CN106106842A - A kind of goldball onion quintessence oil and preparation method thereof - Google Patents
A kind of goldball onion quintessence oil and preparation method thereof Download PDFInfo
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- CN106106842A CN106106842A CN201610473144.8A CN201610473144A CN106106842A CN 106106842 A CN106106842 A CN 106106842A CN 201610473144 A CN201610473144 A CN 201610473144A CN 106106842 A CN106106842 A CN 106106842A
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- oil
- goldball onion
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- onion
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
The present invention relates to a kind of goldball onion quintessence oil, its constituent and parts by weight are as follows: mass concentration be 10% dimethyl disulfide 0.5 2 parts, NSC 97324 0.6 4 parts, diallyl disulphide 0.5 2 parts, Diallytrisin 0.2 1 parts；Mass concentration be 1% dipropyl disulfide 0.8 3 parts, 0.8 3 parts of dipropyl trisulfide ether, methacrylic disulfide 0.7 2 parts, allyl sulfide 0.2 1 parts；Mass concentration is the allium mongolicum regel seed oil 10 20 parts of 100%；Mass concentration is the goldball onion immersion oil 40 80 parts of 100%；Mass concentration be 100% soybean oil be supplemented to 100 parts.Goldball onion quintessence oil of the present invention has nature, strong goldball onion local flavor, meets people's pursuit to local flavor, expands the range of goldball onion, adds the added value of goldball onion.
Description
Technical field
The invention belongs to food processing technology field, especially a kind of goldball onion quintessence oil and preparation method thereof.
Background technology
Goldball onion (Allium mongolicum Regel) has another name called Allium mongolicum Regel, Herba Allii prattii, Herba Alii fistulosi, Hu Muli (Mongolian) etc., is hundred
Conjunction section (LiLiaceae) Allium (Allium) perennial herb xerophyte.Goldball onion containing abundant vegetable protein, dietary fiber and
The multiple nutritional components such as needed by human body mineral, vitamin, record according to mongolian medicine allusion quotation: goldball onion has lowering blood pressure and blood fat, appetizing disappears
Food, strengthening kidney and tonifying Yang, the special efficacy that treats constipation, be a kind of green wild vegetable with high nutritive value and medical value,
It is described as " desert wild herbs ", " the good vegetables of sand plain ", " Ganoderma in dish ".Because of its have that cold-resistant, drought resisting, disease resistance be strong, strong adaptability and
Being prone to the characteristics such as cultivation, checking winds and fixing drifting sand, aspect also functions to certain effect, has the important ecological value.Goldball onion nontoxic edible,
Mild and mellow, pungent rushes nose, unique flavor, typically can cold and dressed with sauce, stir-fry and eat or pickle, deeply liked by the people.
At present the goldball onion overwhelming majority uses as the herbage of sheep, and according to locality pastoral area herdsman experience for many years, sheep searches for food sand
After Herba Alii fistulosi, the speed of growth is accelerated, and sickness rate reduces, and its meat is fresh and does not has a strong smell, fertile and oiliness, and continuous fragrant good to eat, the girth of a garment is alternate, can significantly change
The quality of kind Carnis caprae seu ovis and local flavor.Small part is as edible, the most cold and dressed with sauce, stir-fry and eat, cook filling, seasoning, pickled all have rare
U.S.A hides, and is fully natural green health food.But goldball onion is to eat vegetable raw, it is difficult to long-time storage, and in order to obtain stronger wind
Taste needs to add in large quantities, greatly limit the range of goldball onion, produces so needing a kind of natural, strong goldball onion local flavor badly
Product, meet people's pursuit to local flavor, expand its range, increase its added value.
By retrieval, not yet find the patent publication us relevant to present patent application.
Summary of the invention
In place of it is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of goldball onion quintessence oil and preparation method thereof,
This goldball onion quintessence oil has nature, strong goldball onion local flavor, meets people's pursuit to local flavor, expands the range of goldball onion,
Add the added value of goldball onion.
The present invention solves it and technical problem is that and take techniques below scheme to realize:
A kind of goldball onion quintessence oil, its constituent and parts by weight are as follows:
Wherein, described dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl
The solvent of base disulfide, dipropyl trisulfide ether, methacrylic disulfide and allyl sulfide is soybean oil.
And, described soybean oil is one-level soybean oil.
And, the preparation method of described goldball onion immersion oil is as follows:
(1) raw material prepares: goldball onion is removed Huang Ye, rotten leaf, is placed in clear water and cleans up, and is put at shady and cool backlight and dries,
Then rub and obtain goldball onion slurry, standby；
Extraction: by salad oil according to 5:1～1:1 join step (1) in goldball onion slurry in, 25 DEG C～45 DEG C, batch (-type)
Mechanical agitation, extracts 15h～90h, then solid-liquid separation, and gained filtrate is oil water mixture, is then stood by oil water mixture
4h～12h, Liquid liquid Separation, oil reservoir is goldball onion immersion oil semifinished product；
(3) refine: by step (2) in obtained by goldball onion immersion oil semifinished product be placed in supercritical CO2In extraction kettle, according to extraction
Temperature 35-45 DEG C, separates I temperature 40-60 DEG C, separates II temperature 30-50 DEG C, and extracting pressure is 15-35MPa, separates I pressure 8-
15MPa, separates II pressure natural, CO2Flow be 20-25kg/h, refined 3-6h, obtain goldball onion immersion oil.
The preparation method of goldball onion quintessence oil as above, it is characterised in that: step is as follows:
By raw material monomer dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin,
Dipropyl disulfide, dipropyl trisulfide ether, methacrylic disulfide, allyl sulfide soybean oil are diluted to required
The mass concentration wanted；
(2) various raw materials are combined according to different additions；
(3) it is diluted joining foot to the raw material after combination as solvent with soybean oil, obtains goldball onion quintessence oil.
Advantages of the present invention and good effect be:
1, goldball onion quintessence oil of the present invention has nature, strong goldball onion local flavor, meets people's pursuit to local flavor, expands sand
The range of Herba Alii fistulosi, adds the added value of goldball onion.
2, the inventive method raw material sources are extensive, with low cost, and method is simple, easy to operate, improves work efficiency.
3, abstraction technique is organically combined by the present invention with exquisite meat flavor formulating technology, it is thus achieved that local flavor is natural, strong, full, stay
Fragrant what lasting Herba Alii fistulosi quintessence oil so that people can enjoy this beautiful local flavor whenever and wherever possible.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described；Following embodiment is illustrative, is not determinate,
Protection scope of the present invention can not be limited with following embodiment.
Raw material used in the present invention, if no special instructions, is the commercially available prod of routine；Used in the present invention
Method, if no special instructions, is the conventional method of this area.
Embodiment 1
A kind of goldball onion quintessence oil, its constituent and parts by weight are as follows:
Wherein, described dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl
The solvent of base disulfide, dipropyl trisulfide ether, methacrylic disulfide and allyl sulfide is soybean oil.
The preparation method of above-mentioned goldball onion immersion oil is as follows:
(1) raw material prepares: goldball onion is removed Huang Ye, rotten leaf, is placed in clear water and cleans up, and is put at shady and cool backlight and dries,
Then rub and obtain goldball onion slurry, standby；
Extraction: by salad oil according to 5:1 join step (1) in goldball onion slurry in, 25 DEG C, intermittent type mechanical stir, leaching
Carrying 15h, then solid-liquid separation, gained filtrate is oil water mixture, and then oil water mixture stands 4h, Liquid liquid Separation, oil reservoir
It is goldball onion immersion oil semifinished product；
(3) refine: by step (2) in obtained by goldball onion immersion oil semifinished product be placed in supercritical CO2In extraction kettle, according to extraction
Temperature 35 DEG C, separates I temperature 40 DEG C, separates II temperature 30 DEG C, and extracting pressure is 15MPa, separates I pressure 8MPa, separates II pressure
Power is natural, CO2Flow be 20kg/h, refined 3h, obtain goldball onion immersion oil.
The preparation method of above-mentioned goldball onion quintessence oil, step is as follows:
By raw material monomer dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin,
Dipropyl disulfide, dipropyl trisulfide ether, methacrylic disulfide, allyl sulfide soybean oil are diluted to required
The mass concentration wanted；
(2) various raw materials are combined according to different additions；
(3) it is diluted joining foot to the raw material after combination as solvent with soybean oil, obtains goldball onion quintessence oil.
Embodiment 2
A kind of goldball onion quintessence oil, its constituent and parts by weight are as follows:
Wherein, described dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl
The solvent of base disulfide, dipropyl trisulfide ether, methacrylic disulfide and allyl sulfide is soybean oil.
Wherein, above-mentioned soybean oil can be one-level soybean oil.
The preparation method of above-mentioned goldball onion immersion oil is as follows:
(1) raw material prepares: goldball onion is removed Huang Ye, rotten leaf, is placed in clear water and cleans up, and is put at shady and cool backlight and dries,
Then rub and obtain goldball onion slurry, standby；
Extraction: by salad oil according to 3:1 join step (1) in goldball onion slurry in, 35 DEG C, intermittent type mechanical stir, leaching
Carrying 50h, then solid-liquid separation, gained filtrate is oil water mixture, and then oil water mixture stands 8h, Liquid liquid Separation, oil reservoir
It is goldball onion immersion oil semifinished product；
(3) refine: by step (2) in obtained by goldball onion immersion oil semifinished product be placed in supercritical CO2In extraction kettle, according to extraction
Temperature 40 DEG C, separates I temperature 50 C, separates II temperature 40 DEG C, and extracting pressure is 25MPa, separates I pressure 12MPa, separates II pressure
Power is natural, CO2Flow be 22kg/h, refined 4.5h, obtain goldball onion immersion oil.
The preparation method of above-mentioned goldball onion quintessence oil, step is as follows:
By raw material monomer dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin,
Dipropyl disulfide, dipropyl trisulfide ether, methacrylic disulfide, allyl sulfide soybean oil are diluted to required
The mass concentration wanted；
(2) various raw materials are combined according to different additions；
(3) it is diluted joining foot to the raw material after combination as solvent with soybean oil, obtains goldball onion quintessence oil.
Embodiment 3
A kind of goldball onion quintessence oil, its constituent and parts by weight are as follows:
Wherein, described dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl
The solvent of base disulfide, dipropyl trisulfide ether, methacrylic disulfide and allyl sulfide is soybean oil.
Wherein, above-mentioned soybean oil can be one-level soybean oil.
The preparation method of above-mentioned goldball onion immersion oil is as follows:
(1) raw material prepares: goldball onion is removed Huang Ye, rotten leaf, is placed in clear water and cleans up, and is put at shady and cool backlight and dries,
Then rub and obtain goldball onion slurry, standby；
Extraction: by salad oil according to 1:1 join step (1) in goldball onion slurry in, 45 DEG C, intermittent type mechanical stir, leaching
Carrying 90h, then solid-liquid separation, gained filtrate is oil water mixture, and then oil water mixture stands 12h, Liquid liquid Separation, oil reservoir
It is goldball onion immersion oil semifinished product；
(3) refine: by step (2) in obtained by goldball onion immersion oil semifinished product be placed in supercritical CO2In extraction kettle, according to extraction
Temperature 45 C, separates I temperature 60 C, separates II temperature 50 C, and extracting pressure is 35MPa, separates I pressure 15MPa, separates II pressure
Power is natural, CO2Flow be 25kg/h, refined 3-6h, obtain goldball onion immersion oil.
The preparation method of above-mentioned goldball onion quintessence oil, step is as follows:
By raw material monomer dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin,
Dipropyl disulfide, dipropyl trisulfide ether, methacrylic disulfide, allyl sulfide soybean oil are diluted to required
The mass concentration wanted；
(2) various raw materials are combined according to different additions；
(3) it is diluted joining foot to the raw material after combination as solvent with soybean oil, obtains goldball onion quintessence oil.
The above, be only presently preferred embodiments of the present invention, and technical scheme is not made any form
On restriction.Any simple modification that above example is made by every technical spirit according to the present invention, equivalent variations with repair
Decorations, all still fall within the range of technical scheme.
Claims (4)
1. a goldball onion quintessence oil, it is characterised in that: its constituent and parts by weight are as follows:
Wherein, described dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl two
The solvent of thioether, dipropyl trisulfide ether, methacrylic disulfide and allyl sulfide is soybean oil.
Goldball onion quintessence oil the most according to claim 1, it is characterised in that: described soybean oil is one-level soybean oil.
Goldball onion quintessence oil the most according to claim 1 and 2, it is characterised in that: the preparation method of described goldball onion immersion oil is as follows:
(1) raw material prepares: goldball onion is removed Huang Ye, rotten leaf, is placed in clear water and cleans up, and is put at shady and cool backlight and dries, then
Rubbing obtains goldball onion slurry, standby；
Extraction: by salad oil according to 5:1-1:1 join step (1) in goldball onion slurry in, 25 DEG C-45 DEG C, intermittent type mechanical stirs
Mixing, extract 15h-90h, then solid-liquid separation, gained filtrate is oil water mixture, then oil water mixture is stood 4h-12h,
Liquid liquid Separation, oil reservoir is goldball onion immersion oil semifinished product；
(3) refine: by step (2) in obtained by goldball onion immersion oil semifinished product be placed in supercritical CO2In extraction kettle, according to extraction temperature
35-45 DEG C, separating I temperature 40-60 DEG C, separate II temperature 30-50 DEG C, extracting pressure is 15-35MPa, separates I pressure 8-
15MPa, separates II pressure natural, CO2Flow be 20-25kg/h, refined 3-6h, obtain goldball onion immersion oil.
4. the preparation method of the goldball onion quintessence oil as described in any one of claims 1 to 3, it is characterised in that: step is as follows:
(1) by raw material monomer dimethyl disulfide, NSC 97324, diallyl disulphide, Diallytrisin, dipropyl
Base disulfide, dipropyl trisulfide ether, methacrylic disulfide, allyl sulfide soybean oil are diluted to required
Mass concentration；
(2) various raw materials are combined according to different additions；
(3) it is diluted joining foot to the raw material after combination as solvent with soybean oil, obtains goldball onion quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610473144.8A CN106106842A (en) | 2016-06-24 | 2016-06-24 | A kind of goldball onion quintessence oil and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610473144.8A CN106106842A (en) | 2016-06-24 | 2016-06-24 | A kind of goldball onion quintessence oil and preparation method thereof |
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| CN106106842A true CN106106842A (en) | 2016-11-16 |
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| CN201610473144.8A Pending CN106106842A (en) | 2016-06-24 | 2016-06-24 | A kind of goldball onion quintessence oil and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108308284A (en) * | 2018-03-14 | 2018-07-24 | 山东天博食品配料有限公司 | A kind of chive essential oil and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101781602A (en) * | 2010-03-11 | 2010-07-21 | 南京农业大学 | Method for extracting allium mongolicum regel seed oil by using supercritical carbon dioxide |
| CN104642568A (en) * | 2015-01-21 | 2015-05-27 | 徐晓云 | Preparation method of chive-flavored flavoring oil |
| CN105661451A (en) * | 2016-01-19 | 2016-06-15 | 漯河乐佳食品科技有限公司 | Chive oil essence |
| CN105685937A (en) * | 2016-01-20 | 2016-06-22 | 漯河乐佳食品科技有限公司 | Pork powder prepared by using reaction spice and preparation method thereof |
-
2016
- 2016-06-24 CN CN201610473144.8A patent/CN106106842A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101781602A (en) * | 2010-03-11 | 2010-07-21 | 南京农业大学 | Method for extracting allium mongolicum regel seed oil by using supercritical carbon dioxide |
| CN104642568A (en) * | 2015-01-21 | 2015-05-27 | 徐晓云 | Preparation method of chive-flavored flavoring oil |
| CN105661451A (en) * | 2016-01-19 | 2016-06-15 | 漯河乐佳食品科技有限公司 | Chive oil essence |
| CN105685937A (en) * | 2016-01-20 | 2016-06-22 | 漯河乐佳食品科技有限公司 | Pork powder prepared by using reaction spice and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 刘振伟: "《莱芜鸡腿葱》", 31 December 2012 * |
| 刘艳 等: "新疆野葱挥发油中化学成分的测定", 《中国调味品》 * |
| 司民真 等: "葱属植物挥发性物质研究", 《楚雄师范学院学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108308284A (en) * | 2018-03-14 | 2018-07-24 | 山东天博食品配料有限公司 | A kind of chive essential oil and preparation method thereof |
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