CN109304048A - A kind of traditional Chinese medicine extraction device - Google Patents

A kind of traditional Chinese medicine extraction device Download PDF

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Publication number
CN109304048A
CN109304048A CN201811377730.8A CN201811377730A CN109304048A CN 109304048 A CN109304048 A CN 109304048A CN 201811377730 A CN201811377730 A CN 201811377730A CN 109304048 A CN109304048 A CN 109304048A
Authority
CN
China
Prior art keywords
upper cover
air inlet
inlet pipe
tube
rectifying tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811377730.8A
Other languages
Chinese (zh)
Inventor
孟连枝
崔亚婷
朱和凤
朱永喜
宫安东
江红格
解克伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yuzhou Hetongtai Pharmaceutical Co Ltd
Original Assignee
Yuzhou Hetongtai Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yuzhou Hetongtai Pharmaceutical Co Ltd filed Critical Yuzhou Hetongtai Pharmaceutical Co Ltd
Priority to CN201811377730.8A priority Critical patent/CN109304048A/en
Publication of CN109304048A publication Critical patent/CN109304048A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0203Solvent extraction of solids with a supercritical fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0253Fluidised bed of solid materials
    • B01D11/0257Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40Extractive distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D2011/005Co-current extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The present invention relates to a kind of traditional Chinese medicine extraction devices, it includes rectifying tank and upper cover, strainer is provided in rectifying tank, the bottom of rectifying tank is provided with extract port, rectifying tank is internally provided with cavity, air inlet pipe B is connected with above cavity, escape pipe is connected with below cavity, air inlet pipe B and escape pipe are connected separately with gas outlet and the water inlet of steam engine, motor and pressure gauge are provided on upper cover, shaft is connected on the output shaft of motor, agitating paddle is provided on the outside of shaft, air inlet pipe A is connected on upper cover, bead tube and inlet tube, flowmeter A is provided on air inlet pipe A, air inlet pipe A is connected with CO2 generator, the junction of bead tube and upper cover is provided with rectifying valve, extractor is connected on bead tube, the junction of inlet tube and upper cover is provided with liquid feed valve, flowmeter B is provided on inlet tube, feed liquor Pipe is connected with fluid reservoir;The present invention has the advantages that extraction efficiency is high, economizes on resources, process control.

Description

A kind of traditional Chinese medicine extraction device
Technical field
The present invention relates to a kind of Chinese medicine pharmaceutical technology fields, and in particular to a kind of traditional Chinese medicine extraction device.
Background technique
Chinese medical extract purity is high, easy to operate, energy conservation, extraction efficiency is high, with short production cycle, easily finds in natural plants New active constituent, few to lose volatile components or destroy physiological activator, no solvent residue, product quality are high and wide General application;There are some defects in existing traditional Chinese medicine extraction device, existing some traditional Chinese medicine extractions are right after boiling Chinese medicine mostly Ingredient in Chinese medicine extracts, and this extracting mode is easy to some active constituents destroyed in Chinese medicine, causes to have in Chinese medicine The destructurized of ingredient is imitated, the Chinese Herbs after extracting are directly influenced;Therefore, it is necessary to a kind of traditional Chinese medicine extraction devices.
Summary of the invention
The purpose of the invention is to overcome the deficiencies in the prior art, and provide that a kind of extraction efficiency is high, economizes on resources, mistake A kind of controllable traditional Chinese medicine extraction device of journey.
The object of the present invention is achieved like this: a kind of traditional Chinese medicine extraction device, it includes rectifying tank and upper cover, described Rectifying tank and upper cover are threadedly coupled, and strainer is provided in the rectifying tank, is provided with retainer plate above the strainer, institute The retainer plate stated is fixed on rectifying tank mouth, and the bottom of the rectifying tank is provided with extract port, is provided in the extract port Extractor valve, the rectifying tank are internally provided with cavity, and air inlet pipe B, the air inlet pipe B are connected with above the cavity On be provided with intake valve B, escape pipe is connected with below the cavity, air outlet valve is provided on the escape pipe, it is described Air inlet pipe B and escape pipe be connected separately with gas outlet and the water inlet of steam engine, be provided on the upper cover motor and Pressure gauge is connected with shaft on the output shaft of the motor, agitating paddle, the upper envelope is provided on the outside of the shaft Air inlet pipe A, bead tube and inlet tube are connected on head, the junction of the air inlet pipe A and upper cover is provided with intake valve A, Flowmeter A is provided on the air inlet pipe A, the air inlet pipe A is connected with CO2 generator, the bead tube and upper envelope The junction of head is provided with rectifying valve, and extractor, the connection of the inlet tube and upper cover are connected on the bead tube Place is provided with liquid feed valve, and flowmeter B is provided on the inlet tube, and the inlet tube is connected with fluid reservoir.
Pump is provided on the inlet tube.
The strainer is stainless steel filtering net.
Bracket is provided at left and right sides of the rectifying tank.
The beneficial effects of the present invention are: the present invention first smashes Chinese medicine, it is put into strainer, strainer retainer plate is fixed on Rectifying tank mouth, upper cover is covered;Extraction of the invention is divided into two parts: extraction and rectifying;The present invention uses supercritical CO2Fluid Extraction, supercritical CO2Fluid extraction can be close to room temperature (35 ~ 40 DEG C) and CO2It extracts under gas blanket, effectively prevents The oxidation and loss of heat-sensitive substance are stopped;Therefore, the effective component of medicinal plant is remain in extract, and can be height Boiling point, low volatility, the substance being easily pyrolyzed are extracted in the case where being far below its boiling temperature;Since overall process is without organic molten Agent, therefore the absolutely not remaining vehicle substance of extract, to prevent the presence for the object that is harmful to the human body in extraction process and to ring The pollution in border ensure that 100% pure natural property;And CO2Tasteless, odorless, nontoxic, safety is very good, cheap, pure Degree is high, is easy to produce, and can use in production with repetitive cycling, to significantly reduce cost;It is distilled later, it will By pump from being delivered in rectifying tank in fluid reservoir, starting steam engine heats rectifying tank by thermal energy exchange solvent, Medicinal material effective component is dissolved in solvent, extractor is flowed by rectifying tank;Since air inlet pipe B and escape pipe are connected separately with The gas outlet of steam engine and water inlet save water resource it is thereby achieved that water recycles, and flow into the liquid tool of steam engine There is certain temperature, therefore reduces the consuming of thermal energy;The setting of agitating paddle can both be such that medicinal material merges with solvent more evenly, It is heated more evenly, the foam of generation can also be purged;The setting of flowmeter and pressure gauge keeps reaction process more controllable; To sum up, the present invention has the advantages that extraction efficiency is high, economizes on resources, process control.
Detailed description of the invention
Fig. 1 is a kind of main view of traditional Chinese medicine extraction device of the present invention.
Fig. 2 is a kind of top view of traditional Chinese medicine extraction device of the present invention.
Fig. 3 is the structure chart of strainer in a kind of traditional Chinese medicine extraction device of the present invention.
Wherein: 1, upper cover 2, rectifying valve 3, bead tube 4, motor 5, shaft 6, intake valve A 7, air inlet Pipe A 8, flowmeter A 9, CO2 generator 10, bracket 11, rectifying tank 12, extract port 13, extractor valve 14, sky Chamber 15, steam engine 17, air inlet pipe B 18, escape pipe 19, air outlet valve 20, intake valve B 21, is consolidated agitating paddle 16 Surely 22 are enclosed, strainer 23, pressure gauge 24, liquid feed valve 25, inlet tube 26, flowmeter B 27, fluid reservoir 28, is mentioned Take tank.
Specific embodiment
Following further describes the present invention with reference to the drawings.
Embodiment 1
As shown in Figure 1-3, a kind of traditional Chinese medicine extraction device, it includes rectifying tank 11 and upper cover 1, the rectifying tank 11 and upper envelope First 1 is threadedly coupled, and is provided with strainer 22 in the rectifying tank 11, retainer plate 21 is provided with above the strainer 22, described Retainer plate 21 be fixed on 11 mouthfuls of rectifying tank, the bottom of the rectifying tank 11 is provided with extract port 12, the extract port 12 On be provided with extractor valve 13, the rectifying tank 11 is internally provided with cavity 14, and the top of the cavity 14 is connected with air inlet It is provided with intake valve B20 on pipe B17, the air inlet pipe B17, the lower section of the cavity 14 is connected with escape pipe 18, described Escape pipe 18 on be provided with air outlet valve 19, the air inlet pipe B17 and escape pipe 18 are connected separately with the outlet of steam engine 16 Mouthful and water inlet, be provided with motor 4 and pressure gauge 23 on the upper cover 1, be connected with and turn on the output shaft of the motor 4 Axis 5, the outside of the shaft 5 are provided with agitating paddle 15, be connected on the upper cover 1 air inlet pipe A7, bead tube 3 and into The junction of liquid pipe 25, the air inlet pipe A7 and upper cover 1 is provided with intake valve A6, is provided with stream on the air inlet pipe A7 Meter A8, the air inlet pipe A7 are connected with CO2 generator 9, and the junction of the bead tube 3 and upper cover 1 is provided with essence Valve 2 is evaporated, extractor 28 is connected on the bead tube 3, the junction of the inlet tube 25 and upper cover 1 is provided with feed liquor Valve 24 is provided with flowmeter B26 on the inlet tube 25, and the inlet tube 25 is connected with fluid reservoir 27.
The beneficial effects of the present invention are: the present invention first smashes Chinese medicine, it is put into strainer, strainer retainer plate is fixed on Rectifying tank mouth, upper cover is covered;Extraction of the invention is divided into two parts: extraction and rectifying;The present invention uses supercritical CO2Fluid Extraction, effectively prevents the oxidation and loss of heat-sensitive substance;Therefore, remain in extract medicinal plant it is effective at Point, and can be higher boiling, low volatility, the easily substance that is pyrolyzed far below being extracted under its boiling temperature;And CO2Nothing Taste, odorless, nontoxic, safety are very good, cheap, and purity is high is easy to produce, and can make in production with repetitive cycling With to significantly reduce cost;It is distilled later, solvent is opened by pump from being delivered in rectifying tank in fluid reservoir Dynamic steam engine heats rectifying tank by thermal energy exchange, and medicinal material effective component is dissolved in solvent, rectifying tank is passed through Flow into extractor;Since air inlet pipe B and escape pipe are connected separately with gas outlet and the water inlet of steam engine, it is thereby achieved that water Circulation saves water resource, and the liquid for flowing into steam engine has certain temperature, therefore reduces the consuming of thermal energy;It stirs The setting for mixing paddle can both be such that medicinal material merges with solvent more evenly, be heated more evenly, can also carry out the foam of generation clear It removes;The setting of flowmeter and pressure gauge keeps reaction process more controllable;To sum up, the present invention has, extraction efficiency is high, saves money The advantages of source, process control.
Embodiment 2
As shown in Figure 1-3, a kind of traditional Chinese medicine extraction device, it includes rectifying tank 11 and upper cover 1, the rectifying tank 11 and upper envelope First 1 is threadedly coupled, and is provided with strainer 22 in the rectifying tank 11, retainer plate 21 is provided with above the strainer 22, described Retainer plate 21 be fixed on 11 mouthfuls of rectifying tank, the bottom of the rectifying tank 11 is provided with extract port 12, the extract port 12 On be provided with extractor valve 13, the rectifying tank 11 is internally provided with cavity 14, and the top of the cavity 14 is connected with air inlet It is provided with intake valve B20 on pipe B17, the air inlet pipe B17, the lower section of the cavity 14 is connected with escape pipe 18, described Escape pipe 18 on be provided with air outlet valve 19, the air inlet pipe B17 and escape pipe 18 are connected separately with the outlet of steam engine 16 Mouthful and water inlet, be provided with motor 4 and pressure gauge 23 on the upper cover 1, be connected with and turn on the output shaft of the motor 4 Axis 5, the outside of the shaft 5 are provided with agitating paddle 15, be connected on the upper cover 1 air inlet pipe A7, bead tube 3 and into The junction of liquid pipe 25, the air inlet pipe A7 and upper cover 1 is provided with intake valve A6, is provided with stream on the air inlet pipe A7 Meter A8, the air inlet pipe A7 are connected with CO2 generator 9, and the junction of the bead tube 3 and upper cover 1 is provided with essence Valve 2 is evaporated, extractor 28 is connected on the bead tube 3, the junction of the inlet tube 25 and upper cover 1 is provided with feed liquor Valve 24 is provided with flowmeter B26 on the inlet tube 25, and the inlet tube 25 is connected with fluid reservoir 27;The feed liquor Pump is provided on pipe 25;The strainer 22 is stainless steel filtering net;The left and right sides of the rectifying tank 11 is provided with bracket 10。
The beneficial effects of the present invention are: the present invention first smashes Chinese medicine, it is put into strainer, strainer retainer plate is fixed on Rectifying tank mouth, upper cover is covered;Extraction of the invention is divided into two parts: extraction and rectifying;The present invention uses supercritical CO2Fluid Extraction, supercritical CO2Fluid extraction can be close to room temperature (35 ~ 40 DEG C) and CO2It extracts under gas blanket, effectively prevents The oxidation and loss of heat-sensitive substance are stopped;Therefore, the effective component of medicinal plant is remain in extract, and can be height Boiling point, low volatility, the substance being easily pyrolyzed are extracted in the case where being far below its boiling temperature;Since overall process is without organic molten Agent, therefore the absolutely not remaining vehicle substance of extract, to prevent the presence for the object that is harmful to the human body in extraction process and to ring The pollution in border ensure that 100% pure natural property;And CO2Tasteless, odorless, nontoxic, safety is very good, cheap, pure Degree is high, is easy to produce, and can use in production with repetitive cycling, to significantly reduce cost;It is distilled later, it will By pump from being delivered in rectifying tank in fluid reservoir, starting steam engine heats rectifying tank by thermal energy exchange solvent, Medicinal material effective component is dissolved in solvent, extractor is flowed by rectifying tank;Since air inlet pipe B and escape pipe are connected separately with The gas outlet of steam engine and water inlet save water resource it is thereby achieved that water recycles, and flow into the liquid tool of steam engine There is certain temperature, therefore reduces the consuming of thermal energy;The setting of agitating paddle can both be such that medicinal material merges with solvent more evenly, It is heated more evenly, the foam of generation can also be purged;The setting of flowmeter and pressure gauge keeps reaction process more controllable; To sum up, the present invention has the advantages that extraction efficiency is high, economizes on resources, process control.

Claims (4)

1. a kind of traditional Chinese medicine extraction device, it includes rectifying tank and upper cover, it is characterised in that: the rectifying tank and upper cover spiral shell Line connects, and strainer is provided in the rectifying tank, is provided with retainer plate above the strainer, the retainer plate is fixed on Rectifying tank mouth, the bottom of the rectifying tank are provided with extract port, and extractor valve, the rectifying are provided in the extract port Tank is internally provided with cavity, and air inlet pipe B is connected with above the cavity, is provided with intake valve B on the air inlet pipe B, It is connected with escape pipe below the cavity, air outlet valve, the air inlet pipe B and escape pipe are provided on the escape pipe It is connected separately with gas outlet and the water inlet of steam engine, motor and pressure gauge, the motor are provided on the upper cover Output shaft on be connected with shaft, agitating paddle is provided on the outside of the shaft, is connected with air inlet pipe on the upper cover A, the junction of bead tube and inlet tube, the air inlet pipe A and upper cover is provided with intake valve A, sets on the air inlet pipe A It is equipped with flowmeter A, the air inlet pipe A is connected with CO2The junction of generator, the bead tube and upper cover is provided with essence Valve is evaporated, is connected with extractor on the bead tube, the junction of the inlet tube and upper cover is provided with liquid feed valve, described Inlet tube on be provided with flowmeter B, the inlet tube is connected with fluid reservoir.
2. a kind of traditional Chinese medicine extraction device as described in claim 1, it is characterised in that: be provided with pump on the inlet tube.
3. a kind of traditional Chinese medicine extraction device as described in claim 1, it is characterised in that: the strainer is stainless steel filtering net.
4. a kind of traditional Chinese medicine extraction device as described in claim 1, it is characterised in that: be all provided at left and right sides of the rectifying tank It is equipped with bracket.
CN201811377730.8A 2018-11-19 2018-11-19 A kind of traditional Chinese medicine extraction device Pending CN109304048A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811377730.8A CN109304048A (en) 2018-11-19 2018-11-19 A kind of traditional Chinese medicine extraction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811377730.8A CN109304048A (en) 2018-11-19 2018-11-19 A kind of traditional Chinese medicine extraction device

Publications (1)

Publication Number Publication Date
CN109304048A true CN109304048A (en) 2019-02-05

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Application Number Title Priority Date Filing Date
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Country Status (1)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110280042A (en) * 2019-07-17 2019-09-27 梁慧 A kind of Chinese herbal medicine effective ingredients supercritical extract device
CN112915580A (en) * 2021-01-12 2021-06-08 曹洪亮 Supercritical extraction method for effective components of Chinese herbal medicine
CN114931768A (en) * 2022-05-23 2022-08-23 安徽保金药业有限公司 Extraction device for preparing traditional Chinese medicine composition

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1243760A (en) * 1998-07-30 2000-02-09 吕胜一 Multifunctional Rapid Extraction and Fusion Device
CN206486491U (en) * 2017-01-23 2017-09-12 衢州市展宏生物科技有限公司 It is a kind of be used to producing rose isolate and purify device
CN207769268U (en) * 2017-12-28 2018-08-28 江苏卫生健康职业学院 A kind of supercritical extraction reactor
CN207913278U (en) * 2018-02-02 2018-09-28 厦门医学院 A kind of Chinese medicine distillation extraction kettle
CN207941233U (en) * 2017-12-16 2018-10-09 江苏盛信重工有限公司 A kind of supercritical extract reaction kettle
CN108714313A (en) * 2018-07-18 2018-10-30 徐涛 A kind of tea polyphenol extract device

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1243760A (en) * 1998-07-30 2000-02-09 吕胜一 Multifunctional Rapid Extraction and Fusion Device
CN206486491U (en) * 2017-01-23 2017-09-12 衢州市展宏生物科技有限公司 It is a kind of be used to producing rose isolate and purify device
CN207941233U (en) * 2017-12-16 2018-10-09 江苏盛信重工有限公司 A kind of supercritical extract reaction kettle
CN207769268U (en) * 2017-12-28 2018-08-28 江苏卫生健康职业学院 A kind of supercritical extraction reactor
CN207913278U (en) * 2018-02-02 2018-09-28 厦门医学院 A kind of Chinese medicine distillation extraction kettle
CN108714313A (en) * 2018-07-18 2018-10-30 徐涛 A kind of tea polyphenol extract device

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110280042A (en) * 2019-07-17 2019-09-27 梁慧 A kind of Chinese herbal medicine effective ingredients supercritical extract device
CN110280042B (en) * 2019-07-17 2021-09-03 云南裕丰药业有限公司 Supercritical extractor for effective components of Chinese herbal medicine
CN112915580A (en) * 2021-01-12 2021-06-08 曹洪亮 Supercritical extraction method for effective components of Chinese herbal medicine
CN112915580B (en) * 2021-01-12 2022-04-01 深圳太阳生物科技股份有限公司 Supercritical extraction method for effective components of Chinese herbal medicine
CN114931768A (en) * 2022-05-23 2022-08-23 安徽保金药业有限公司 Extraction device for preparing traditional Chinese medicine composition
CN114931768B (en) * 2022-05-23 2023-09-22 安徽保金药业有限公司 Extraction device for preparing traditional Chinese medicine composition

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Application publication date: 20190205

RJ01 Rejection of invention patent application after publication