CN106962613A - A kind of oligomerization sugar composite and preparation method thereof and feed - Google Patents
A kind of oligomerization sugar composite and preparation method thereof and feed Download PDFInfo
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- CN106962613A CN106962613A CN201710152408.4A CN201710152408A CN106962613A CN 106962613 A CN106962613 A CN 106962613A CN 201710152408 A CN201710152408 A CN 201710152408A CN 106962613 A CN106962613 A CN 106962613A
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Abstract
The present invention provides a kind of oligomerization sugar composite and preparation method thereof and feed, is related to field of feed processing.Oligomerization sugar composite, by mass percentage, including：Oligosaccharide 1 88%, sweet substance 0.5 50%, flavoring agent 0.5 10%, soluble carrier 10 90%, and adsorbent 0 10%, wherein, sweet substance includes neotame, and this oligomerization sugar composite can effectively facilitate animal intestinal tract health.In addition the invention further relates to a kind of preparation method of above-mentioned oligomerization sugar composite, oligosaccharide, sweet substance, flavoring agent, soluble carrier and adsorbent are mixed, simple operation can be such that each active ingredient of oligomerization sugar composite is sufficiently mixed uniformly.Include the feed of above-mentioned oligomerization sugar composite, palatability is good.
Description
Technical field
The present invention relates to field of feed processing, and more particularly to a kind of oligomerization sugar composite and preparation method thereof and feed.
Background technology
The gut flora of animal is a complicated ecosystem, and host organism is closely coupled, facilitates the stable state of host
And health.In the rear antibiotic epoch for limiting the use of and disabling antibiotic, animal and bird intestines problem becomes increasingly conspicuous, intestinal health be poultry and
The essential condition that domestic animal efficiently produces, maintains high viability and yield products of quality.
The sugariness of neotame is 7000 to 13000 times of sucrose, and sweet taste is pure long, but also extends and strengthen with local flavor
The effect of agent, is most sweet tea and the most sweet substance of cost performance in towering like a mountain peak modern commercialization.Substantial amounts of result of study shows, neotame application
In animal diet, to improving its palatability, animal feed intake is improved, promotes growth of animal to have obvious effect.But neotame
In the presence of certain deficiency：One is that sugariness is high, and addition is few, it is difficult to well mixed, has a strong impact on the using effect of sweetener, especially
Powder material.Two be neotame under customary storage conditions, neotame dry powder has preferable stability, but stability in aqueous
There is certain limitation, its stability is influenceed larger by factors such as temperature, acid-base value, times, sugariness has to be declined to a certain degree, is entered
And lose sweet tea.
The content of the invention
It is an object of the invention to provide a kind of oligomerization sugar composite, its reasonable mixture ratio, effectively by oligosaccharide and neotame knot
Close, improve the stability of neotame in aqueous, promote animal intestinal tract health.
Another object of the present invention is to provide a kind of preparation method for manufacturing oligomerization sugar composite, this method is operated just
Victory, is produced on a large scale, and each active ingredient of oligomerization sugar composite is sufficiently mixed uniformly, palatability is good.
Another object of the present invention is to provide a kind of feed, including above-mentioned oligomerization sugar composite, palatability is good.
The present invention is solved its technical problem and realized using following technical scheme：
The present invention proposes a kind of oligomerization sugar composite, by mass percentage, including：Oligosaccharide 1-88%, sweet substance
0.5-50%, flavoring agent 0.5-10%, soluble carrier 10-90%, and adsorbent 0-10%.
Wherein, sweet substance includes neotame.
The present invention propose it is a kind of manufacture oligomerization sugar composite preparation method, by oligosaccharide, sweet substance, flavoring agent, can
Solubleness carrier and adsorbent mixing.
The present invention proposes a kind of feed, and it includes above-mentioned oligomerization sugar composite.
The beneficial effect of oligomerization sugar composite provided in an embodiment of the present invention and preparation method thereof and feed is：Neotame is in pH
Be worth for 4.5 when it is most stable, and oligosaccharide pH between 3.0-6.0 it is stable, therefore oligosaccharide and neotame are rationally combined, can be with
The stability of neotame is significantly improved, prevents its sugariness from declining, and improves feed palatability, promotes feed intake, meanwhile, collaboration is few
Glycan promotes animal intestinal tract health together, collectively promotes animal growth, quick weightening.
In said composition, each active ingredient reasonable mixture ratio, synergy, the addition of adsorbent and soluble carrier makes
Neotame is easy to uniform diffusion, after being well mixed by the manufacture method, efficiently solves the easy moisture absorption of neotame and glues wall, facile hydrolysis mistake
The uneven problem of sweet tea, mixing, by the cooperation of sweet substance and flavoring agent, is effectively improved and enriches oligomerization sugar composite
Overall local flavor, improves feed palatability, reduces feeding cost.
Embodiment
, below will be in the embodiment of the present invention to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, are the conventional production that can be obtained by commercially available purchase
Product.
Oligomerization sugar composite of the embodiment of the present invention and preparation method thereof and feed are specifically described below.
A kind of oligomerization sugar composite, by mass percentage, including：Oligosaccharide 1-88%, sweet substance 0.5-50%, increase
Taste agent 0.5-10%, soluble carrier 10-90%, and adsorbent 0-10%；Should in the range of, by oligosaccharide, sweet substance and
Flavoring agent reasonable combination, is effectively improved palatability, can effectively facilitate promotion animal feed intake, and promote animal intestinal tract to be good for
Health, by soluble carrier and adsorbent, makes oligosaccharide, sweet substance and flavoring agent be more easy to be well mixed.
Specifically, sweet substance includes neotame, can be effectively improved palatability.Neotame chemical name is N- [N- (3,3- diformazans
Base butyl)-L- α-aspartoyl]-L-phenylalanine -1- methyl esters is a kind of white crystalline powder, containing about 4.5% crystallization water.
It has pure sweet taste, and sweet taste is coordinated, and bitter taste and metallic taste without the normal band of other intense sweeteners can significantly prolong
The long, mouthfeel of enhancing product and fragrance, security are higher, and can improve animal feed intake, promote animal health growth.
Preferably, sweet substance also includes in sweetening agent, i.e. the oligomerization sugar composite, and neotame can be used alone,
It can also be acted synergistically with sweetening agent, palatability is improved jointly, reduce cost of manufacture.
Specifically, sweetening agent can be the material such as saccharin or saccharin salts substances, it is highly preferred that sweetening agent is selected
From at least one of saccharin sodium, calcium benzosulphimide, saccharin zinc, Sucralose, acesulfame potassium and stevioside, such as sweetening agent can be with
Can also be mixture of Sucralose, acesulfame potassium and stevioside etc., effectively reduction is made for saccharin sodium, or saccharin, or acesulfame potassium
Make cost, and improve the stability of neotame, when sweetening agent is that plurality of active ingredients is mixed, the ratio between each active ingredient
Do not limit, belong in the scope of protection of the invention.
Oligosaccharide refers to the compound being polymerized containing 2-10 glycosidic bond, and it can improve animal intestinal tract microorganism species
Balance, can improve immunity with the immune system of stimulating animal body, improve efficiency of feed utilization, so that promote growth of animal,
The probability that disease occurs for animal is effectively reduced in the case of reduction or without antibiotic.
Specifically, oligosaccharide is selected from xylo-oligosaccharide, galactooligosaccharide, chitosan oligomer, chitosan oligosaccharide, FOS and sweet dew
At least one of oligosaccharides.Such as oligosaccharide can be xylo-oligosaccharide, or galactooligosaccharide, or chitosan oligomer and shell
Mixture of oligosaccharides etc., can promote animal intestinal tract health.When oligosaccharide is that plurality of active ingredients is mixed, between each active ingredient
Ratio do not limit, belong in the scope of protection of the invention.
Flavoring agent is mainly used in improving palatability, promotes feed intake rate, while promoting animal metabolism.Specifically,
Flavoring agent is selected from maltol, ethylmaltol, vanillic aldehyde, Ethyl vanillin, AMP, IMP, 5 '-bird
Thuja acid disodium, sodium glutamate, malic acid, citric acid, neohesperidin dihydrochalcone, glycyrrhizin, mogroside and the tertiary fourths of s-
At least one of base-Cys methyl ester, such as flavoring agent can be ethylmaltol, or vanillic aldehyde can also be
The mixture of AMP and IMP, or sodium glutamate and malic acid mixture etc..
The application of soluble carrier makes oligomerization sugar composite be more convenient for being assimilated by animal, and fills each active ingredient
Divide well mixed.
Specifically, soluble carrier be selected from maltodextrin, glucose, soluble starch, sodium sulphate, magnesium sulfate, sodium chloride,
At least one of sodium dihydrogen phosphate, disodium hydrogen phosphate and sodium tripolyphosphate, such as soluble carrier can be maltodextrin, or
Sodium chloride, or sodium tripolyphosphate, can also be mixture of glucose, soluble starch and sodium sulphate etc..
Adsorbent is mainly used in each active ingredient being uniformly distributed in its surface, specifically, and adsorbent is selected from titanium dioxide
At least one of silicon, medical stone and microcrystalline cellulose, such as adsorbent can be silica, can also be medical stone and micro-
Mixture of crystalline cellulose etc..
Present invention also offers the preparation method for manufacturing above-mentioned oligomerization sugar composite, specifically, by oligosaccharide, sweet taste thing
Matter, flavoring agent, soluble carrier and adsorbent mixing.
Preferably, be mixed in 50-95 DEG C of water and carry out, obtain mixed liquor, 50-95 DEG C of water can make it is above-mentioned it is each effectively
Composition quickly dissolves, and is thoroughly mixed together.Preferably, oligosaccharide, sweet substance, flavoring agent, soluble carrier and adsorbent
Gross mass and water quality ratio be 1:0.5-3, prevents from dissolving insufficient or hypervolia caused by water shortage
Caused drying efficiency is low.
It is highly preferred that the first mixed liquor is obtained after mixed dissolution in water by oligosaccharide and sweet substance prior to 50-95 DEG C,
Flavoring agent, soluble carrier and adsorbent are added into the first mixed liquor again, mixed dissolution is carried out, obtains mixed liquor, step-wise dissolution
Make dissolving more abundant, mixing is evenly.
It is further preferred that mixed process is with stirring, mixing efficiency is effectively improved, stirring can be mechanical agitation,
It can be ultrasonic wave stirring, be sufficiently mixed each active ingredient in mixed liquor, be uniformly distributed in water.Preferably, in absorption
When agent is 0, the transparent shape of mixed solution prevents dissolving is insufficient from causing crystal to separate out.
It it is 150-170 DEG C preferably in EAT, leaving air temp is 90- when then by mixed liquor centrifugal spray drying
Centrifugal spray drying is carried out under conditions of 110 DEG C, moment volatilization moisture obtains solid-phase intermediate.
Solid-phase intermediate is finally crossed into 60-65 mesh sieves, obtained undersize material is purpose particle, the as present invention is carried
The oligomerization sugar composite of confession.The particle of the oligomerization sugar composite makes each active ingredient in every particle by fully dissolving emulsification
Middle uniformity, realizes the efficient combination of oligosaccharide and sweet substance, promotes feed intake rate, and is easily consumed absorption,
Animal intestinal tract health is effectively facilitated, so as to promote growth of animal.
Mixing can also directly mix for the solid particle of each active ingredient, it is preferable that also include before direct mixing
60-65 mesh sieves are crossed to each active ingredient, undersize material is obtained, undersize material is mixed in proportion, the drying to obtain present invention
The oligomerization sugar composite of offer；It is further preferred that the on-the-sieve material that sieving is obtained further is crushed, sieve, improve
The utilization rate of each material, reduces cost of manufacture.
And include the feed of above-mentioned oligomerization sugar composite, by improving feed palatability and intestinal health, effectively facilitate
Feed intake rate, promotes animal weightening, improves the utilization rate of feed, feeding cost is reduced, with splendid commercial application value.
The feature and performance to the present invention are described in further detail with reference to embodiments.
Embodiment 1
A kind of oligomerization sugar composite, it is made by following methods：By 55kg xylo-oligosaccharide syrup, 12kg neotame and
The mixture of saccharin sodium, is completely dissolved in the water that 200kg temperature is 75 DEG C, obtains the first mixed liquor, then toward the first mixing
2kg neohesperidin dihydrochalcone, maltol, vanillic aldehyde, IMP and 5'-GMP2Na are added in liquid
Mixture, 60kg maltodextrin and the mixture of glucose, fully dissolving, obtain the mixed liquor of transparent state, in air intake
Mixed liquor is carried out after centrifugal spray drying under conditions of 150 DEG C of temperature, 110 DEG C of leaving air temp, 60 mesh sieves is crossed and produces.
Embodiment 2
A kind of oligomerization sugar composite, it is made by following methods：By 55kg xylo-oligosaccharide syrup and galactooligosaccharide
Mixture, 20kg neotame and the mixture of saccharin sodium are completely dissolved in the water that 150kg temperature is 50 DEG C, obtain first and mix
Liquid is closed, then toward maltol, vanillic aldehyde, IMP and the 5'-GMP2Na of addition 1.5kg in the first mixed liquor
Mixture, 53kg maltodextrin and the mixture of glucose, fully dissolving obtain the mixed liquor of transparent state, entered
Mixed liquor is carried out after centrifugal spray drying under conditions of 170 DEG C of air temperature, 100 DEG C of leaving air temp, 63 mesh sieves is crossed and produces.
Embodiment 3
A kind of feed, including oligomerization sugar composite, wherein oligomerization sugar composite are made by following methods：By the low of 40kg
The mixture of xylan syrup and galactooligosaccharide, 10kg neotame and the mixture of saccharin sodium, 2kg maltol, vanillic aldehyde,
The mixture of IMP and 5'-GMP2Na, 48kg maltodextrin, soluble starch, sodium chloride and trimerization phosphorus
The mixture of sour sodium, is completely dissolved in the water that 300kg temperature is 95 DEG C, the mixed liquor of transparent state is obtained, in air intake
Mixed liquor is carried out after centrifugal spray drying under conditions of 165 DEG C of temperature, 90 DEG C of leaving air temp, 65 mesh sieves is crossed and produces.
Embodiment 4
A kind of oligomerization sugar composite, it is made by following methods：By 60kg xylo-oligosaccharide, 15kg neotame and saccharin
The mixture of sodium, 3kg maltol, vanillic aldehyde, the mixture of IMP and 5'-GMP2Na, 20kg malt
The mixture of dextrin and DEXTROSE ANHYDROUS, and 2kg silica and dextrin, respectively cross 60 mesh sieves, by obtained screenings
Material is well mixed, produces.
Embodiment 5
A kind of oligomerization sugar composite, it is made by following methods：By the mixed of 65kg xylo-oligosaccharide and galactooligosaccharide
Compound, 20kg neotame and the mixture of saccharin sodium, 2kg maltol, vanillic aldehyde, IMP and 5'-GMP two
The mixture of sodium, 10kg maltodextrin and the mixture of DEXTROSE ANHYDROUS, and 3kg silica and dextrin, mistake respectively
63 mesh sieves, obtained undersize material is well mixed, produced.
Embodiment 6
A kind of feed, including oligomerization sugar composite, wherein oligomerization sugar composite are made by following methods：By 69.5kg's
The mixture of xylo-oligosaccharide and galactooligosaccharide, 0.5kg neotame and the mixture of saccharin sodium, 10kg maltol, vanillic aldehyde,
The mixture of IMP and 5'-GMP2Na, 10kg maltodextrin and the mixture of DEXTROSE ANHYDROUS, and
10kg silica and dextrin, crosses 65 mesh sieves, obtained undersize material is well mixed, produced respectively.
Embodiment 7
A kind of feed, including oligomerization sugar composite, wherein oligomerization sugar composite are made by following methods：By the low of 30kg
The mixture of xylan, chitosan oligosaccharide and galactooligosaccharide, 35kg neotame, 0.5kg maltol, vanillic aldehyde, 5'-inosinic acid two
The mixture of sodium and 5'-GMP2Na, 17kg maltodextrin and the mixture of DEXTROSE ANHYDROUS, and 17.5kg dioxy
SiClx and dextrin, cross 60 mesh sieves, obtained undersize material are well mixed, produced respectively.
30 nests wean sucking pig is chosen, control group and test group, the common basal diet in control group feeding market is equally divided into
Feed, the feed of test group feeding is using the basal diet feed of control group feeding as substrate, and being added with for appropriateness is of the invention real
The oligomerization sugar composite of example offer is provided.Feeding way uses nature Feeding way, i.e., freely drink water, freely take food.During feeding
Between for sucking pig wean start to be born after untill 70 days.
By test group, the comparison of control group, the result of the test of collection is as follows：
The result of the test of table 1 is counted
It can be obtained, started in sucking pig wean to after being born in 70 day this period by table 1, in the average just initial body of control group
It is great in the case of test group, the feed of test group of the present invention can effectively improve sucking pig daily ingestion amount, and sucking pig averagely has a net increase of
Weight ratio control group averagely has a net increase of the high 2.37kg of body weight, illustrates that oligomerization sugar composite can be effectively improved feed palatability, promotes breast
Pig grazing rate, and promote it to digest and assimilate feed, sucking pig weightening is effectively facilitated, and improve sucking pig function of intestinal canal, prevent
Sucking pig diarrhoea reduction diarrhea rate.
After 70 days after sucking pig is born terminate feeding, selected respectively after 2 sucking pig anesthesia from test group and control group at random
Sacrificed by exsanguination, opens rapidly abdominal cavity, in collection jejunum end content under aseptic condition, and the above thing is placed in freezer
Freeze, specifically, using DNS colorimetric method for determining jejunal content amylase activities, prolease activity is determined using Forint phenol method.
As a result it is as shown in table 2.
The test result of table 2
It can be obtained by table 2, test group sucking pig sky intestinal proteases and amylase activity are above control group, illustrate oligomerization
Sugar composite can effectively facilitate flora in sucking pig body and breed, and promote intestinal enzyme activity to raise, and promote digesting and assimilating for nutriment,
The conversion ratio of feed is improved, with significant economic benefit.
In summary, oligomerization sugar composite provided in an embodiment of the present invention and preparation method thereof and feed, the oligosaccharide group
Each composition safety non-toxic in compound, synergy, effect stability effectively improves animal intestinal tract health, added with oligosaccharide combination
The feed palatability of thing is good, effectively improves the utilization rate of feed.The preparation method controllability is good, simple and convenient, effectively drop
Low cost of manufacture.
Embodiments described above is a part of embodiment of the invention, rather than whole embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
1. a kind of oligomerization sugar composite, it is characterised in that by mass percentage, including：Oligosaccharide 1-88%, sweet substance
0.5-50%, flavoring agent 0.5-10%, soluble carrier 10-90%, and adsorbent 0-10%；
The sweet substance includes neotame.
2. composition according to claim 1, it is characterised in that the sweet substance also includes sweetening agent, described
Sweetening agent is selected from least one of saccharin sodium, calcium benzosulphimide, saccharin zinc, Sucralose, acesulfame potassium and stevioside.
3. composition according to claim 1, it is characterised in that the oligosaccharide be selected from xylo-oligosaccharide, galactooligosaccharide,
At least one of chitosan oligomer, chitosan oligosaccharide, FOS and manna oligosacchride.
4. composition according to claim 1, it is characterised in that the soluble carrier be selected from maltodextrin, glucose,
At least one in soluble starch, sodium sulphate, magnesium sulfate, sodium chloride, sodium dihydrogen phosphate, disodium hydrogen phosphate and sodium tripolyphosphate
Kind.
5. composition according to claim 1, it is characterised in that the adsorbent is selected from silica, medical stone and micro-
At least one of crystalline cellulose.
6. composition according to claim 1, it is characterised in that the flavoring agent is selected from maltol, ethylmaltol, perfume (or spice)
Lan Su, Ethyl vanillin, AMP, IMP, 5'-GMP2Na, sodium glutamate, malic acid, lemon
At least one in acid, neohesperidin dihydrochalcone, glycyrrhizin, mogroside and the s- tert-butyl groups-Cys methyl ester
Kind.
7. a kind of preparation method for manufacturing the composition as described in claim any one of 1-6, it is characterised in that by the oligomerization
Sugared, described sweet substance, the flavoring agent, the soluble carrier and adsorbent mixing.
8. preparation method according to claim 7, it is characterised in that be mixed in 50-95 DEG C of water and carry out.
9. preparation method according to claim 8, it is characterised in that in carrying out centrifugal spray drying after mixing, it is described from
Heart spray drying is 150-170 DEG C in EAT, and leaving air temp is progress under conditions of 90-110 DEG C.
10. a kind of feed, it is characterised in that including the oligomerization sugar composite as described in claim any one of 1-6.
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| CN108813167A (en) * | 2018-05-25 | 2018-11-16 | 成都大帝汉克生物科技有限公司 | A kind of composite sweetener and preparation method thereof with reduction diarrhea |
| CN109480112A (en) * | 2018-12-29 | 2019-03-19 | 广州傲农生物科技有限公司 | A kind of composite feed additive and the preparation method and application thereof |
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Application publication date: 20170721 |