CN106107056A - A kind of preparation method containing neotame microcapsule-type sweeting agent - Google Patents
A kind of preparation method containing neotame microcapsule-type sweeting agent Download PDFInfo
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Abstract
The invention discloses a kind of preparation method containing neotame microcapsule-type sweeting agent, it is therefore an objective to solve high-load neotame in mixed feed sweeting agent, mix uneven technical problem.Technical scheme is as follows: take 10 ~ 90 parts of sweet substances, 0.5 ~ 15 part of synergist, 1 ~ 15 part of flavoring agent, 5 ~ 90 parts of soluble carrier, 5 ~ 20 parts of adsorbents, 200 ~ 400 weight portion water purification are in heating kettle, go to after uniform stirring in transfer still after being heated to 90 ~ 95 DEG C, transfer still is atomized pelletize under specific technological parameter, is dried to spherical particle, adsorption dry in fluid bed more again in drying tower.The sweeting agent neotame content that the present invention prepares is high, neotame is evenly distributed in every microcapsule, solve the neotame fusing point moisture absorption low, easy glue wall, facile hydrolysis lose sweet, mix a uneven difficult problem, improve and enrich the overall local flavor of sweeting agent, to improving feedstuff palatability, alleviate the feedstuff industry dependence to saccharin sodium, reduce the environmental pollution produced because of saccharin sodium, reduce feeding cost, there is critically important realistic meaning.
Description
Technical field
The present invention relates to feed processing technology field, be specifically related to feed sweetener technical field, particularly to one
Preparation method containing neotame microcapsule-type sweeting agent.
Background technology
Neotame is that Niu Te company of the U.S. is through 20 years of researches, the sweeting agent of a new generation of creativity and innovation, this sweeting agent
The development history making sweeting agent enters new chapter, and neotame is national by more than 30 as sweetening agent and flavour enhancer
Approval uses.China is common to various food and drink by ministry of Health of China approval neotame as sweeting agent on March 10th, 2003
In material, on October 19th, 2015, the Ministry of Agriculture permitted using in feed additive.
The sugariness of neotame is 7000 to 13000 times of sucrose, and sweet taste is pure long, but also has local flavor and extend and strengthen
The effect of agent, is the sweetest and most cost performance sweet substance in commodity so far.Substantial amounts of result of study shows, neotame is applicable to
All groups including child, anemia of pregnant woman, women breast-feeding their children and diabetics.It is applied to animal diet, fits improving it
Mouth property, improves animal feed intake, promotes that growth of animal has obvious effect.
But neotame there is also certain deficiency.One is that sugariness is high, and addition is few, it is difficult to mix homogeneously, has a strong impact on sweet taste
The using effect of agent, especially powder material.Additionally, due to the fusing point of neotame is the lowest, the easy moisture absorption, viscous wall, dissolve spray even if using
Mist drying process also is difficult to realize the high powder sweeting agent of neotame content and produces.Two be neotame under customary storage conditions, neotame
Dry powder has preferable stability, but stability in aqueous has certain limitation, its stability by temperature, acid-base value, time
Between etc. factor impact relatively big, sugariness has and to a certain degree declines, and then loses sweet.
Summary of the invention
Present invention aim to address that in prior art, neotame is difficult to mix homogeneously in sweeting agent, be not suitable for being spray-dried
Producing, during storage, sweet problem is lost in hydrolysis, and the feed sweetener the most also caused because saccharin sodium raw material is nervous for alleviation produces
Quagmire, for preferably solve feedstuff palatability, promote growth of animal provide solution.
For reaching above-mentioned purpose, the technical solution used in the present invention is as follows:
A kind of preparation method containing neotame microcapsule-type sweeting agent, comprises the following steps:
(1) take 200 ~ 400 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 10 ~ 90 parts of sweet substances, stirring
Dissolving, temperature is maintained at 90 ~ 95 DEG C, is then sequentially added into 0.5 ~ 15 part of synergist, 1 ~ 15 part of flavoring agent, 5 ~ 90 parts of solubilities loads
Body, 5 ~ 20 parts of adsorbents, uniform stirring, after being completely dissolved, in going to the material merged after purification by tubular filter
Turn in still；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.
Further, the sweet substance described in step (1) includes saccharin sodium, Calcium o-benzolsulfimide, saccharin zinc, sucralose, peace
One or more in match honey.
Further, the synergist described in step (1) includes neohesperidin dihydrochalcone, alitame, stevioside, sweet
Grass glucin, Momordica-Glycosides, neotame, the S-tert-butyl group-Cys methyl ester) in one or more.
Further, the flavoring agent described in step (1) include ethylmaltol, ethyl vanillin, AMP,
5 '-inosine monophosphate, 5 '-guanosine monophosphate disodium, sodium glutamate, malic acid, citric acid one or more；
Further, step (1) described soluble carrier include glucose, soluble starch, sodium sulfate, magnesium sulfate, sodium chloride,
One or more in disodium hydrogen phosphate, sodium tripolyphosphate.
Further, the adsorbent described in step (1) includes silicon dioxide, Maifanitum, maltodextrin, microcrystalline cellulose
Element, sodium carboxymethyl cellulose one or more.
Further, the adsorption liquid described in step (4) is by edible ethanol 10-20 part, neotame 8-10 part stirring and dissolving system
?.
Further, described edible ethanol alcoholic strength >=95%.
After using above-mentioned technique, there is advantages that
1, the present invention is directed to high-load neotame in mixed feed sweeting agent, mix uneven technical problem provide a kind of solution
Certainly scheme, solve the hydrolysis of neotame lose sweet, fusing point is low, be insoluble in water, a difficult problem for inapplicable spray drying.
2, the feed sweetener that the present invention produces, has good mobility, and neotame is all uniformly distributed in every microcapsule,
It initiates sweet sense and is similar to sucrose, and has lasting, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect
Fruit is better than sucrose.
3, the present invention is that the quagmire alleviating the feed sweetener production caused because saccharin sodium raw material is nervous provides solution
Scheme.Meanwhile, the production of this sweeting agent and popularization, decrease the feed sweetener dependence to saccharin sodium, thus reduce because of saccharin
The production of sodium and the problem of environmental pollution that causes.
4, production process equipment of the present invention is the dry spraying of routine, fluidized bed coating equipment, and raw material is easy to get, and can give birth in batches
Producing, needed for meeting large-scale production, application is strong.
To sum up, the one microcapsule-type sweeting agent Han neotame using present invention process to produce has an obvious advantage: neotame content
Height, neotame is evenly distributed in every microcapsule, solve the neotame fusing point moisture absorption low, easy glue wall, facile hydrolysis lose sweet, mix uneven
A difficult problem, improve and enrich the overall local flavor of sweeting agent, to improving feedstuff palatability, alleviate feedstuff industry saccharin sodium is depended on
Rely, reduce because saccharin sodium produces the environmental pollution caused, reduce feeding cost, there is critically important realistic meaning.
Detailed description of the invention
The present invention being expanded on further below in conjunction with embodiment, the number described in the present embodiment is parts by weight.
Embodiment 1
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, Calcium o-benzolsulfimide, sucralose) 10 parts；
Synergist (alitame, Momordica-Glycosides, glycyrrhizin) 0.5 part；
Flavoring agent (maltol, vanillin, 5 '-inosine monophosphate, 5 '-guanosine monophosphate disodium, sodium glutamate, malic acid) 1 part；
Soluble carrier (glucose, sodium sulfate, sodium dihydrogen phosphate, magnesium sulfate, sodium tripolyphosphate) 5 parts；
Adsorbent (silicon dioxide, Maifanitum) 5 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 10 parts
Neotame 8 parts
3, production process
(1) take 200 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 10 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 0.5 part of synergist, 5 parts of flavoring agent, 5 parts of soluble carrier, 5 parts of adsorbents, all
Even stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 10-60 micron, has good flowing
Property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Embodiment 2
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, acesulfame-K, sucralose) 40 parts；
Synergist (neohesperidin dihydrochalcone, stevioside) 5 parts；
Flavoring agent (maltol, vanillin, 5 '-inosine monophosphate, 5 '-guanosine monophosphate disodium, citric acid) 5 parts；
Soluble carrier (glucose, sodium sulfate, sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium tripolyphosphate) 50 parts；
Adsorbent (maltodextrin, microcrystalline cellulose) 10 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 12 parts
Neotame 8 parts
3, production process
(1) take 250 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 40 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 5 parts of synergists, 5 parts of flavoring agent, 50 parts of soluble carrier, 10 parts of adsorbents, all
Even stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 10-130 micron, has good flowing
Property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Embodiment 3
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, acesulfame-K, sucralose) 30 parts；
Synergist (neohesperidin dihydrochalcone, stevioside) 4 parts；
Flavoring agent (maltol, vanillin, 5 '-inosine monophosphate, 5 '-guanosine monophosphate disodium, citric acid) 6 parts；
Soluble carrier (sodium sulfate, sodium dihydrogen phosphate, sodium tripolyphosphate) 55 parts；
Adsorbent (the fine micro-element sodium of silicon dioxide, maltodextrin, carboxymethyl) 15 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 16 parts
Neotame 10 parts
3, production process
(1) take 280 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 30 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 4 parts of synergists, 6 parts of flavoring agent, 55 parts of soluble carrier, 15 parts of adsorbents, all
Even stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, room temperature
Lower startup boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump,
Adsorption liquid is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried convulsion
Device, keeps 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 20-150 micron, has good flowing
Property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Embodiment 4
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, saccharin zinc, acesulfame potassium) 20 parts；
Synergist (alitame, Momordica-Glycosides, the S-tert-butyl group-Cys methyl ester, neotame) 4 parts；
Flavoring agent (AMP, vanillin, citric acid, 5 '-guanosine monophosphate disodium, sodium glutamate, malic acid) 7 parts；
Soluble carrier (glucose, magnesium sulfate, sodium tripolyphosphate) 20 parts；
Adsorbent (silicon dioxide, microcrystalline Cellulose) 6 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 13 parts
Neotame 9 parts
3, production process
(1) take 300 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 20 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 4 parts of synergists, 7 parts of flavoring agent, 20 parts of soluble carrier, 6 parts of adsorbents, uniformly
Stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 20-110 micron, has good flowing
Property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Embodiment 5
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, saccharin zinc, acesulfame potassium) 70 parts；
Synergist (alitame, Momordica-Glycosides, the S-tert-butyl group-Cys methyl ester, neotame) 10 parts；
Flavoring agent (AMP, vanillin, citric acid, 5 '-guanosine monophosphate disodium, sodium glutamate, malic acid) 10 parts；
Soluble carrier (glucose, magnesium sulfate, sodium tripolyphosphate) 70 parts；
Adsorbent (silicon dioxide, microcrystalline Cellulose) 15 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 13 parts
Neotame 9 parts
3, production process
(1) take 360 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 70 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 10 parts of synergists, 10 parts of flavoring agent, 70 parts of soluble carrier, 15 parts of adsorbents,
Uniform stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 80-170 micron, has good flowing
Property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Embodiment 6
1, sweeting agent microcapsule proportioning
Sweet substance (saccharin sodium, saccharin zinc, sucralose) 90 parts；
Synergist (alitame, Momordica-Glycosides, the S-tert-butyl group-Cys methyl ester) 15 parts；
Flavoring agent (AMP, vanillin, 5 '-inosine monophosphate, 5 '-guanosine monophosphate disodium, sodium glutamate, malic acid) 15 parts；
Soluble carrier (glucose, sodium dihydrogen phosphate, magnesium sulfate, sodium tripolyphosphate) 90 parts；
Adsorbent (maltodextrin, microcrystalline Cellulose) 20 parts
2, the proportioning of adsorptive liquid
Edible ethanol (>=95%) 20 parts
Neotame 10 parts
3, production process
(1) take 400 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 90 parts of sweet substances, stirring and dissolving, temperature
Degree is maintained at 90 ~ 95 DEG C, is then sequentially added into 15 parts of synergists, 15 parts of flavoring agent, 90 parts of soluble carrier, 20 parts of adsorbents,
Uniform stirring, after being completely dissolved, is gone in transfer still by tubular filter after purification by the material merged；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.This product has relatively regular spheroidal particle, and its granular size, at 100-300 micron, has good stream
Dynamic property and dissolubility.
After measured, in this sweeting agent, neotame is all uniformly distributed in every microcapsule, and it initiates sweet sense and is similar to sucrose, and has
Persistently, joyful sweet taste, more can improve and cover the bad flavor of feedstuff, application effect is better than sucrose.
Above-mentioned listed embodiment is the preferred result of test of many times of the present invention, and the limit embodiment of non-invention, this
Skilled person it should be understood that the method also by orthogonal test draws other embodiments, and the present invention is at this most one by one
Limit.
Claims (7)
1. the preparation method containing neotame microcapsule-type sweeting agent, it is characterised in that comprise the following steps:
(1) take 200 ~ 400 weight portion water purification in heating kettle, after being heated to 90 ~ 95 DEG C, put into 10 ~ 90 parts of sweet substances, stirring
Dissolving, temperature is maintained at 90 ~ 95 DEG C, is then sequentially added into 0.5 ~ 15 part of synergist, 1 ~ 15 part of flavoring agent, 5 ~ 90 parts of solubilities loads
Body, 5 ~ 20 parts of adsorbents, uniform stirring, after being completely dissolved, in going to the material merged after purification by tubular filter
Turn in still；
(2) by the material in transfer still at 1. high-pressure pump pressure: 4-20mpa, 2. feeding temperature: 50～90 DEG C, 3. inlet temperature:
230～275 DEG C, 4. temperature of outgoing air: 85～120 DEG C, under the process conditions of 5. evaporation capacity: 200kg/h, atomization polymerization, is formed vaporific
Microgranule, the most vaporific microgranule sprays into drying tower and hot air, is dried to spherical particle, is deposited in bottom drying tower；
(3) crossing 60 mesh vibrosieves by being deposited in the spherical particle bottom drying tower, its siftage is that microcapsule granule type sweeting agent half becomes
Product；
(4) microcapsule granule type sweeting agent semi-finished product step (3) prepared are put in fluidized bed coating Granulation Equipments, open under room temperature
Dynamic boiling device, makes microcapsule granule type sweeting agent semi-finished product seethe with excitement in granulation tank flowing, hereafter opens peristaltic pump, by adsorption liquid
It is sprayed on microcapsule granule type sweeting agent semi-finished product with vaporific, baking temperature 40-65 DEG C is set, start and be dried extractor fan, protect
Hold 10 ~ 30 minutes；
(5) the sweeting agent microcapsule granule after step (4) adsorption dry is released from fluid bed and carry out subpackage, obtain containing neotame microcapsule
Type sweetener product.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 1, it is characterised in that step (1)
Described in sweet substance include one or more in saccharin sodium, Calcium o-benzolsulfimide, saccharin zinc, sucralose, acesulfame potassium.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 1, it is characterised in that step (1)
Described in synergist include neohesperidin dihydrochalcone, alitame, stevioside, glycyrrhizin, Momordica-Glycosides, neotame,
The S-tert-butyl group-Cys methyl ester) in one or more.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 1, it is characterised in that step (1)
Described in flavoring agent include ethylmaltol, ethyl vanillin, AMP, 5 '-inosine monophosphate, 5 '-guanyl two
Sodium, sodium glutamate, malic acid, citric acid one or more；
A kind of preparation method containing neotame microcapsule-type sweeting agent according to claim 1, it is characterised in that step (1) institute
State soluble carrier and include glucose, soluble starch, sodium sulfate, magnesium sulfate, sodium chloride, sodium dihydrogen phosphate, sodium tripolyphosphate
In one or more.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 1, it is characterised in that step (1)
Described in adsorbent include silicon dioxide, Maifanitum, maltodextrin, microcrystalline Cellulose, the one of sodium carboxymethyl cellulose or
Multiple.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 1, it is characterised in that step (4)
Described in adsorption liquid by edible ethanol 10 ~ 20 parts, 8 ~ 10 parts of stirring and dissolving of neotame prepare.
A kind of preparation method containing neotame microcapsule-type sweeting agent the most according to claim 7, it is characterised in that described food
With alcohol degree >=95%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610575887.6A CN106107056A (en) | 2016-07-21 | 2016-07-21 | A kind of preparation method containing neotame microcapsule-type sweeting agent |
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| CN106962613A (en) * | 2017-03-15 | 2017-07-21 | 成都合生元生物科技有限公司 | A kind of oligomerization sugar composite and preparation method thereof and feed |
| CN109497291A (en) * | 2018-11-10 | 2019-03-22 | 中国平煤神马集团开封兴化精细化工有限公司 | A kind of feed addictive and its production method |
| CN109770324A (en) * | 2018-12-19 | 2019-05-21 | 山东奔月生物科技有限公司 | A kind of compound sweetener and preparation method thereof |
| CN110495599A (en) * | 2019-09-16 | 2019-11-26 | 河北省天利海香精香料有限公司 | A kind of compound cocrystallization fumet and preparation method thereof |
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