CN103923748A - Volatile oil extracting, collecting and separating device - Google Patents
Volatile oil extracting, collecting and separating device Download PDFInfo
- Publication number
- CN103923748A CN103923748A CN201410178436.XA CN201410178436A CN103923748A CN 103923748 A CN103923748 A CN 103923748A CN 201410178436 A CN201410178436 A CN 201410178436A CN 103923748 A CN103923748 A CN 103923748A
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- volatile oil
- condenser
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- separating device
- separating
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 39
- 239000000284 extract Substances 0.000 claims description 14
- 238000000926 separation method Methods 0.000 abstract description 11
- 238000000605 extraction Methods 0.000 abstract description 10
- 239000003814 drug Substances 0.000 abstract description 9
- 235000013305 food Nutrition 0.000 abstract description 4
- 238000003889 chemical engineering Methods 0.000 abstract 2
- 229940079593 drug Drugs 0.000 abstract 2
- 238000000034 method Methods 0.000 description 11
- 239000000463 material Substances 0.000 description 7
- 238000004821 distillation Methods 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000000194 supercritical-fluid extraction Methods 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 230000003321 amplification Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011982 device technology Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 150000002773 monoterpene derivatives Chemical class 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 239000002547 new drug Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 238000011020 pilot scale process Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to a volatile oil extracting, collecting and separating device which is a device for collecting and separating volatile oil, and applicable to the fields of chemical engineering, medicines, foods and the like. The volatile oil extracting, collecting and separating device comprises an extracting tank, a condenser and a collecting and separating facility, wherein the top of the extracting tank is collected with the upper end of the condenser by virtue of a collecting pipeline, the lower end of the condenser enters the inner layer of the collecting and separating facility by virtue of an inlet pipeline, and the outer layer of the collecting and separating facility is connected with the extracting tank through an outlet pipeline; the collecting and separating facility is provided with an air filter; the air pressure balance between the inner layer and the outer layer is kept so as to prevent pollution. The device disclosed by the invention is simple, strong in maneuverability, and applicable to the extraction and separation of volatile oil in the fields of chemical engineering, foods, medicines, and the like.
Description
Technical field
The present invention relates to a kind of volatile oil and extract collection separating device, the equipment for volatile oil collection, separation, is applicable to the fields such as chemical industry, medicine, food.
Background technology
Volatile oil also claims essential oil, is that the class being present in plant materials has volatility, can be with steam distillation, and with the not miscible oily liquids of water.Volatile oil mostly has fragrance and smells taste, and has many-sided biological activity.Volatile oil is wide at vegitabilia's distributed pole, and the plant of using as Chinese medicine just has hundreds of volatile oil that contains.Volatilization oil composition is quite complicated, and it basic composition is terpenoid, aromatics, fatty compounds etc., and ratio that wherein terpene accounts for is maximum and be mainly monoterpene, sesquiterpene and containing oxygen derivative thereof.Volatile oil, as the important substance of Chinese medicine generation effect, is studied it and is extracted with separated significant for developing new drug and the modernization of promotion Chinese materia medica.For a long time, Chinese scholars has been carried out a large amount of research and probes to the extraction of traditional medicine volatile oil with separated, although its extraction and separation method are constantly improving, majority, still in the laboratory study stage, cannot carry out commercial application.
At present, traditional medicine volatile oil extracts and mainly contains distillation method, solvent method, CO2 supercritical fluid extraction.Distillation method is the most frequently used method in the extracting method of volatile oil, easy to operate and safe, and free from environmental pollution, and especially in large production, this method can make the extraction of volatile oil and medicinal material decoction carry out simultaneously, has saved time and the energy, is widely used.But because volatile oil collection tripping device technology level current and that extraction equipment is supporting is low, collect, separation efficiency is low, to part medicinal material, in large production, even cannot collect volatile oil, cause medicinal material utilization ratio low, energy consumption is large, high in cost of production problem, volatile oil extracts, separated equipment has badly influenced the production of Chinese medicine preparation and the quality of product.Solvent method is to adopt the similar principle that mixes, containing volatile medicinal material, use the organic solvent of lower boiling and the fine dissolving volatile oil component of energy as sherwood oil, benzene, ethanol etc., continuous backflow or cold soaking extract, and through distillation or underpressure distillation, remove desolventizing, can obtain rough volatile oil.But the volatile oil that this method obtains is impure more, other oil-soluble impurities is also suggested as resin chlorophyll etc. simultaneously, further refining purification, and widely apply organic solvent in producing, environmental pollution is serious, and in volatile oil, residual organic solvent also makes its security be under suspicion.CO2 supercritical fluid extraction is a kind of novel extraction isolation technique developing rapidly over nearly 20 years, possess and extract that temperature is low, efficiency is high, pollute the plurality of advantages such as little, but it is only suitable for extracting those lipotropys, material that relative molecular mass is little, and the material large for polarity, relative molecular mass is too large, need to add entrainment agent or extract under very high pressure, therefore investment is large, to industrialization, brings certain difficulty and restriction.Make a general survey of traditional method and new technology, most extraction and separation technologies still rests on the conceptual phase in laboratory at present, and the simulation amplification of full scale plant and the use of new technology in industry remain a major issue.Various extractions and isolation technique combine use, with reinforced effects, and strengthening new technology, at volatile oil, to extract applying of separation field be technology trends.
Summary of the invention
In order to overcome above-mentioned defect, the object of the present invention is to provide a kind of volatile oil to extract and collect separating device.
To achieve these goals, the present invention adopts following technical scheme:
A kind of volatile oil extracts collects separating device, it comprises extractor, condenser, collection separator, extractor top is connected with upper end of condenser by conduit, and condenser lower end is entered and collected separator internal layer by inlet pipe road, collects separator skin and is connected with extractor by going out pipeline;
On described collection separator, air filter is housed; Keep internal layer and outer air pressure balance, prevent from polluting.
Inlet pipe road and go out pipeline thermometer I, thermometer II are housed respectively.
Describedly go out on pipeline to be provided with valve.
The kind of described condenser is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Schedule of operation:
Pack raw material into extractor, soaking post-heating extracts, water vapor containing volatile oil enters condenser by conduit, phlegma enters collects the separation of separator internal layer, water liquid after separation enters skin, by reflux line, be back to extractor, continuous still battery is extracted after certain hour, from collecting separator lower end, emits volatile oil.
Beneficial effect of the present invention:
1, the invention solves a difficult problem for traditional medicine volatile oil extraction, separation, simultaneously separated light oil, heavy oil.
2, volatile oil yield of the present invention is high, and purity is high, and quality is good.
3, the present invention is applied widely, both can air distillation, and also can underpressure distillation; Both applicable to laboratory lab scale, pilot scale, also applicable to large industrial scaleization, produced.
4, the present invention can on-line cleaning, sterilizing, in production process, can prevent from polluting guaranteed quality.
5, present device is simple, workable, and the extraction that is applicable to the industry volatile oil such as chemical industry, food, medical treatment is separated.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Embodiment
Below in conjunction with accompanying drawing 1, describe the present invention:
A kind of volatile oil extracts collects separating device, it comprises extractor 7, condenser 1, collects separator 6, extractor 7 tops are connected with condenser 1 upper end by conduit 10, condenser 1 lower end is entered and is collected separator 6 internal layers by inlet pipe road 8, collects separator 6 skins and is connected with extractor 7 by going out pipeline 9;
On described collection separator 6, air filter 2 is housed;
Inlet pipe road 8 and go out pipeline 9 thermometer I 4, thermometer II 3 are housed respectively.Can show according to temperature, regulate the flow of condenser cooling water.Keep internal layer and outer air pressure balance, prevent from polluting.
Describedly go out on pipeline 9 to be provided with valve 5.
The kind of described condenser 1 is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Pack raw material into extractor, soaking post-heating extracts, water vapor containing volatile oil enters condenser by conduit, phlegma enters collects the separation of separator internal layer, water liquid after separation enters skin, by reflux line, be back to extractor, continuous still battery is extracted after certain hour, from collecting separator lower end, emits volatile oil.
Claims (3)
1. a volatile oil extracts and collects separating device, it comprises extractor (7), condenser (1), collects separator (6), it is characterized in that: extractor (7) top is connected with condenser (1) upper end by conduit (10), condenser (1) lower end is entered and is collected separator (6) internal layer by inlet pipe road (8), collects separator (6) skin and is connected with extractor (7) by going out pipeline (9);
Air filter (2) is housed on described collection separator (6);
Inlet pipe road (8) and go out pipeline (9) thermometer I (4), thermometer II (3) are housed respectively.
2. volatile oil according to claim 1 extracts and collects separating device, it is characterized in that: described in go out on pipeline (9), to be provided with valve (5).
3. volatile oil according to claim 1 extracts and collects separating device, it is characterized in that: the kind of described condenser (1) is a kind of in shell-and tube condenser, plate-type condenser, spiral condenser.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410178436.XA CN103923748B (en) | 2014-04-30 | 2014-04-30 | A kind of volatile oil extracts collects separation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410178436.XA CN103923748B (en) | 2014-04-30 | 2014-04-30 | A kind of volatile oil extracts collects separation equipment |
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| Publication Number | Publication Date |
|---|---|
| CN103923748A true CN103923748A (en) | 2014-07-16 |
| CN103923748B CN103923748B (en) | 2016-05-11 |
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| CN201410178436.XA Active CN103923748B (en) | 2014-04-30 | 2014-04-30 | A kind of volatile oil extracts collects separation equipment |
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| CN (1) | CN103923748B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104789365A (en) * | 2015-04-28 | 2015-07-22 | 浙江温兄机械阀业有限公司 | Extraction equipment for light (heavy) volatile oil |
| CN105159074A (en) * | 2015-08-19 | 2015-12-16 | 四川九渊医药科技有限公司 | Optimization method for large-scale volatile oil extraction from medicinal materials |
| CN106054948A (en) * | 2016-05-25 | 2016-10-26 | 江苏康缘药业股份有限公司 | Volatile oil stable collection device in artemisia carvifolia extraction process and control method thereof |
| CN106110709A (en) * | 2016-06-18 | 2016-11-16 | 沈永贤 | A kind of Novel oil-water separator |
| CN106350227A (en) * | 2016-09-14 | 2017-01-25 | 梧州市西江林产化工技术设备研究所 | Energy-saving high-efficiency adjustable temperature plant essential oil distillation kettle and distillation process thereof |
| CN106398874A (en) * | 2016-12-16 | 2017-02-15 | 江西中医药大学 | Volatile oil multi-effect separation device |
| CN106902541A (en) * | 2017-04-25 | 2017-06-30 | 山东省中医药研究院 | A kind of collection device of Chinese medicine volatile materials |
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| CN2221441Y (en) * | 1995-06-12 | 1996-03-06 | 周希勤 | External-heating multi-stage multi-energy extraction device |
| CN202322781U (en) * | 2011-11-28 | 2012-07-11 | 湖北中烟工业有限责任公司 | Extracting system for volatile oil |
| CN202359093U (en) * | 2011-12-09 | 2012-08-01 | 广西圣保堂药业有限公司 | Plant essential oil extraction device |
| CN203096030U (en) * | 2013-02-27 | 2013-07-31 | 湖北中烟工业有限责任公司 | Volatile oil extraction separator |
| CN203846006U (en) * | 2014-04-30 | 2014-09-24 | 江西中医药大学 | Volatile oil extracting, collecting and separating equipment |
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2014
- 2014-04-30 CN CN201410178436.XA patent/CN103923748B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN2221441Y (en) * | 1995-06-12 | 1996-03-06 | 周希勤 | External-heating multi-stage multi-energy extraction device |
| CN202322781U (en) * | 2011-11-28 | 2012-07-11 | 湖北中烟工业有限责任公司 | Extracting system for volatile oil |
| CN202359093U (en) * | 2011-12-09 | 2012-08-01 | 广西圣保堂药业有限公司 | Plant essential oil extraction device |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104789365A (en) * | 2015-04-28 | 2015-07-22 | 浙江温兄机械阀业有限公司 | Extraction equipment for light (heavy) volatile oil |
| CN104789365B (en) * | 2015-04-28 | 2018-01-02 | 浙江温兄机械阀业有限公司 | A kind of extraction equipment of light/heavy volatile oil |
| CN105159074A (en) * | 2015-08-19 | 2015-12-16 | 四川九渊医药科技有限公司 | Optimization method for large-scale volatile oil extraction from medicinal materials |
| CN105159074B (en) * | 2015-08-19 | 2017-08-29 | 四川九渊医药科技有限公司 | The optimization method of volatile oil in a kind of extensive extraction medicinal material |
| CN106054948A (en) * | 2016-05-25 | 2016-10-26 | 江苏康缘药业股份有限公司 | Volatile oil stable collection device in artemisia carvifolia extraction process and control method thereof |
| CN106110709A (en) * | 2016-06-18 | 2016-11-16 | 沈永贤 | A kind of Novel oil-water separator |
| CN106350227A (en) * | 2016-09-14 | 2017-01-25 | 梧州市西江林产化工技术设备研究所 | Energy-saving high-efficiency adjustable temperature plant essential oil distillation kettle and distillation process thereof |
| CN106398874A (en) * | 2016-12-16 | 2017-02-15 | 江西中医药大学 | Volatile oil multi-effect separation device |
| CN106902541A (en) * | 2017-04-25 | 2017-06-30 | 山东省中医药研究院 | A kind of collection device of Chinese medicine volatile materials |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103923748B (en) | 2016-05-11 |
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Effective date of registration: 20210315 Address after: 330004 No. 818 Xingwan Avenue, Wanli District, Nanchang City, Jiangxi Province Patentee after: JIANGXI University OF TRADITIONAL CHINESE MEDICINE Address before: 330004 No. 818 Xingwan Avenue, Wanli District, Nanchang City, Jiangxi Province Patentee before: JIANGXI University OF TRADITIONAL CHINESE MEDICINE Patentee before: CHENGDU KEER PHARMACEUTICAL Co.,Ltd. |
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Effective date of registration: 20211025 Address after: 330000 floors 1-3, building 1, xinqizhou public R & D center, innovation city of traditional Chinese medicine, directly managed District, Ganjiang new area, Nanchang City, Jiangxi Province Patentee after: Ganjiang New Area Zhiyao Shanhe Technology Co.,Ltd. Address before: 330000 inside Jiangxi College of traditional Chinese medicine, No. 56, Yangming Road, Donghu District, Nanchang City, Jiangxi Province Patentee before: Jiangxi Huizhong Asset Management Co.,Ltd. |
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Application publication date: 20140716 Assignee: JIANGXI HBKHPHARM PHARMACEUTICAL EQUIPMENT CO.,LTD. Assignor: Ganjiang New Area Zhiyao Shanhe Technology Co.,Ltd. Contract record no.: X2022980022998 Denomination of invention: A volatile oil extraction, collection and separation equipment Granted publication date: 20160511 License type: Common License Record date: 20221202 |
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