%,
Water surplus；
Described spray printing operation uses reactive dye；
The preparation method of described environment-friendly type dyeing paste, comprises the following steps:
A, corn starch and sodium hydroxide, brucite are sufficiently mixed after, use screw extruder extruding, later half at extruder
Journey sprays ethanol to material, and finally dry, mechanical activation comminution, prepares powder；
B, the powder in step A and citric acid are added in deionized water, through high speed ball milling, be finally spray-dried, changed
Property corn starch；
C into, modified corn starch, galactomannan, sodium alginate are poured stirring mixing in agitator, to obtain final product；
The particle diameter of the described brucite described in step A is 200-500 μm；
The particle diameter of the described corn starch described in step A is 80-200 μm；
The particle diameter of the described modified corn starch described in step B is 10-30 μm；
Described environment-friendly type dyeing paste, including following main component:
Corn starch 70%
Sodium alginate 7%
Brucite 3.5%
Sodium hydroxide 1.5%
Galactomannan 12.5%
Ethanol 1.5%
Citric acid surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610504359.1A CN106120408B (en) | 2016-06-28 | 2016-06-28 | A kind of digital printing process of silk fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610504359.1A CN106120408B (en) | 2016-06-28 | 2016-06-28 | A kind of digital printing process of silk fabric |
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| Publication Number | Publication Date |
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| CN106120408A true CN106120408A (en) | 2016-11-16 |
| CN106120408B CN106120408B (en) | 2018-10-26 |
Family
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| CN201610504359.1A Active CN106120408B (en) | 2016-06-28 | 2016-06-28 | A kind of digital printing process of silk fabric |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758382A (en) * | 2017-01-03 | 2017-05-31 | 广州强品新材料有限公司 | A kind of reactive dye digit printing slurry of environmental protection |
| CN112267313A (en) * | 2020-11-05 | 2021-01-26 | 湖州金玺丝绸科技股份有限公司 | Light-color printing process of washable silk fabric |
Citations (4)
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|---|---|---|---|---|
| CN101864092A (en) * | 2010-06-13 | 2010-10-20 | 陕西科技大学 | Layered silicate clay-based starch suspension stabilizer and preparation method thereof |
| CN102174739A (en) * | 2011-01-20 | 2011-09-07 | 日冠(福建)针纺织机械有限公司 | Preparation method and application of digital inkjet printing fabric pretreatment agent |
| CN103451970A (en) * | 2013-09-10 | 2013-12-18 | 石家庄市荷西服饰贸易有限公司 | Digital reactive dye printing process for mulberry silk fabric |
| CN103911885A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Printing and dyeing paste |
-
2016
- 2016-06-28 CN CN201610504359.1A patent/CN106120408B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101864092A (en) * | 2010-06-13 | 2010-10-20 | 陕西科技大学 | Layered silicate clay-based starch suspension stabilizer and preparation method thereof |
| CN102174739A (en) * | 2011-01-20 | 2011-09-07 | 日冠(福建)针纺织机械有限公司 | Preparation method and application of digital inkjet printing fabric pretreatment agent |
| CN103451970A (en) * | 2013-09-10 | 2013-12-18 | 石家庄市荷西服饰贸易有限公司 | Digital reactive dye printing process for mulberry silk fabric |
| CN103911885A (en) * | 2014-04-17 | 2014-07-09 | 苏州润弘贸易有限公司 | Printing and dyeing paste |
Non-Patent Citations (1)
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| 胡华宇等: ""淀粉柠檬酸酯的固相酯化反应制备"", 《湖北农业科学》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758382A (en) * | 2017-01-03 | 2017-05-31 | 广州强品新材料有限公司 | A kind of reactive dye digit printing slurry of environmental protection |
| CN112267313A (en) * | 2020-11-05 | 2021-01-26 | 湖州金玺丝绸科技股份有限公司 | Light-color printing process of washable silk fabric |
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| CN106120408B (en) | 2018-10-26 |
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