CN106074241B - A kind of preparation method of activity aloe water - Google Patents
A kind of preparation method of activity aloe water Download PDFInfo
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- CN106074241B CN106074241B CN201610432765.1A CN201610432765A CN106074241B CN 106074241 B CN106074241 B CN 106074241B CN 201610432765 A CN201610432765 A CN 201610432765A CN 106074241 B CN106074241 B CN 106074241B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The present invention discloses a kind of preparation method of active aloe water, and aloe leaf is cleaned, peeling, crushing, sterilization, enzymatic hydrolysis, plate-frame filtering are made Aloe gel juice, then remove anthraquinone, pigment by macroporous anion exchange resin column；Then it is filtered with the microfiltration membranes that molecular cut off is 200,000, collects filtered fluid, then be filtered with the nanofiltration membrane that molecular cut off is 0.05 ten thousand, collect dialyzate, routinely carry out pasteurization, then cooling obtains active aloe water.The present invention can obtain molecular weight distribution 1000~10000 specified molecular weight section asparagus juice；Method of the invention is easy manipulation, and the resin used can be recycled, be reduced environmental pollution；Meanwhile being extracted using nanofiltration, product yield is high, reduces production cost.
Description
Technical field
The present invention relates to a kind of preparation methods of active aloe water, belong to plant processing technique field.
Background technique
Aloe is the evergreen herbage of Liliaceae, Aloe, with originating in Mediterranean and African, american torrid zone
Area is also distributed in Yunnan Province of China.Aloe is a kind of ancient, traditional conventional Chinese medicine, no matter in traditional medicine or modern times
In medicine, the medical value of aloe has all been affirmed, this has specific note in the medical book and modern drug encyclopedia in China's one's early years
It carries.Aloe has biggish application in fields such as cosmetics, food, health care products in recent years.
With the further exploitation of aloe food, aloe health product, aloe cosmetics, especially answering in cosmetic field
With having higher requirement to the quality of aloe products, especially have higher standard requirements to the molecular weight distribution of asparagus juice.
As some transdermal, infiltration, deep layer reparation cosmetics, molecular weight distribution has extraordinary infiltration to imitate at 1000~10000
Fruit.
Summary of the invention
It repairs in cosmetics and applies to meet Aloe gel juice in infiltration, deep layer, the purpose of the present invention is to provide one kind
The preparation method of active aloe water utilizes resin, micro-filtration, nanofiltration Combined machining activity aloe water.
The present invention is realized by following technical proposal: a kind of preparation method of activity aloe water, by following each step:
A, aloe leaf is cleaned, peeling, crushing, sterilization, enzymatic hydrolysis, the obtained soluble solid of plate-frame filtering are 0.5
~1.25% Aloe gel juice；
B, by macroporous anion exchange resin=10 Lu Hui gel juice ︰~15 ︰ 1 volume ratio, aloe obtained by step A is coagulated
Glue juice controls 15~25min of time of contact by macroporous anion exchange resin column to get the aloe of removal anthraquinone, pigment is arrived
Gel juice I；
C, the microfiltration membranes for being 200,000 with molecular cut off are filtered Aloe gel juice I obtained by step B, collect filtering
Liquid obtains Aloe gel juice II；
D, the nanofiltration membrane for being 0.05 ten thousand with molecular cut off is filtered Aloe gel juice II obtained by step C, collects saturating
Liquid is analysed, the active asparagus juice of small molecule is obtained；
E, by active asparagus juice obtained by step D, pasteurization is routinely carried out, is cooled back to 25 DEG C hereinafter, through sterile filling
It fills to get active aloe water is arrived.
The large pore anion resin of the step B is commercially available technical grade product.
The microfiltration membranes that the molecular cut off of the step C is 200,000 are commercially available technical grade product.
The nanofiltration membrane that the molecular cut off of the step D is 0.05 ten thousand is commercially available technical grade product.
The step E be pasteurization condition be temperature be 80~85 DEG C, the time be 10~30s.
The advantages of present invention has and effect: the present invention is completed using primary ion exchange adsorption, micro-filtration, nanofiltration combination
Aloe gel juice is made through plate-frame filtering, sterilization in aloe gel juice by the production of active aloe water；Gained Aloe gel juice
Active aloe water is made through ion exchange adsorption, micro-filtration, nanofiltration.Microfiltration membranes have clarification, go deimpurity effect；Nanofiltration retention
Macromolecular pectin, protein in aloe, are applied in combination by microfiltration membranes, nanofiltration membrane, remove macromolecular pectin, egg in aloe
White matter, obtain molecular weight distribution 1000~10000 specified molecular weight section asparagus juice；Ion exchange resin has very high
Power of regeneration and excellent antifouling property, can recycle, reduce environmental pollution.Method of the invention is easy manipulation, makes
Resin can recycle, and reduce environmental pollution；Meanwhile being extracted using nanofiltration, product yield is high, reduces and is produced into
This.
Specific embodiment
The present invention is described further below with reference to embodiment.
Embodiment 1
A, 40 tons of aloe leafs are cleaned, peeling, crushing, sterilization, enzymatic hydrolysis, plate-frame filtering are made soluble solid and are
18.4 tons of 1% Aloe gel juice；
B, by Lu Hui gel juice ︰ macroporous anion exchange resin=10 ︰ 1 volume ratio, by Aloe gel juice obtained by step A
By macroporous anion exchange resin column, time of contact 20min is controlled to get the Aloe gel juice I of removal anthraquinone, pigment is arrived；
C, the microfiltration membranes for being 200,000 with molecular cut off are filtered Aloe gel juice I obtained by step B, collect filtering
Liquid obtains 17.9 tons of transparent, clear Aloe gel juices II, soluble solid 1%；
D, the nanofiltration membrane for being 0.05 ten thousand with molecular cut off is filtered Aloe gel juice II obtained by step C, collects saturating
Liquid is analysed, the active asparagus juice of 15.2 tons of small molecules, soluble solid 0.25% are obtained；
E, by active asparagus juice obtained by step D, pasteurization 20s is carried out at being routinely 82 DEG C in temperature, is cooled back to
25 DEG C hereinafter, through sterile filling to get to active aloe water.
The active aloe molecular weight water of table 1 and molecular weight distribution detect table
Embodiment 2
A, 25 tons of aloe leafs are cleaned, peeling, crushing, sterilization, enzymatic hydrolysis, plate-frame filtering are made soluble solid and are
11.4 tons of 1~1.25% Aloe gel juice；
B, by Lu Hui gel juice ︰ macroporous anion exchange resin=15 ︰ 1 volume ratio, by Aloe gel juice obtained by step A
By macroporous anion exchange resin column, time of contact 25min is controlled to get the Aloe gel juice I of removal anthraquinone, pigment is arrived；
C, the microfiltration membranes for being 200,000 with molecular cut off are filtered Aloe gel juice I obtained by step B, collect filtering
Liquid obtains 10.6 tons of transparent, clear Aloe gel juices II；
D, the nanofiltration membrane for being 0.05 ten thousand with molecular cut off is filtered Aloe gel juice II obtained by step C, collects saturating
Liquid is analysed, 8.6 tons of small molecule active asparagus juices, soluble solid 0.5% are obtained；
E, by active asparagus juice obtained by step D, pasteurization 30s is carried out at being routinely 80 DEG C in temperature, is cooled back to
25 DEG C hereinafter, through sterile filling to get to active aloe water.
The active aloe molecular weight water of table 2 and molecular weight distribution detect table
Embodiment 3
A, 50 tons of aloe leafs are cleaned, peeling, crushing, sterilization, enzymatic hydrolysis, plate-frame filtering are made soluble solid and are
21.3 tons of 0.5~0.75% Aloe gel juice；
B, by Lu Hui gel juice ︰ macroporous anion exchange resin=12 ︰ 1 volume ratio, by Aloe gel juice obtained by step A
By macroporous anion exchange resin column, time of contact 15min is controlled to get the Aloe gel juice I of removal anthraquinone, pigment is arrived；
C, the microfiltration membranes for being 200,000 with molecular cut off are filtered Aloe gel juice I obtained by step B, collect filtering
Liquid obtains 20.2 tons of transparent, clear Aloe gel juices II, soluble solid 0.75%；
D, the nanofiltration membrane for being 0.05 ten thousand with molecular cut off is filtered Aloe gel juice II obtained by step C, collects saturating
Liquid is analysed, 16.2 tons of small molecule active asparagus juices, soluble solid 0.25% are obtained；
E, by active asparagus juice obtained by step D, pasteurization 10s is carried out at being routinely 85 DEG C in temperature, is cooled back to
25 DEG C hereinafter, through sterile filling to get to active aloe water.
The active aloe molecular weight water of table 3 and molecular weight distribution detect table
Claims (5)
1. a kind of preparation method of activity aloe water, it is characterised in that pass through following each step:
A, aloe leaf is cleaned, peeling, crush, sterilization, enzymatic hydrolysis, plate-frame filtering be made soluble solid be 0.5~
1.25% Aloe gel juice；
B, by macroporous anion exchange resin=10 Lu Hui gel juice ︰~15 ︰ 1 volume ratio, by Aloe gel juice obtained by step A
By macroporous anion exchange resin column, 15~25min of time of contact is controlled to get the aloe gel of removal anthraquinone, pigment is arrived
Juice I；
C, the microfiltration membranes for being 200,000 with molecular cut off are filtered Aloe gel juice I obtained by step B, collect filtered fluid, obtain
To Aloe gel juice II；
D, the nanofiltration membrane for being 0.05 ten thousand with molecular cut off is filtered Aloe gel juice II obtained by step C, collects dialyzate,
Obtain the active asparagus juice of small molecule；
E, by active asparagus juice obtained by step D, pasteurization is routinely carried out, is cooled back to 25 DEG C hereinafter, through sterile filling, i.e.,
Obtain molecular weight distribution 1000~10000 specified molecular weight section active aloe water.
2. it is according to claim 1 activity aloe water preparation method, it is characterised in that: the macropore yin of the step B from
Subtree rouge is commercially available technical grade product.
3. the preparation method of activity aloe water according to claim 1, it is characterised in that: the retention molecule of the step C
Amount is commercially available technical grade product for 200,000 microfiltration membranes.
4. the preparation method of activity aloe water according to claim 1, it is characterised in that: the retention molecule of the step D
Amount is commercially available technical grade product for 0.05 ten thousand nanofiltration membrane.
5. the preparation method of activity aloe water according to claim 1, it is characterised in that: the step E is pasteurization
Condition be temperature be 80~85 DEG C, the time be 10~30s.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610432765.1A CN106074241B (en) | 2016-06-17 | 2016-06-17 | A kind of preparation method of activity aloe water |
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| CN201610432765.1A CN106074241B (en) | 2016-06-17 | 2016-06-17 | A kind of preparation method of activity aloe water |
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| CN106074241A CN106074241A (en) | 2016-11-09 |
| CN106074241B true CN106074241B (en) | 2019-02-19 |
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| CN110384653A (en) * | 2019-09-06 | 2019-10-29 | 奢脉国际化妆品(北京)有限公司 | It is a kind of to have effects that the multi-faceted polypeptide Essence for dispelling yellow and its preparation process |
| CN112655856A (en) * | 2020-12-02 | 2021-04-16 | 云南万绿生物股份有限公司 | Preparation method of aloe gel beverage |
| CN115737511A (en) * | 2022-05-19 | 2023-03-07 | 云南万绿生物股份有限公司 | Method for obtaining aloe flower extract, aloe flower emulsion and device |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824287A (en) * | 2012-09-07 | 2012-12-19 | 云南万绿生物股份有限公司 | Method for removing calcium and magnesium in aloe gel juice |
| CN104693314A (en) * | 2015-03-16 | 2015-06-10 | 云南万绿生物股份有限公司 | Processing method for 2000: 1 aloe gel dry powder |
| CN104738746A (en) * | 2015-03-26 | 2015-07-01 | 云南万绿生物股份有限公司 | Method for processing small molecular active aloe juice |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824287A (en) * | 2012-09-07 | 2012-12-19 | 云南万绿生物股份有限公司 | Method for removing calcium and magnesium in aloe gel juice |
| CN104693314A (en) * | 2015-03-16 | 2015-06-10 | 云南万绿生物股份有限公司 | Processing method for 2000: 1 aloe gel dry powder |
| CN104738746A (en) * | 2015-03-26 | 2015-07-01 | 云南万绿生物股份有限公司 | Method for processing small molecular active aloe juice |
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