CN106083429A - A kind of method preparing Bt biological pesticide for raw material with straw - Google Patents
A kind of method preparing Bt biological pesticide for raw material with straw Download PDFInfo
- Publication number
- CN106083429A CN106083429A CN201610423203.0A CN201610423203A CN106083429A CN 106083429 A CN106083429 A CN 106083429A CN 201610423203 A CN201610423203 A CN 201610423203A CN 106083429 A CN106083429 A CN 106083429A
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- China
- Prior art keywords
- straw
- stalk
- raw material
- biological pesticide
- method preparing
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/002—Solid waste from mechanical processing of material, e.g. seed coats, olive pits, almond shells, fruit residue, rice hulls
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
- C05F5/008—Waste from biochemical processing of material, e.g. fermentation, breweries
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Pest Control & Pesticides (AREA)
- Environmental & Geological Engineering (AREA)
- Biotechnology (AREA)
- Plant Pathology (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of method preparing Bt biological pesticide for raw material with straw, comprise the following steps: S1, pretreatment for stalk: after collecting stalk, soak dry in the sun, pretreatment is carried out for stalk so that stalk effective ratio area increases；S2, stalk is hydrolyzed into can zymolysis sugar: stalk is added in hydrolytic tank, heat hydrolytic tank to 120 DEG C, keep temperature-resistant, add catalyst, solid-to-liquid ratio is 1:3, react 3h；S3, for the solidification of raw material after hydrolysis: after the stalk taking-up that will hydrolyze, after addition solid-state carrier, put into centrifugal stirrer and be stirred；S4, the solidification fermentation of straw: the raw material being cured is added in fermentation tank, carries out solidification fermentation；S5, the molding of fertilizer: the raw material fermented is taken out and dries, be shaped in adding fertilizer forming machine.Excellent BT biological pesticide can be prepared well by straw is processed, is worthy to be popularized.
Description
Technical field
The present invention relates to biological pesticide technical field, particularly relate to a kind of side preparing Bt biological pesticide with straw for raw material
Method.
Background technology
Straw is the general name of ripe crops stem and leaf (fringe) part.It is often referred to Semen Tritici aestivi, Oryza sativa L., Semen Maydis, potato class, Brassica campestris L, cotton
Flower, Caulis Sacchari sinensis and other crops (usually coarse grain) remainder after results seed.The photosynthetic product of crops has
More than half is present in straw, straw rich in nitrogen, phosphorus, potassium, calcium, magnesium and organic matter etc., be one have multiduty can be again
Raw living resources, straw is also a kind of roughage.Feature is that crude fiber content is high (30%-40%), and containing lignin etc..Wood
Though quality cellulose can not be utilized by pig, chicken, but can be absorbed by domestic animals such as ruminant cattle, sheep and utilize.BT biology agriculture
Medicine, microorganism belonging to genus insecticide, can be used for agricultural and forestry, lepidoptera pest and pine moth are had good prevention effect.Along with
The development of society, the most increasing straw is all incinerated, and the most not only brings the pollution of environment, also results in substantial amounts of
The wasting of resources, therefore devises a kind of method preparing Bt biological pesticide for raw material with straw.
Summary of the invention
For solving technical problem present in background technology, the present invention proposes a kind of to prepare Bt biology agriculture with straw for raw material
The method of medicine, can prepare excellent BT biological pesticide well by being processed straw, can well be applied to agriculture and animal husbandry
In fruit-bearing forest, effectively kill off the insect pests, it is to avoid the environmental pollution that crop straw burning causes, well make use of straw, be worthy to be popularized.
To this end, the invention provides a kind of method preparing Bt biological pesticide for raw material with straw, comprise the following steps:
S1, pretreatment for stalk: after collecting stalk, soak dry in the sun, pretreatment is carried out for stalk, makes
Obtain stalk effective ratio area to increase；
S2, stalk is hydrolyzed into can zymolysis sugar: stalk is added in hydrolytic tank, heat hydrolytic tank to 120 DEG C, keep
Temperature-resistant, add catalyst, solid-to-liquid ratio is 1:3, reacts 3h；
S3, for the solidification of raw material after hydrolysis: after the stalk taking-up that will hydrolyze, after addition solid-state carrier, put into centrifugal
It is stirred in agitator；
S4, the solidification fermentation of straw: the raw material being cured is added in fermentation tank, carries out solidification fermentation；
S5, the molding of fertilizer: the raw material fermented is taken out and dries, be shaped in adding fertilizer forming machine.
Preferably, the method increasing effective ratio area in described step S1 uses chemical method, utilizes mineral acid for straw
Stalk raw material soaking so that in stalk, native cellulose dissolves and degrades, improves stalk digestic property.
Preferably, described step S2 inner catalyst cation resin catalyzing agent, cation resin catalyzing agent surface acidity base
First group contacts with straw, is micromolecular polysaccharide by straw degradative, and micromolecular polysaccharide enters catalytic inner subsequently, drops further
Solve as little molecule monosaccharide.
Preferably, in described step S2, Heating pool heating rate is 12-15 DEG C/min.
Preferably, in described step S3 solid-state carrier be Testa Tritici, Testa oryzae, soybean cake powder, peanut cake powder, expanded perlite and
The one of distiller's grains of beer.
Preferably, in described step S3, centrifugal stirrer rotary speed is 16000-18000r/min.
Preferably, in described step S4, fermentation tank uses pressure fluctuation solid state fermentation tank, and holding pressure is 0.25-
0.32MPa。
Preferably, in described step S5, flash-off time is 24-36h.
A kind of method preparing Bt biological pesticide for raw material with straw that the present invention proposes, increases the side of effective ratio area
Method uses chemical method, utilizes mineral acid to soak for stalk so that in stalk, native cellulose dissolves and degrades, and carries
High stalk digestic property, first cation resin catalyzing agent surface acidic groups contacts with straw, is little by straw degradative
Molecular polysaccharide, micromolecular polysaccharide enters catalytic inner subsequently, is degraded to little molecule monosaccharide further, and fermentation tank uses pressure arteries and veins
Dynamic solid state fermentation tank, greatly reduces the toxicity evaluation of Bt biological pesticide, can prepare well by being processed straw
Go out excellent BT biological pesticide, can well be applied in agriculture and animal husbandry fruit-bearing forest, effectively kill off the insect pests, it is to avoid crop straw burning causes
Environmental pollution, well make use of straw, be worthy to be popularized.
Accompanying drawing explanation
Fig. 1 is the flow chart of a kind of method preparing Bt biological pesticide with straw for raw material of the specific embodiment of the invention.
Detailed description of the invention
Below, by specific embodiment, technical scheme is described in detail.
Embodiment:
With reference to Fig. 1, the present invention proposes a kind of method preparing Bt biological pesticide for raw material with straw, comprises the following steps:
S1, pretreatment for stalk: after collecting stalk, soak dry in the sun, pretreatment is carried out for stalk, makes
Obtain stalk effective ratio area to increase, Physical pretreatment such as mechanical activation comminution, can be well by the fibre in fibrous raw material
Dimension element efflorescence, softening, but this method is when for the process of straw, and effect is poor, here increases effective ratio area
Method use chemical method, utilize mineral acid for stalk soak so that in stalk, native cellulose dissolves and drops
Solve, improve stalk digestic property；
S2, stalk is hydrolyzed into can zymolysis sugar: stalk is added in hydrolytic tank, heat hydrolytic tank to 120 DEG C, keep
Temperature-resistant, add catalyst, solid-to-liquid ratio is 1:3, reacts 3h, catalyst cation resin catalyst, cation resin catalyzing
First agent surface acidic groups contacts with straw, is micromolecular polysaccharide by straw degradative, and micromolecular polysaccharide enters catalyst subsequently
Inside, is degraded to little molecule monosaccharide further, is sugar by the cellulose degradation in stalk, can so that zymolysis afterwards,
Heating pool heating rate is 12-15 DEG C/min；
S3, for the solidification of raw material after hydrolysis: after the stalk taking-up that will hydrolyze, after addition solid-state carrier, put into centrifugal
Being stirred in agitator, solid-state carrier is the one of Testa Tritici, Testa oryzae, soybean cake powder, peanut cake powder, expanded perlite and distiller's grains of beer
Kind, centrifugal stirrer rotary speed is 16000-18000r/min；
S4, the solidification fermentation of straw: being added in fermentation tank by the raw material being cured, carry out solidification fermentation, fermentation tank uses pressure
Pulsation solid state fermentation tank, holding pressure is 0.25-0.32MPa, effectively reduces the toxicity evaluation of Bt biological pesticide；
S5, the molding of fertilizer: being taken out by the raw material fermented and dry, be shaped in adding fertilizer forming machine, flash-off time is
24-36h so that raw material can keep being dried, it is simple to forming machine completes the molding of pesticide.
The method increasing effective ratio area in the present invention uses chemical method, utilizes mineral acid to soak for stalk,
In making stalk, native cellulose dissolves and degrades, and improves stalk digestic property, cation resin catalyzing agent surface
First acidic-group contacts with straw, is micromolecular polysaccharide by straw degradative, and micromolecular polysaccharide enters catalytic inner subsequently, enters
One step is degraded to little molecule monosaccharide, and fermentation tank uses pressure fluctuation solid state fermentation tank, greatly reduces the poison of Bt biological pesticide
Power titer, can prepare excellent BT biological pesticide well by being processed straw, can well be applied to agriculture and animal husbandry fruit
In woods, effectively kill off the insect pests, it is to avoid the environmental pollution that crop straw burning causes, well make use of straw, be worthy to be popularized.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (8)
1. the method preparing Bt biological pesticide for raw material with straw, it is characterised in that comprise the following steps:
S1, pretreatment for stalk: after collecting stalk, soak dry in the sun, pretreatment is carried out for stalk, makes
Obtain stalk effective ratio area to increase；
S2, stalk is hydrolyzed into can zymolysis sugar: stalk is added in hydrolytic tank, heat hydrolytic tank to 120 DEG C, keep
Temperature-resistant, add catalyst, solid-to-liquid ratio is 1:3, reacts 3h；
S3, for the solidification of raw material after hydrolysis: after the stalk taking-up that will hydrolyze, after addition solid-state carrier, put into centrifugal
It is stirred in agitator；
S4, the solidification fermentation of straw: the raw material being cured is added in fermentation tank, carries out solidification fermentation；
S5, the molding of fertilizer: the raw material fermented is taken out and dries, be shaped in adding fertilizer forming machine.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
The method increasing effective ratio area in rapid S1 uses chemical method, utilizes mineral acid to soak for stalk so that straw is former
In material, native cellulose dissolves and degrades, and improves stalk digestic property.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
Rapid S2 inner catalyst cation resin catalyzing agent, first cation resin catalyzing agent surface acidic groups contacts with straw, by straw
Stalk is degraded to micromolecular polysaccharide, and micromolecular polysaccharide enters catalytic inner subsequently, is degraded to little molecule monosaccharide further.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
In rapid S2, Heating pool heating rate is 12-15 DEG C/min.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
In rapid S3, solid-state carrier is the one of Testa Tritici, Testa oryzae, soybean cake powder, peanut cake powder, expanded perlite and distiller's grains of beer.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
In rapid S3, centrifugal stirrer rotary speed is 16000-18000r/min.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
In rapid S4, fermentation tank uses pressure fluctuation solid state fermentation tank, and holding pressure is 0.25-0.32MPa.
A kind of method preparing Bt biological pesticide for raw material with straw, it is characterised in that described step
In rapid S5, flash-off time is 24-36h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610423203.0A CN106083429A (en) | 2016-06-16 | 2016-06-16 | A kind of method preparing Bt biological pesticide for raw material with straw |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610423203.0A CN106083429A (en) | 2016-06-16 | 2016-06-16 | A kind of method preparing Bt biological pesticide for raw material with straw |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106083429A true CN106083429A (en) | 2016-11-09 |
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ID=57846730
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610423203.0A Pending CN106083429A (en) | 2016-06-16 | 2016-06-16 | A kind of method preparing Bt biological pesticide for raw material with straw |
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| CN (1) | CN106083429A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1400194A (en) * | 2001-08-03 | 2003-03-05 | 中国科学院化工冶金研究所 | Method for preparing ecological fertilizer by using steam-puffed plant straw and stalk as raw material through solid fermentation |
| CN1964767A (en) * | 2004-04-13 | 2007-05-16 | 埃欧金能量有限公司 | Recovery of inorganic salt during processing of lignocellulosic feedstocks |
| CN102134616A (en) * | 2011-01-28 | 2011-07-27 | 中国科学院过程工程研究所 | Method for fully utilizing biobased products prepared by semicellulose of straws as well as components thereof |
| CN102553898A (en) * | 2012-02-03 | 2012-07-11 | 刘文治 | Method for realizing resource utilization and zero emission by carrying out chemical catalytic hydrolysis processing on straws |
-
2016
- 2016-06-16 CN CN201610423203.0A patent/CN106083429A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1400194A (en) * | 2001-08-03 | 2003-03-05 | 中国科学院化工冶金研究所 | Method for preparing ecological fertilizer by using steam-puffed plant straw and stalk as raw material through solid fermentation |
| CN1964767A (en) * | 2004-04-13 | 2007-05-16 | 埃欧金能量有限公司 | Recovery of inorganic salt during processing of lignocellulosic feedstocks |
| CN102134616A (en) * | 2011-01-28 | 2011-07-27 | 中国科学院过程工程研究所 | Method for fully utilizing biobased products prepared by semicellulose of straws as well as components thereof |
| CN102553898A (en) * | 2012-02-03 | 2012-07-11 | 刘文治 | Method for realizing resource utilization and zero emission by carrying out chemical catalytic hydrolysis processing on straws |
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Application publication date: 20161109 |