CN106118878B

CN106118878B - A kind of perfume base with fruity and the essence containing the perfume base and its application

Info

Publication number: CN106118878B
Application number: CN201610630981.7A
Authority: CN
Inventors: 叶静
Original assignee: Guangzhou Apple Flavor Co
Current assignee: Guangzhou Apple Flavor Co
Priority date: 2016-08-04
Filing date: 2016-08-04
Publication date: 2017-06-30
Anticipated expiration: 2036-08-04
Also published as: CN106118878A

Abstract

The present invention provides a kind of perfume base with fruity, the natural fruity of the fresh and tender succulence that berry fruits are built jointly can be embodied, existing Kiwi berry, raspberry, gooseberry it is fragrant and sweet, have the fruity notes of tropical fruit (tree) guava, Kiwi berry etc. again, with have an effect strong, sweet fruity thoroughly and without acrid odors；The perfume base is added in essence, essence can be allowed to send abundant, complicated, full fruity notes thoroughly, the fruity head perfume atmosphere that sweet, natural sense is strong, have an effect strong thoroughly is built, and can well be concocted with the fruity in essence and fragrance of a flower raw material, build the abundant fruity fragrance of a flower atmosphere of stereovision；Essence containing the perfume base can be used in the product for need fruits note, such as perfume, shower cream, shampoo.

Description

A kind of perfume base with fruity and the essence containing the perfume base and its application

Technical field

The present invention relates to spices science and technology field, more particularly, to a kind of perfume base with fruity and contain the perfume The essence of base and its application.

Background technology

In many perfume, head perfume has the fruity of complexity, can build a kind of sentiment of foreign country's fruity.In perfume What is be most widely used is exactly berry note, such as grape, Kiwi berry, raspberry, gooseberry, cowberry, fruit mulberry, fig, pomegranate, poplar Peach, sapodilla, papaya, guava, Portugal, passionflower etc..Perfume is made up of water, alcohol, essence substantially.And perfume base, then it is The basis of essence main body fragrant, therefore also referred to as basic note agent or type-odor.Usual perfume base is not directly used in perfumed products, is only made It is the fragrance key component of essence, so perfume base is the basis for preparing essence.

Generally, the originals such as compounding acetic isoborneol ester, verdox, linalool, first position terpinol are contained in perfume base Material, this several raw material can strengthen the fragrance of perfume base.However, this several raw material also brings along pungent smell, to the perfume (or spice) of perfume base Taste brings detrimental effect.Accordingly, it would be desirable to it is a kind of with have an effect strong, sweet fruity thoroughly and without the perfume base of acrid odors.

The content of the invention

The present invention is to overcome at least one defect described in above-mentioned prior art, there is provided a kind of perfume base with fruity, energy Embody berry fruits jointly build fresh and tender succulence natural fruity, existing Kiwi berry, raspberry, gooseberry it is fragrant and sweet, have heat again Fruity notes with fruit guava, Kiwi berry etc., its fruity have an effect thoroughly it is strong, sweet and without acrid odors.

The present invention also aims to provide a kind of essence containing the perfume base, wherein the perfume base can with essence in Raw material reconciles well, builds berry and tropical fruit (tree) class note.

In addition, the present invention also aims to provide a kind of essence containing the perfume base in perfume, shower cream, shampoo Etc. the application in the product for needing fruits note.

To realize the purpose of the present invention, technical program of the present invention lies in employing a kind of perfume base with fruity, it is special Levy and be, by weight percentage by isoamyl acetate 0.05-0.08%, Leaf Acetate 0.1-0.3%, rose oxide 0.01- 0.05%, ligustral 0.1-0.5%, vertenex 4-7%, compounding acetic isoborneol ester 0.04-0.08%, Damascenone 0.3-0.6%, benzyl acetate 1-2%, vanillyl alcohol 2-4.5%, phenethyl acetate 0.1-0.2%, Hai Feng Quan " 0.1-0.4%, purple sieve in second position Blue ketone 0.45-0.6%, third nonalactone 0.6-0.9%, lilial 1-1.8%, indoles flower 0.1-0.4%, MDJ 6-8%, alpha-amyl cinnamic aldehyde 5-6%, salicylic acid benzyl ester 1-2%, astrotone 1-2%, orange oil 1-3%, fourth damascone 0.01- 0.015%, hexyl acetate 0.6-0.8%, 2,6- dimethyl enanthol 0.1-0.4%, leaf-alcohol 0.02-0.05%, linalool 10-18%, second Sour o-tert-butyl cyclohexyl 7-9%, first position terpinol 1.5-3.4%, terpinyl acetate 3-5%, geranyl acetate 0.1-0.4% are fragrant Leaf-alcohol 8-10%, second position damascone 0.1-0.3%, benzyl carbinol 0.7-0.8%, eugenol methyl ether 0.02-0.04%, phenylpropanol 0.04- 0.1%, eugenol 0.4-0.5%, vertofix coeur 6-7%, first hexyl cinnamic aldehyde 1-2%, third undecalactone 0.6-1.8%, folium eucalypti Plain 0.4-0.6%, D- limonene 5-6%, cyclic ethers 0.3-0.5%, appropriate two polypropylene glycols composition.The perfume base has the fruity of complexity, The slight delicate fragrance of berry sample, and the fragrance sensation of a kind of lichee, Kiwi berry and raspberry can be aroused, needs can be widely used in The essence of berry and tropical fruit (tree) class note.The perfume base can embody the natural fruit of the fresh and tender succulence that berry fruits are built jointly Perfume (or spice), existing Kiwi berry, raspberry, gooseberry it is fragrant and sweet, have the fruity notes of tropical fruit (tree) guava, Kiwi berry etc. again.And guava, The explosive sweet sense of the tropical fruit (tree)s such as Kiwi berry can modify compounding acetic isoborneol ester, verdox, linalool, first The pungent note that the raw material of position terpinol etc. is carried, so as to make the fragrance of perfume base more sweet, and remains strong and has an effect thoroughly.With The existing also enlightening fruit base with fruity is compared, the fruit flavor more horn of plenty of perfume base of the invention.

The preparation method of the perfume base is that each component is well mixed prepared.The hybrid mode is preferably stirring.

Additionally, technical program of the present invention also lies in employing a kind of essence containing the perfume base.

Specifically, in the essence, the content of perfume base is 0.01-10%.

For certain form of essence, the content of perfume base is excessive, may override the original fragrance of essence.Preferably, In the essence, the content of perfume base is 0.01 ~ 1%.

Preferably, in the essence, the content of perfume base is 0.05 ~ 0.25%.

Preferably, the essence is by weight percentage by two polypropylene glycols 46.335%, hexanol 0.005%, leaf-alcohol 0.050%, Vanillyl alcohol 0.050%, geraniol 1.250%, linalool 4.800%, methyl decenol 0.130%, ethyl linalool 1.500%, dihydro Myrcenol 2.500%, nerolidol 2.000%, rose oxide 0.100%, helional 0.100%, citral 0.040%, glossy privet Aldehyde 0.010%, first hexyl cinnamic aldehyde 3.000%, benzaldehyde 0.010%, raspberry ketone 0.200%, B position violet ketone 0.850% is all Road ketone 0.010%, ambrotone 6.000%, dihydro first position damascone 0.015%, Damascenone 0.030%, phenyl acetaldehyde dimethyl acetal 0.070%, Leaf Acetate 0.100%, hexyl acetate 0.300%, acetic acid dimethylamino benzylidene base ester 0.500%, allyl heptanoate 0.350%, the own ester 0.800% of salicylic acid, geranyl acetate 0.150%, Vanillin acetate 0.070%, verdox 2.600%, allyl cyclohexyl propionate 0.040%, neryl acetate 0.020%, benzyl acetate 0.900%, dihydro jasmone acid first Ester 14.500%, bergamio 2.800%, ethyl acetoacetate 0.060%, acetyl isoeugenol 0.250%, gamma decalactone 0.070%, third undecalactone 0.450%, jasmonyl 0.600%, jasmine pyrans 0.050%, astrotone 2.800%, heliotropin 0.020%, glacial acetic acid 0.010%, santal 208 3.150%, santal 803 0.030% synthesizes oak moss 0.200%, white grapefruit oil 0.200%, perfume base 0.15%, Java santal 0.060%, Florol 1.300% is constituted.Perfume base is added in essence can allow essence to be sent out thoroughly Go out abundant, complicated, full fruity notes, build the fruity head perfume atmosphere that sweet, natural sense is strong, have an effect strong thoroughly, and can and it is white The fruity such as grapefruit oil, allyl cyclohexyl propionate, benzyl acetate, MDJ and fragrance of a flower raw material are concocted well, Build a kind of abundant fruity-fragrance of a flower atmosphere of stereovision.

Technical program of the present invention also lies in providing application of the perfume base in essence is prepared.

In addition, technical program of the present invention also lies in the offer essence in the product for needing fruits note is prepared Using.

Preferably, the product for needing fruits note is selected from perfume, shower cream, shampoo etc..

The present invention has the advantages that：

The perfume base with fruity that the present invention is provided, can embody the natural fruit of the fresh and tender succulence that berry fruits are built jointly Perfume (or spice), existing Kiwi berry, raspberry, gooseberry it is fragrant and sweet, have the fruity notes of tropical fruit (tree) guava, Kiwi berry etc. again, with thoroughly hair Strong, the sweet fruity of power and without acrid odors；The perfume base is added in essence, essence can be allowed to send thoroughly abundant, complicated, full Full fruity notes, build the fruity head perfume atmosphere that sweet, natural sense is strong, have an effect strong thoroughly, and can be with the fruity and flower in essence Perfume material is concocted well, builds the abundant fruity-fragrance of a flower atmosphere of stereovision；Essence containing the perfume base can be used to need In the product of fruits note, such as perfume, shower cream, shampoo.

Specific embodiment

With reference to specific embodiment, the present invention is further illustrated, but specific embodiment is not made to the present invention Any restriction.Unless stated otherwise, reagent involved in embodiment, method are reagent and method commonly used in the art.

Embodiment 1

Perfume base 1 is prepared using the method for stirring, its formula is as follows：

。

Embodiment 2

Perfume base 2 is prepared using the method for stirring, its formula is as follows：

。

Embodiment 3

Perfume base 3 is prepared using the method for stirring, its formula is as follows：

。

Sensory evaluation：

Take a set of " 40 points " the scorings method of inspection in spices and essence industry：Fragrance is carried out to a spices or essence to comment Fixed, " full marks " are 40 points, and " pure " is 39.1-40 points, and " purer " is 36.0-39.0 points, and " can with " be 32.0-35.9 points, " fine " is 28.0-31.9 points, and " qualifying " is 24.0-27.9 points, and " failing " is less than 24.0 points.

Tissue 5 perfumers and 2 comment fragrant Shi Zuowei to comment fragrant member to take the perfume base and existing enlightening fruit base of embodiment 1-3 Above-mentioned " 40 points " sensory evaluation method is evaluated and is recorded their descriptions to fragrance, and the result for drawing is as follows：

。

According to commenting scoring of the fragrant member to embodiment 1-3, the scoring of the scoring of embodiment 1-3 enlightening fruit base substantially than buying Height, and the scoring of embodiment 1 is higher than embodiment 2 and 3.

In addition, according to sensory experience of the fragrant member to embodiment 1-3 is commented, it is common that embodiment 1-3 can embody berry fruits Build fresh and tender succulence natural fruity, it is existing have Kiwi berry, raspberry, gooseberry it is fragrant and sweet, have tropical fruit (tree) guava, macaque again The fruity notes of peach etc., with having an effect strong, sweet fruity thoroughly and the basic effect without acrid odors, and embodiment 1 The taste of complicated tropical fruit (tree) is sent out the most thoroughly, does not have pungent taste.And the enlightening fruit base bought has complicated fruity, berry The fragrance of sample and slight herbal, and with pungent fragrance.

Application Example 1

The perfume base 1 of embodiment 1 is added in essence, is formulated as follows：

Material name	Consumption %
		Two polypropylene glycols	46.435
Hexanol	0.005
		Leaf-alcohol	0.050
Vanillyl alcohol	0.050
		Geraniol	1.250
Linalool	4.800
		Methyl decenol	0.130
Ethyl linalool	1.500
		Dihydromyrcenol	2.500
Nerolidol	2.000
		Rose oxide	0.100
Helional	0.100
		Citral	0.040
Ligustral	0.010
		First position hexyl cinnamic aldehyde	3.000
Benzaldehyde	0.010
		Raspberry ketone	0.200
B position violet ketone	0.850
		All road ketone	0.010
Ambrotone	6.000
		Dihydro first position damascone	0.015
Damascenone	0.030
		Phenyl acetaldehyde dimethyl acetal	0.070
Leaf Acetate	0.100
		Hexyl acetate	0.300
Acetic acid dimethylamino benzylidene base ester	0.500
		Allyl heptanoate	0.350
The own ester of salicylic acid	0.800
		Geranyl acetate	0.150
Vanillin acetate	0.070
		Verdox	2.600
Allyl cyclohexyl propionate	0.040
		Neryl acetate	0.020
Benzyl acetate	0.900
		MDJ	14.500
Bergamio	2.800
		Ethyl acetoacetate	0.060
Acetyl isoeugenol	0.250
		Gamma decalactone	0.070
Third undecalactone	0.450
		Jasmonyl	0.600
Jasmine pyrans	0.050
		Astrotone	2.800
Heliotropin	0.020
		Glacial acetic acid	0.010
Santal 208	3.150
		Santal 803	0.030
Synthesis oak moss	0.200
		White grapefruit oil	0.200
Java santal	0.060
		Florol	1.300
Perfume base 1	0.050
		Summation	100.000

Application Example 2

The perfume base 1 of embodiment 1 is added in essence, the consumption of perfume base 1 is 0.150%, two polypropylene glycol consumptions are 46.335%, remaining raw material and consumption are identical with Application Example 1.

Application Example 3

The perfume base 1 of embodiment 1 is added in essence, the consumption of perfume base 1 is 0.250%, two polypropylene glycol consumptions are 46.235%, remaining raw material and consumption are identical with Application Example 1.

Comparative example 1

The perfume base 1 of embodiment 1 is added without in essence, two polypropylene glycol consumptions are 46.335%, remaining raw material and consumption with Application Example 1 is identical.

Comparative example 2

The enlightening fruit base that will be bought is added in essence, and enlightening fruit base consumption is 0.15%, and two polypropylene glycol consumptions are 46.335%, Remaining raw material and consumption are identical with Application Example 1.

That the fragrant hair thoroughly of the head in perfumed applications experiment is stated with digital 0-5 goes out abundant, complicated, full fruity notes, The intensity for building the fruity head perfume atmosphere that sweet, natural sense is strong, have an effect strong thoroughly is stated, and 0=does not exist, and 1=can just smell, 2=is weak, and 3=is medium, and 4=is strong, and 5=is very strong.Application Example 1-3, essence obtained in comparative example 1-2 are added separately to same nature And in the shower cream base-material of identical amount, addition is 0.5%, contained with same container, sticked corresponding with the essence for being added Label.

By perfumer and commenting fragrant Shi Zuowei to comment fragrant member to evaluate Application Example 1-3 and comparative example 1-2, draw following Evaluation result：

。

By above-mentioned evaluation result, it is known that the perfume base of same amount of embodiment 1 and the enlightening fruit base bought are added To in essence, it will be apparent that, add the comparative example 2 of enlightening fruit base that the Application Example of the perfume base of embodiment 1 is bought than addition more Essence can be allowed to send abundant, complicated, full fruity notes thoroughly, build the fruity head perfume atmosphere that sweet, natural sense is strong, have an effect strong thoroughly Enclose, and can and fruity and the fragrance of a flower raw material such as white grapefruit oil, allyl cyclohexyl propionate, benzyl acetate, MDJ Blending well, builds the abundant fruity-fragrance of a flower atmosphere of stereovision.

Obviously, the above embodiment of the present invention is only intended to clearly illustrate example of the present invention, and is not right The restriction of embodiments of the present invention.For those of ordinary skill in the field, may be used also on the basis of the above description To make other changes in different forms.There is no need and unable to be exhaustive to all of implementation method.It is all this Any modification, equivalent and improvement made within the spirit and principle of invention etc., should be included in the claims in the present invention Protection domain within.

Claims

1. a kind of perfume base with fruity, it is characterised in that by weight percentage by isoamyl acetate 0.05-0.08%, acetic acid leaf Alcohol ester 0.1-0.3%, rose oxide 0.01-0.05%, ligustral 0.1-0.5%, vertenex 4-7%, the different dragon of acetic acid Brain ester 0.04-0.08%, Damascenone 0.3-0.6%, benzyl acetate 1-2%, vanillyl alcohol 2-4.5%, phenethyl acetate 0.1-0.2%, Hai Feng Quan " 0.1-0.4%, B position violet ketone 0.45-0.6%, third nonalactone 0.6-0.9%, lilial 1-1.8%, indoles flower 0.1-0.4%, MDJ 6-8%, alpha-amyl cinnamic aldehyde 5-6%, salicylic acid benzyl ester 1-2%, astrotone 1-2%, orange oil 1-3%, fourth position damascone 0.01-0.015%, hexyl acetate 0.6-0.8%, 2,6- dimethyl enanthol 0.1-0.4%, leaf-alcohol 0.02- 0.05%, linalool 10-18%, verdox 7-9%, first position terpinol 1.5-3.4%, terpinyl acetate 3-5%, Geranyl acetate 0.1-0.4%, geraniol 8-10%, second position damascone 0.1-0.3%, benzyl carbinol 0.7-0.8%, eugenol methyl ether 0.02-0.04%, phenylpropanol 0.04-0.1%, eugenol 0.4-0.5%, vertofix coeur 6-7%, first position hexyl cinnamic aldehyde 1-2%, third Position undecalactone 0.6-1.8%, Cineole 0.4-0.6%, D- limonene 5-6%, cyclic ethers 0.3-0.5%, appropriate two polypropylene glycols group Into.

2. a kind of essence containing perfume base according to claim 1.

3. essence according to claim 2, it is characterised in that in the essence, the content of perfume base is 0.01-10%.

4. essence according to claim 3, it is characterised in that in the essence, the content of perfume base is 0.01 ~ 1%.

5. essence according to claim 4, it is characterised in that in the essence, the content of perfume base is 0.05 ~ 0.25%.

6. essence according to claim 2, it is characterised in that by weight percentage by two polypropylene glycols 46.335%, oneself Alcohol 0.005%, leaf-alcohol 0.050%, vanillyl alcohol 0.050%, geraniol 1.250%, linalool 4.800%, methyl decenol 0.130%, Ethyl linalool 1.500%, dihydromyrcenol 2.500%, nerolidol 2.000%, rose oxide 0.100%, helional 0.100%, citral 0.040%, ligustral 0.010%, first hexyl cinnamic aldehyde 3.000%, benzaldehyde 0.010%, raspberry ketone 0.200%, B position violet ketone 0.850%, all road ketone 0.010%, ambrotone 6.000%, dihydro first position damascone 0.015%, Tujue Ketenes 0.030%, phenyl acetaldehyde dimethyl acetal 0.070%, Leaf Acetate 0.100%, hexyl acetate 0.300%, acetic acid dimethylamino benzylidene base Ester 0.500%, allyl heptanoate 0.350%, the own ester 0.800% of salicylic acid, geranyl acetate 0.150%, Vanillin acetate 0.070%, second Sour o-tert-butyl cyclohexyl 2.600%, allyl cyclohexyl propionate 0.040%, neryl acetate 0.020%, benzyl acetate 0.900%, MDJ 14.500%, bergamio 2.800%, ethyl acetoacetate 0.060%, Sucrose Acetate is fragrant Phenolic ester 0.250%, gamma decalactone 0.070%, third undecalactone 0.450%, jasmonyl 0.600%, jasmine pyrans 0.050%, musk deer Fragrant T 2.800%, heliotropin 0.020%, glacial acetic acid 0.010%, santal 208 3.150%, santal 803 0.030% synthesizes oak moss 0.200%, white grapefruit oil 0.200%, perfume base 0.15% described in claim 1, Java santal 0.060%, Florol 1.300% is constituted.

7. application of the perfume base described in claim 1 in essence is prepared.

8. application of the essence described in any one of claim 2-6 in the product for needing fruits note is prepared.

9. application according to claim 8, it is characterised in that the product for needing fruits note is selected from perfume, washes one's hair Bath lotion, shampoo.