CN203846006U - Volatile oil extracting, collecting and separating equipment - Google Patents
Volatile oil extracting, collecting and separating equipment Download PDFInfo
- Publication number
- CN203846006U CN203846006U CN201420216158.8U CN201420216158U CN203846006U CN 203846006 U CN203846006 U CN 203846006U CN 201420216158 U CN201420216158 U CN 201420216158U CN 203846006 U CN203846006 U CN 203846006U
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- China
- Prior art keywords
- condenser
- volatile oil
- collecting
- separating device
- separator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 38
- 239000000284 extract Substances 0.000 claims description 14
- 238000000605 extraction Methods 0.000 abstract description 10
- 238000000926 separation method Methods 0.000 abstract description 10
- 239000003814 drug Substances 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 4
- 229940079593 drug Drugs 0.000 abstract 1
- 238000000034 method Methods 0.000 description 11
- 239000000463 material Substances 0.000 description 7
- 238000004821 distillation Methods 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000000194 supercritical-fluid extraction Methods 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 230000003321 amplification Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011982 device technology Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 150000002773 monoterpene derivatives Chemical class 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 239000002547 new drug Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 238000011020 pilot scale process Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model relates to volatile oil extracting, collecting and separating equipment. The equipment is used for collecting and separating volatile oils and is suitable for the fields of chemical industry, medicines, foods and the like. The equipment comprises an extracting tank, a condenser and a collecting and separating device, wherein the upper end of the condenser is connected to the top of the extracting tank through a collecting pipeline; the lower end of the condenser enters the inner layer of the collecting and separating device through an inlet pipeline; the outer layer of the collecting and the separating device is connected with the extracting tank through an outlet pipeline; an air filter is arranged on the collecting and separating device; the air pressure balance of the inner layer and the outer layer is kept to prevent pollution. The equipment disclosed by the utility model is simple and strong in operability and suitable for the extraction and the separation of volatile oils of chemical industry, food industry, medical industry and the like.
Description
Technical field
The utility model relates to a kind of volatile oil and extracts collection separating device, and the equipment for volatile oil collection, separation, is applicable to the fields such as chemical industry, medicine, food.
Background technology
Volatile oil also claims essential oil, is that the class being present in plant materials has volatility, can be with steam distillation, and with the not miscible oily liquids of water.Volatile oil mostly has fragrance and smells taste, and has many-sided biological activity.Volatile oil is wide at vegitabilia's distributed pole, and the plant of using as Chinese medicine just has hundreds of volatile oil that contains.Volatilization oil composition is quite complicated, and it basic composition is terpenoid, aromatics, fatty compounds etc., and ratio that wherein terpene accounts for is maximum and be mainly monoterpene, sesquiterpene and containing oxygen derivative thereof.Volatile oil, as the important substance of Chinese medicine generation effect, is studied it and is extracted with separated significant for developing new drug and the modernization of promotion Chinese materia medica.For a long time, Chinese scholars has been carried out a large amount of research and probes to the extraction of traditional medicine volatile oil with separated, although its extraction and separation method are constantly improving, majority, still in the laboratory study stage, cannot carry out commercial application.
At present, traditional medicine volatile oil extracts and mainly contains distillation method, solvent method, CO2 supercritical fluid extraction.Distillation method is the most frequently used method in the extracting method of volatile oil, easy to operate and safe, and free from environmental pollution, and especially in large production, this method can make the extraction of volatile oil and medicinal material decoction carry out simultaneously, has saved time and the energy, is widely used.But because volatile oil collection tripping device technology level current and that extraction equipment is supporting is low, collect, separation efficiency is low, to part medicinal material, in large production, even cannot collect volatile oil, cause medicinal material utilization ratio low, energy consumption is large, high in cost of production problem, volatile oil extracts, separated equipment has badly influenced the production of Chinese medicine preparation and the quality of product.Solvent method is to adopt the similar principle that mixes, containing volatile medicinal material, use the organic solvent of lower boiling and the fine dissolving volatile oil component of energy as sherwood oil, benzene, ethanol etc., continuous backflow or cold soaking extract, and through distillation or underpressure distillation, remove desolventizing, can obtain rough volatile oil.But the volatile oil that this method obtains is impure more, other oil-soluble impurities is also suggested as resin chlorophyll etc. simultaneously, further refining purification, and widely apply organic solvent in producing, environmental pollution is serious, and in volatile oil, residual organic solvent also makes its security be under suspicion.CO2 supercritical fluid extraction is a kind of novel extraction isolation technique developing rapidly over nearly 20 years, possess and extract that temperature is low, efficiency is high, pollute the plurality of advantages such as little, but it is only suitable for extracting those lipotropys, material that relative molecular mass is little, and the material large for polarity, relative molecular mass is too large, need to add entrainment agent or extract under very high pressure, therefore investment is large, to industrialization, brings certain difficulty and restriction.Make a general survey of traditional method and new technology, most extraction and separation technologies still rests on the conceptual phase in laboratory at present, and the simulation amplification of full scale plant and the use of new technology in industry remain a major issue.Various extractions and isolation technique combine use, with reinforced effects, and strengthening new technology, at volatile oil, to extract applying of separation field be technology trends.
Summary of the invention
In order to overcome above-mentioned defect, the purpose of this utility model is to provide a kind of volatile oil to extract and collects separating device.
To achieve these goals, the utility model adopts following technical scheme:
A kind of volatile oil extracts collects separating device, it comprises extractor, condenser, collection separator, extractor top is connected with upper end of condenser by conduit, and condenser lower end is entered and collected separator internal layer by inlet pipe road, collects separator skin and is connected with extractor by going out pipeline;
On described collection separator, air filter is housed; Keep internal layer and outer air pressure balance, prevent from polluting.
Inlet pipe road and go out pipeline thermometer I, thermometer II are housed respectively.
Describedly go out on pipeline to be provided with valve.
The kind of described condenser is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Schedule of operation:
Pack raw material into extractor, soaking post-heating extracts, water vapor containing volatile oil enters condenser by conduit, phlegma enters collects the separation of separator internal layer, water liquid after separation enters skin, by reflux line, be back to extractor, continuous still battery is extracted after certain hour, from collecting separator lower end, emits volatile oil.
The beneficial effects of the utility model:
1, the utility model has solved traditional medicine volatile oil extraction, a separated difficult problem, simultaneously separated light oil, heavy oil.
2, the utility model volatile oil yield is high, and purity is high, and quality is good.
3, the utility model is applied widely, both can air distillation, and also can underpressure distillation; Both applicable to laboratory lab scale, pilot scale, also applicable to large industrial scaleization, produced.
4, the utility model can on-line cleaning, sterilizing, in production process, can prevent from polluting guaranteed quality.
5, the utility model equipment is simple, workable, and the extraction that is applicable to the industry volatile oil such as chemical industry, food, medical treatment is separated.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with 1 pair of the utility model of accompanying drawing, be described in detail:
A kind of volatile oil extracts collects separating device, it comprises extractor 7, condenser 1, collects separator 6, extractor 7 tops are connected with condenser 1 upper end by conduit 10, condenser 1 lower end is entered and is collected separator 6 internal layers by inlet pipe road 8, collects separator 6 skins and is connected with extractor 7 by going out pipeline 9;
On described collection separator 6, air filter 2 is housed;
Inlet pipe road 8 and go out pipeline 9 thermometer I 4, thermometer II 3 are housed respectively.Can show according to temperature, regulate the flow of condenser cooling water.Keep internal layer and outer air pressure balance, prevent from polluting.
Describedly go out on pipeline 9 to be provided with valve 5.
The kind of described condenser 1 is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Pack raw material into extractor, soaking post-heating extracts, water vapor containing volatile oil enters condenser by conduit, phlegma enters collects the separation of separator internal layer, water liquid after separation enters skin, by reflux line, be back to extractor, continuous still battery is extracted after certain hour, from collecting separator lower end, emits volatile oil.
Claims (3)
1. a volatile oil extracts and collects separating device, it comprises extractor (7), condenser (1), collects separator (6), it is characterized in that: extractor (7) top is connected with condenser (1) upper end by conduit (10), condenser (1) lower end is entered and is collected separator (6) internal layer by inlet pipe road (8), collects separator (6) skin and is connected with extractor (7) by going out pipeline (9);
Air filter (2) is housed on described collection separator (6);
Inlet pipe road (8) and go out pipeline (9) thermometer I (4), thermometer II (3) are housed respectively.
2. volatile oil according to claim 1 extracts and collects separating device, it is characterized in that: described in go out on pipeline (9), to be provided with valve (5).
3. volatile oil according to claim 1 extracts and collects separating device, it is characterized in that: the kind of described condenser (1) is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420216158.8U CN203846006U (en) | 2014-04-30 | 2014-04-30 | Volatile oil extracting, collecting and separating equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420216158.8U CN203846006U (en) | 2014-04-30 | 2014-04-30 | Volatile oil extracting, collecting and separating equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203846006U true CN203846006U (en) | 2014-09-24 |
Family
ID=51559044
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420216158.8U Expired - Lifetime CN203846006U (en) | 2014-04-30 | 2014-04-30 | Volatile oil extracting, collecting and separating equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203846006U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103923748A (en) * | 2014-04-30 | 2014-07-16 | 江西中医药大学 | Volatile oil extracting, collecting and separating device |
-
2014
- 2014-04-30 CN CN201420216158.8U patent/CN203846006U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103923748A (en) * | 2014-04-30 | 2014-07-16 | 江西中医药大学 | Volatile oil extracting, collecting and separating device |
| CN103923748B (en) * | 2014-04-30 | 2016-05-11 | 江西中医药大学 | A kind of volatile oil extracts collects separation equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230118 Address after: Building 2, No. 168, Huangqin Road, Zhihe street, Pengzhou, Chengdu, Sichuan 610000 Patentee after: Sichuan Tianfu fragrant health Technology Research Institute Co.,Ltd. Address before: 330004 No. 818 Xingwan Avenue, Wanli District, Nanchang City, Jiangxi Province Patentee before: JIANGXI University OF TRADITIONAL CHINESE MEDICINE Patentee before: CHENGDU KEER PHARMACEUTICAL Co.,Ltd. |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20140924 |