CN106118883B - Camphor tree essential oil leaching device and application - Google Patents
Camphor tree essential oil leaching device and application Download PDFInfo
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- CN106118883B CN106118883B CN201610518072.4A CN201610518072A CN106118883B CN 106118883 B CN106118883 B CN 106118883B CN 201610518072 A CN201610518072 A CN 201610518072A CN 106118883 B CN106118883 B CN 106118883B
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- extraction tank
- essential oil
- pipe
- mixing
- pump
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- 241000723346 Cinnamomum camphora Species 0.000 title claims abstract description 36
- 239000000341 volatile oil Substances 0.000 title claims abstract description 29
- 238000002386 leaching Methods 0.000 title claims abstract description 17
- 238000000605 extraction Methods 0.000 claims abstract description 36
- 238000002156 mixing Methods 0.000 claims abstract description 33
- 238000007789 sealing Methods 0.000 claims abstract description 7
- 230000000903 blocking effect Effects 0.000 claims abstract 5
- 238000007599 discharging Methods 0.000 claims abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 3
- 238000005265 energy consumption Methods 0.000 abstract description 6
- 241000196324 Embryophyta Species 0.000 abstract description 5
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 description 13
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 10
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 7
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 4
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 229930007744 linalool Natural products 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 3
- 210000000170 cell membrane Anatomy 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- -1 open the pump Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 1
- 230000036592 analgesia Effects 0.000 description 1
- 230000002155 anti-virotic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0223—Moving bed of solid material
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a camphor tree essential oil leaching device and application, and the camphor tree essential oil leaching device comprises an extraction tank (2), a mixing pipe (3), a pump (6) and a feeding port (9), wherein the mixing pipe (3) is fixed on a central axis of the extraction tank (2) through a mixing pipe support rod (3b), one end of the extraction tank (2) is provided with a nozzle (8) in a sealing cover manner, the other end of the extraction tank (2) is provided with a blocking cover (1), the nozzle (8) is communicated with a discharging port of the pump (6) through a circulating pipe (7) provided with a heater (5), the feeding port of the pump (6) is connected with the other port of the extraction tank (2) through the circulating pipe (7), the feeding port (9) is arranged above the extraction tank (2), and the bottom of the extraction tank (2) is also provided with a discharging port (4). The device has the advantages of simple structure, reasonable design, low energy consumption, low cost, high extraction rate and the like, is suitable for extracting camphor tree essential oil and other plant active ingredients, and has wide application value.
Description
Technical Field
The invention relates to the technical field of essential oil extraction, in particular to a camphor tree essential oil leaching device and application.
Background
The camphor tree essential oil is colorless or light yellow oily transparent liquid at normal temperature, partial components can separate out solid components at normal temperature, and the camphor tree essential oil has strong special smell, strong volatility and high refractive index and optical rotation mostly; the specific gravity is between O.86 and 1.065; the product is hardly soluble in water, can be completely soluble in absolute ethyl alcohol, can be soluble in organic solvents with small polarity such as ether, chloroform, petroleum ether and the like, is sensitive to air, light and temperature, and is easy to volatilize and decompose.
The camphor tree essential oil contains linalool, linalool and the like in the largest content, is known as 3, 7-dimethyl-1, 6-octadien-3-ol in a chemical formula C10H18And O. Linalool is colorless or light yellow transparent liquid, is insoluble in water, can be dissolved in ethanol and diethyl ether, has pleasant sweet smell, soft fragrance, and is widely applied to spices, essence, perfume and perfumed soap, is important in monomer spices, and is called as spice Meiwang; meanwhile, linalool is a raw material for synthesizing vitamin E, and is applied to medicines due to the effects of antibiosis, antivirus, analgesia and the like.
In recent years, researchers have made more studies on the extraction method of camphor tree essential oil, but have made less studies on the production apparatus thereof. In the camphor tree essential oil extraction device, the problems of high energy consumption, high production cost, uneven heating, low yield, long extraction time and the like still exist. With the rapid development of the perfume industry and the pharmaceutical industry, the demand of camphor tree essential oil is increasing year by year. Therefore, it is very important to research a camphor tree essential oil extraction device with high yield, low energy consumption and low cost.
Disclosure of Invention
Aiming at the technical problems of the conventional camphor tree essential oil extraction device, the invention provides the camphor tree essential oil extraction device with high extraction rate, low energy consumption and low cost.
In order to achieve the purpose, the invention is realized by the following technical scheme:
the utility model provides a camphor tree essential oil leaching device, is including drawing jar, hybrid tube, pump and charge door, the hybrid tube is fixed on the axis of drawing the jar through the hybrid tube bracing piece, the one end closing cap of drawing the jar is equipped with the nozzle, and the other end of drawing the jar is equipped with the fender lid, the fender lid is fixed on the closing cap of drawing the jar through keeping off the lid bracing piece, the nozzle is through the circulating pipe that is equipped with the heater and the discharge gate intercommunication of pump, the feed inlet of pump passes through the circulating pipe and is connected with another port of drawing the jar, the top of drawing the jar is equipped with the charge door, and the bottom of drawing the jar still is equipped with the bin outlet.
Preferably, the above extraction tank is further provided with a temperature measuring instrument.
Preferably, a water filling port is arranged between the upper part of the extraction tank and the circulating pipe.
Preferably, a pressure gauge and a safety valve are further arranged above the extracting tank.
Preferably, the above-mentioned feed inlet is provided with a quick-opening sealing cover.
Preferably, 3-4 supporting rods are arranged on the baffle cover.
Preferably, the mixing pipe is an internal spiral pipe body, and a trumpet-shaped feed inlet is formed in one end, corresponding to the nozzle, of the mixing pipe.
Preferably, 8-12 support rods of the mixing tube are arranged on the front section and the rear section of the mixing tube respectively.
Preferably, the connection mode of the circulating pipe is flange type or quick-opening type joint connection.
The use method of the device comprises the following steps: during the use, open the charge door of extracting the jar, add solvent and cinnamomum camphora leaf material, open the pump, solvent and cinnamomum camphora leaf mix through pump pressurization, nozzle jet mixes, the mixing tube mixes, the mixed reflection of shelves lid, jar body flow mixes 6 of the mixed and pipeline flow mixes with higher speed leaching mixed area for collision that cinnamomum camphora leaf powder material and solvent can be abundant accelerates the infiltration of solvent to cinnamomum camphora leaf cell membrane, and cinnamomum camphora essential oil releases from the cell.
The leaching device is suitable for extracting camphor tree essential oil and other plant effective components.
Compared with the prior art, the invention has the advantages and beneficial effects that:
1. according to the device, 6 accelerated leaching mixing areas of pump pressurization mixing, nozzle jet mixing, mixing pipe mixing, baffle cover reflection mixing, tank body flow mixing and pipeline flow mixing are designed, so that camphor tree leaf powder materials and a solvent can be fully collided, the permeation of the solvent to camphor tree leaf cell membranes is accelerated, camphor tree essential oil is more easily released from cells, the materials and the solvent flow back continuously, solute diffusion is facilitated, and the oil yield of the essential oil is improved.
2. The device of the invention achieves a back flushing effect between the materials and the solvent by designing the mixing pipe and the baffle cover of the internal screw, accelerates the flushing of the leaching materials, and improves the solvent permeability of the leaching materials and the extraction rate of the essential oil.
3. The device of the invention improves the pressure of the discharge port circulating pipe of the pump by designing the nozzle to form pressurized leaching.
4. The device of the invention is provided with the heater on the circulating pipe, and can adapt to the extraction of effective components of plants at different temperatures by controlling the heating power.
5. The device of the invention is convenient for feeding and maintaining the interior of the extraction tank by designing the large-caliber feeding port of the quick-opening type sealing cover.
6. Compared with the conventional steam distillation, the solvent extraction device has the advantages of lower energy consumption, higher extraction efficiency and higher production efficiency, and can solve the problems that the effective components of the steam distillation are easy to dissipate and the like.
7. The oil yield of the camphor tree essential oil extracted by the traditional method is generally 1.8-2.2%, and the oil yield of the extraction device of the invention reaches more than 2.5%.
8. The device has the advantages of simple structure, reasonable design, low energy consumption, low cost, high extraction rate and the like, is suitable for extracting camphor tree essential oil, can also be used for extracting active ingredients of other plants, and has wide application value.
Drawings
FIG. 1 is a schematic view of the leaching apparatus for camphor tree essential oil according to the present invention;
in the reference numerals, 1-baffle cover, 2-extraction tank, 3-mixing tube, 3 a-mixing tube feed inlet, 3 b-mixing tube support rod, 4-discharge outlet, 5-heater, 6-pump, 7-circulating tube, 8-nozzle, 9-feed inlet, 10-water inlet, 11-temperature measuring instrument, 12-pressure gauge, 13-safety valve.
Detailed Description
The invention will be further described with reference to the following figures and specific examples, without limiting the scope of the invention.
Example 1
As shown in the drawing, a camphor tree essential oil leaching device, including extracting jar 2, hybrid tube 3, pump 6 and charge door 9, hybrid tube 3 is fixed on the axis of extracting jar 2 through hybrid tube bracing piece 3b, the one end closing cap of extracting jar 2 is equipped with nozzle 8, and the other end of extracting jar 2 is equipped with fender lid 1, fender lid 1 is fixed on the closing cap of extracting jar 2 through keeping off lid bracing piece 1a, nozzle 8 is through the discharge gate intercommunication of circulating pipe 7 and pump 6 that is equipped with heater 5, the feed inlet of pump 6 passes through circulating pipe 7 and is connected with another port of extracting jar 2, the top of extracting jar 2 is equipped with charge door 9, and the bottom of extracting jar 2 still is equipped with bin outlet 4.
The extracting tank 2 is also provided with a temperature measuring instrument 11.
A water filling opening 10 is arranged between the upper part of the extracting tank 2 and the circulating pipe 7.
A pressure gauge 12 and a safety valve 13 are also arranged above the extracting tank 2.
The feed inlet is provided with a quick-opening type sealing cover.
The mixing pipe 3 is an internal spiral pipe body, and one end of the mixing pipe 3 corresponding to the nozzle 8 is provided with a horn-shaped feeding hole.
3-4 supporting rods for the retaining cover are arranged on the supporting rod 1 a.
The support rods 3b of the mixing pipe are designed into 8-12 pieces and are respectively arranged at the front section and the rear section of the mixing pipe.
The circulating pipe 7 is connected by a flange type or quick-opening type joint.
The use method of the device comprises the following steps: during the use, open the charge door of extracting the jar, add solvent and cinnamomum camphora leaf material, open the pump, solvent and cinnamomum camphora leaf mix through pump pressurization, nozzle jet mixes, the mixing tube mixes, the mixed reflection of shelves lid, jar body flow mixes 6 of the mixed and pipeline flow mixes with higher speed leaching mixed area for collision that cinnamomum camphora leaf powder material and solvent can be abundant accelerates the infiltration of solvent to cinnamomum camphora leaf cell membrane, and cinnamomum camphora essential oil releases from the cell.
The leaching device is suitable for extracting camphor tree essential oil and other plant effective components.
Claims (1)
1. The utility model provides a camphor tree essential oil leaching device which characterized in that: the device comprises an extraction tank (2), a mixing tube (3), a pump (6) and a feeding port (9), wherein the mixing tube (3) is fixed on the central axis of the extraction tank (2) through a mixing tube support rod (3 b); a nozzle (8) is arranged at one end of the extraction tank (2) in a sealing manner, a blocking cover (1) is arranged at the other end of the extraction tank (2), and the blocking cover (1) is fixed on the sealing cover of the extraction tank (2) through a blocking cover supporting rod (1 a); the nozzle (8) is communicated with a discharge hole of the pump (6) through a circulating pipe (7) provided with a heater (5); the feed inlet of the pump (6) is connected with the other port of the extraction tank (2) through a circulating pipe (7); a feeding port (9) is arranged above the extraction tank (2), and a discharging port (4) is also arranged at the bottom of the extraction tank (2); the extraction tank (2) is also provided with a temperature measuring instrument (11); a water filling port (10) is arranged between the upper part of the extraction tank (2) and the circulating pipe (7); a pressure gauge (12) and a safety valve (13) are also arranged above the extraction tank (2); the feed inlet is provided with a quick-opening type sealing cover; the mixing pipe (3) is an inner spiral pipe body, the right end of the mixing pipe (3) is opposite to the nozzle (8) and is provided with a horn-shaped feeding hole, and the left end of the mixing pipe (3) is provided with a discharging hole; 3-4 supporting rods (1a) of the blocking cover are arranged; 8-12 support rods (3b) of the mixing pipe are respectively arranged at the front section and the rear section of the mixing pipe; the connecting mode of the circulating pipe (7) is flange type or quick-opening type joint connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518072.4A CN106118883B (en) | 2016-06-29 | 2016-06-29 | Camphor tree essential oil leaching device and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518072.4A CN106118883B (en) | 2016-06-29 | 2016-06-29 | Camphor tree essential oil leaching device and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106118883A CN106118883A (en) | 2016-11-16 |
| CN106118883B true CN106118883B (en) | 2020-04-21 |
Family
ID=57468303
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610518072.4A Active CN106118883B (en) | 2016-06-29 | 2016-06-29 | Camphor tree essential oil leaching device and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106118883B (en) |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9101967D0 (en) * | 1991-01-30 | 1991-03-13 | Atomic Energy Authority Uk | Reagent mixing |
| DE19836807A1 (en) * | 1998-08-14 | 2000-02-17 | Basf Ag | Production of aldehyde and or alcohol or amine from olefin involves catalytic hydroformylation in a vertical jet-loop reactor with an internal tube and deflector plate to optimize gas-liquid mixing |
| JP3555557B2 (en) * | 2000-06-16 | 2004-08-18 | 栗田工業株式会社 | Aeration device |
| CN103845923A (en) * | 2012-12-07 | 2014-06-11 | 五峰赤诚生物科技有限公司 | Extraction device |
| CN204543634U (en) * | 2015-04-13 | 2015-08-12 | 福州法莫优科机械科技有限公司 | A kind of outer circulating extracting jar structure |
| CN205061644U (en) * | 2015-08-20 | 2016-03-02 | 陕西立佳环保工程有限公司 | Save reinforceing of medicament and thoughtlessly congeal clarifier |
-
2016
- 2016-06-29 CN CN201610518072.4A patent/CN106118883B/en active Active
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| Publication number | Publication date |
|---|---|
| CN106118883A (en) | 2016-11-16 |
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Application publication date: 20161116 Assignee: Wuzhou Guisheng Agricultural Technology Co.,Ltd. Assignor: GUANGXI ZHUANG AUTONOMOUS REGION FORESTRY Research Institute Contract record no.: X2023980045134 Denomination of invention: A camphor tree essential oil extraction device and its application Granted publication date: 20200421 License type: Common License Record date: 20231101 |
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