CN106047093A - 纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法 - Google Patents
纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法 Download PDFInfo
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Abstract
纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，包括灯罩壳体，所述灯罩壳体包括基层和功能涂层，所述基层和功能涂层自内而外依次排列，所述功能涂层完全包覆基层的外表面，所述功能涂层包括活性矿物质粉和中药精油成分，本发明不仅具有驱赶蚊虫的功效，还可以释放负离子，具有一定的去除甲醛、甲苯和TVOC等污染物的功能，同时气味芳香，性质温和，丰富了传统灯具的使用功能。
Description
技术领域
本发明涉及照明灯具领域，尤其涉及一种纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法。
背景技术
随着社会的发展和进步，人们的绿色环保观念越来越强，因而绿色环保的照明装置会更受到人们的青睐，日渐成熟的LED技术由于其具有高效、节能、环保、使用寿命长、功率低等优点，LED照明灯已经逐渐开始取代传统的照明灯具。
一方面，随着全球气温的不断升高，蚊子的种群和数量都将大幅提高，正日益威胁人类的健康。蚊子除直接叮刺吸血、骚扰睡眠外，更严重的是传播多种疾病。我国的蚊传病有疟疾、淋巴丝虫病、流行性乙型脑炎和登革热（或登革出血热）四类，蚊传较重要的病毒病还有黄热病及各种马脑炎等。
另一方面，将空气负离子技术运用于节能灯产品中，使用后的节能灯在室内长期释放空气负离子，尤其是负氧离子。由于其在结构上与超氧阴离子自由基相似，因此具有相似的生物活性，能够使活的生物细胞带负电荷，从而使病毒失去对细胞的攻击能力；同时，负氧离子能够和甲醛、甲苯、TVOC等装修污染物发生反应，产物为无毒无味的二氧化碳和水，无二次污染的产生，具有一定的净化室内空气的功效，例如，在人造空气负离子环境中，经测定空气中霉菌、细菌数可降低90％以上。负氧离子被吸入人体后，能调节神经中枢的兴奋状态，改善肺的换气功能，改善血液循环，促进新陈代谢、增强免疫系统能力、使人精神振奋、提高工作效率等，它还对高血压、气喘、流感、失眠、关节炎等许多疾病有一定的治疗作用，所以人称负离子为“空气中的维生素”“长寿素”。
迄今，使传统灯具产品同时具有驱蚊虫以及释放负离子功能的技术设计还未有见。
发明内容
针对现有技术存在的不足，本发明所要解决的技术问题是提供纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，不仅长期释放负离子，还具有一定的驱赶蚊虫功效，同时也具有一定的抗菌作用，具有一举多得的效果。
本发明的目的是通过如下技术方案实现的：
纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，所述的LED灯罩包括灯罩壳体，所述灯罩壳体包括基层和功能涂层，所述基层和功能涂层自内而外依次排列，所述功能涂层完全包覆灯罩基层的外表面，所述功能涂层由下列组份按照重量份数组成：环保树脂15-25重量份；阻燃剂3-6重量份；改性芳香胺固化剂2-3.5重量份；纳米荧光粉0.1-0.2重量份；汽巴艳佳固754光引发剂1.5-3重量份；聚醚胺催化剂0.5-0.7重量份；羟乙基纤维素2-3重量份；二氧化铈0.1-0.15重量份；活性矿物质粉0.75-1.3重量份；中药精油0.6-1.1重量份；其中，所述环保树脂为环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的混合物，所述环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的质量比为1.5:1，所述阻燃剂为多聚磷酸铵、三聚氰胺以及膨胀型石墨的混合物，所述多聚磷酸铵、三聚氰胺以及膨胀型石墨的质量比1.5:1.2:1，所述的纳米荧光粉为Ce和YAG的混合物，所述纳米荧光粉的粒径≤13μm，所述的活性矿物质粉为锗石、萤石、电气石、六环石按重量比2.5：3：3.7：2的混合物，其中电气石为镁电气石和锂电气石按重量比5：3的混合物，所述活性矿物质粉的粒径≤13μm，所述功能涂层通过如下步骤制备而成：
S1、将所需重量份数的环保树脂、阻燃剂、纳米荧光粉、羟乙基纤维素、汽巴艳佳固754光引发剂以及聚醚胺催化剂置于搅拌机中，在65-85℃下集中高速搅拌调匀，搅拌时间为15-30分钟，待混合均匀后从搅拌机中取出，即制得混合物A，备用；
S2、将物料打破碗花花65-85重量份，大青叶15-20重量份，贯众4-6重量份，普洱茶4-6重量份，丁香罗勒1.5-2.5重量份，柴胡1-3重量份，芦荟1-3重量份，黄柏1-3重量份，连翘1-3重量份以及白芍药1-3重量份去杂质，一起置于-20℃的真空釜2-3小时，然后再置于微波干燥机进行预处理，其中干燥时间为30-40分钟，微波功率为17kw；
S3、将步骤S2处理后的物料一起投入超微粉碎机中粉碎至60目，制得原料药粉末，备用；
S4、将步骤S3中制得的原料药粉末投入超临界二氧化碳萃取装置的萃取釜中，调节萃取压力28MPa，萃取温度45℃，二氧化碳流量为1100L/h，动态萃取2小时，直接在分离釜出口用三角瓶收集粗油，备用；
S5、将步骤S4中制得的粗油置于5℃环境中冷冻70分钟，再将冷冻后的粗油置于转速为17000r/min的高速冷冻离心机中离心25分钟，去除杂质后置于85℃真空箱抽真空3小时，即制得挥发油B，备用；
S6、将麝香0.6-1重量份，马齿苋3-4重量份，丹参3-4重量份，辣蓼草3-4重量份，百部7-9重量份，藿香3-4重量份，狼毒3-4重量份，栀子3-4重量份，板蓝根15-18重量份以及酸枣仁3-4重量份洗净烘干，一起投入超微粉碎机中粉碎至30目，然后加去离子水浸泡5小时，加水量为所浸泡原料药质量的7倍，搅拌分散调匀，制得中药混合物，备用；
S7、将步骤S6制得的中药混合物于80℃煎煮2小时，收集蒸馏液，并加入乙醚萃取，蒸馏液与乙醚的体积比为2.5:1，取上层油相，然后加无水硫酸钠0.1-0.25重量份进行干燥处理，即制得挥发油C，备用；
S8、将步骤S5和S7所制挥发油B和挥发油C混合调匀制得混合油，再边搅拌边依次加入薄荷精油、玫瑰精油、番红花精油和杜松精油，充分搅拌45分钟，静置30分钟，过滤除杂，即得中药精油，其中，所述混合油与薄荷精油、玫瑰精油、番红花精油和杜松精油的质量比为2：0.5：0.4：0.6：0.5；
S9、将步骤S8制得的中药精油与步骤S1制得的混合物A，在70-80℃下，在搅拌机中集中搅拌混合15分钟，得到预混料，然后在预混料中加入二氧化铈、活性矿物质粉以及改性芳香胺固化剂，在65-85℃下，集中搅拌35分钟后，然后浇铸在基层的外表面，固化脱模，即得功能涂层。
在一较佳实施例中，在步骤S8中的中药精油还包括以下重量份的组分：表面活性剂1.7份、避蚊胺0.2份、丁酸丁酯1份、桉树油1.2份、醋酸氯已定0.5份、脂肪醇聚氧乙烯醚硫酸钠1份和苯甲酸钠0.2份。
一种LED灯具，所述LED灯具包括LED照明组件、底座以及通过上述方法制备的灯罩A。
需要说明的是，经实验证明，在活性矿物质粉中加入适量的二氧化铈（CeO2），利用该稀土元素的辐射能量高，半衰减期限长的特点，可以大幅增加活性矿物质粉的负离子产率，其原理如下：二氧化铈中的Ce4+在光照环境下转化成Ce3+，在转化过程中，电子-空穴的复合几率降低，再在活性矿物质粉中电气石等物质电场的作用下，部分电子被动随电场方向定向移动，电子-空穴复合几率降低，从而在电气石/ CeO2复合粉末表面积聚了大量的电解空气分子的能量，进而产生了高浓度的空气负离子，同时Ce3+又氧化成为Ce4+，继而重复前述的转化过程；同时，经实践检测，在经过本发明复合配比的活性矿物质粉中添加二氧化铈组分，比未经添加二氧化铈的活性矿物质粉负离子的浓度高10倍以上，r射线与自然环境相同。
本发明基于祖国传统医学，参考现代中药药理研究，从现有中药的药物筛选和反复验证，充分发挥各组份协同作用，其中主要原料的作用简介如下。
打破碗花花：①《陕西中草药》：“苦,凉,有小毒。”②《四川常用中草药》：“苦辛,温,有小毒。”解毒,排脓生肌,消肿散瘀,具有杀蛆虫、孑孓,化积,消肿,散瘀,治顽癣,秃疮,疟疾,小儿疳积,痢疾,痈疖疮肿,瘰疬,跌打损伤。
大青叶：对金黄色葡萄球菌、甲型链球菌、脑膜炎双球菌、肺炎链球菌、卡他球菌、伤寒杆菌、大肠杆菌、流感杆菌、白喉杆菌及痢疾杆菌有一定抑制作用；大青叶对乙型脑炎病毒、腮腺炎病毒、流感病毒等也有抑制作用．此外大青叶有杀灭钩端螺旋体的作用。
贯众：苦微寒,归肝脾经,有小毒。杀虫,清热解毒,止血。
普洱茶：云南独有大叶种茶树所产的茶,具有抑菌消炎、抗毒、灭菌、预防便秘等。
丁香罗勒:辛,温,具有驱蚊,发汗解表,祛风利湿,散瘀止痛的功效。
柴胡: 和解少阳,舒肝和胃,升阳举陷。治寒热往来,胸满胁痛,口苦耳聋,头痛目眩,疟疾,下利脱肛,月经不调,子宫下垂,热入血室。
芦荟：《本草经疏》：芦荟,寒能除热,苦能泄热燥湿,苦能杀虫,至苦至寒,故为除热杀虫之要药。其主热风烦闷,胸胁间热气,明目,镇心,小儿癫痫凉风,疗五疳,杀三虫者,热则生风,热能使人烦闷,热除则风热烦闷及胸膈间热气自解。
黄柏：对金黄色葡萄球菌、肺炎球菌、白喉杆菌、草绿色链球菌、痢疾杆菌（宋内氏除外）、溶血性链球菌、脑膜炎球菌、霍乱弧菌、炭疽杆菌均有效或有较强的抑制作用；对枯草杆菌、百日咳杆菌、破伤风杆菌亦有抑制作用。
连翘：清热解毒,消肿散结,疏散风热,有“疮家圣药”之称,可抑制伤寒杆菌、副伤寒杆菌、大肠杆菌、痢疾杆菌、白喉杆菌及霍乱弧菌、葡萄球菌、链球菌等。
白芍药：其中芍药甙有抗菌、解热、抗炎、增加冠状动脉流量、改善心肌营养血流、扩张血管、对抗急性心肌缺血、抑制血小板聚集、镇静、镇痛、解痉、抗溃疡、调节血糖的作用。白芍煎剂能抑制痢疾杆菌、肺炎链球菌、大肠杆菌、伤寒杆菌、溶血性链球菌、绿脓杆菌等。
麝香: 具有开窍,辟秽,通络,散瘀的功效；治中风,痰厥,惊痫,中恶烦闷,心腹暴痛,癥瘕癖积,跌打损伤,痈疽肿毒。《本经》：主辟恶气,温疟,痫痉,去三虫。
马齿苋：马齿苋科一年生草本植物。肥厚多汁,无毛,高10-30cm, 生于田野路边及庭园废墟等向阳处。国内各地均有分布。该种为药食两用植物。全草供药用,有清热利湿、解毒消肿、消炎、止渴、利尿作用。
丹参：性味苦,微寒。归心、肝经。《滇南本草》记载：补心定志,安神宁心。治健忘怔冲,惊悸不寐,有祛瘀止痛,活血通经,清心除烦之功效,用于月经不调,经闭痛经,症瘕积聚,胸腹刺痛,热痹疼痛,疮疡。
辣蓼草：对各种痢疾杆菌于试管内均有抑制作用,现代临床医学研究表明,辣蓼具有抗菌、抗病毒、抗炎、抗氧化等功效。
百部：可驱除蚊虫,抗病原微生物作用,对乙型溶血性链球菌、脑膜炎球菌、金黄色葡萄球菌、白色葡萄球菌、伤寒杆菌、肺炎杆菌、鼠疫杆菌、炭疽杆菌等多种致病真菌有一定的抑制作用,其水浸液对蚊蝇幼虫、头虱、衣虱及臭虫等均有杀灭作用。
藿香：味辛,性微温。功效：化湿和中,解表、解署的功效,主治湿阻脾胃,胸脘闷胀,食欲不香,恶心、呕吐；夏季暑湿困倦,胸闷不舒,以及外感风寒.恶寒胸闷等病症,具有有较强的抑制真菌作用和抗菌作用。
狼毒：别名川狼毒、续毒、绵大戟、山萝卜、闷花头、热加巴、一扫光、搜山虎、一把香、药罗卜、生扯拢、红火柴头花、猴子根、断肠草,中医学上用其根祛痰、止痛、消积、杀虫。
栀子：其果实是传统中药,属卫生部颁布的第l批药食两用资源,具有护肝、利胆、降压、镇静、止血、消肿等作用,对白喉杆菌、金黄色葡萄球菌、伤寒杆菌有抑制作用,对多种皮肤真菌也有不同程度的抑制作用。
板蓝根：对多种细菌有抑制作用,水浸液对枯草杆菌、金黄色葡萄球菌、八联球菌、大肠杆菌、伤寒杆菌、副伤寒杆菌、痢疾（志贺、弗氏）杆菌、肠炎杆菌等都有不同程度的抑制作用；丙酮浸出液也有类似作用, 且对溶血性链球菌有效。
酸枣仁:有显著的镇静和催眠作用以及抗惊厥作用,据《本草再新》记载：平肝理气,润肺养阴,温中利湿,敛气止汗,益志,聪耳明目。
需要说明的是，经实践证明，将一定重量份的丹参、辣蓼草和百部进行复配后，不仅可显著提高除菌抗菌的能力，还会产生一种无毒副作用的清香味道，沁人心脾，具有一定的提神效果；同时，经实践证明，将一定重量份的大青叶、普洱茶、芦荟、麝香和打破碗花花进行复配后，使该组合物的驱蚊虫能力得到显著提高；另外，柴胡、黄柏和连翘等组分进行配伍后，大大提高了组合物的抗菌除菌能力，经实践检测，复配后的组合物对金黄色葡萄球菌、炭疽杆菌、流感杆菌、卡他球菌、肺炎球菌、大肠杆菌、乙型链球菌、白喉杆菌、伤寒杆菌、绿脓肝菌、痢疾杆菌等30余种病菌具有一定的抑制和杀灭作用，使本发明具有了一定的抗菌除菌能力。
本发明的效果：
本发明采用中药与活性矿物质复配，使本发明不仅可以驱赶蚊虫，还可以释放负离子，清新空气，同时气味芳香，性质温和，具有健身、驱蚊、防霉杀菌的功效。
附图说明
图1是本发明整体示意图。
图2是本发明灯罩壳体截面示意图。
具体实施方式
实施例1：
请参见图1、图2所示，纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，所述的LED灯罩包括灯罩壳体A，所述灯罩壳体A包括基层1和功能涂层2，所述基层1和功能涂层2自内而外依次排列，所述功能涂层2完全包覆灯罩基层1的外表面，所述功能涂层2由下列组份按照重量份数组成：
环保树脂15重量份；阻燃剂6重量份；改性芳香胺固化剂2重量份；纳米荧光粉0.2重量份；汽巴艳佳固754光引发剂1.5重量份；聚醚胺催化剂0.7重量份；羟乙基纤维素2重量份；二氧化铈0.15重量份；活性矿物质粉0.75重量份；中药精油1.1重量份；其中，所述环保树脂为环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的混合物，所述环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的质量比为1.5:1，所述阻燃剂为多聚磷酸铵、三聚氰胺以及膨胀型石墨的混合物，所述多聚磷酸铵、三聚氰胺以及膨胀型石墨的质量比1.5:1.2:1，所述的纳米荧光粉为Ce和YAG的混合物，所述纳米荧光粉的粒径≤13μm，所述的活性矿物质粉为锗石、萤石、电气石、六环石按重量比2.5：3：3.7：2的混合物，其中电气石为镁电气石和锂电气石按重量比5：3的混合物，所述活性矿物质粉的粒径≤13μm，所述功能涂层通过如下步骤制备而成：
S1、将所需重量份数的环保树脂、阻燃剂、纳米荧光粉、羟乙基纤维素、汽巴艳佳固754光引发剂以及聚醚胺催化剂置于搅拌机中，在65℃下集中高速搅拌调匀，搅拌时间为30分钟，待混合均匀后从搅拌机中取出，即制得混合物A，备用；
S2、将物料打破碗花花85重量份，大青叶15重量份，贯众6重量份，普洱茶4重量份，丁香罗勒2.5重量份，柴胡1重量份，芦荟3重量份，黄柏1重量份，连翘3重量份，白芍药1重量份去杂质，一起置于-20℃的真空釜2小时，然后再置于微波干燥机进行预处理，其中干燥时间为40分钟，微波功率为17kw；
S3、将步骤S2处理后的物料一起投入超微粉碎机中粉碎至60目，制得原料药粉末，备用；
S4、将步骤S3中制得的原料药粉末投入超临界二氧化碳萃取装置的萃取釜中，调节萃取压力28MPa，萃取温度45℃，二氧化碳流量为1100L/h，动态萃取2小时，直接在分离釜出口用三角瓶收集粗油，备用；
S5、将步骤S4中制得的粗油置于5℃环境中冷冻70分钟，再将冷冻后的粗油置于转速为17000r/min的高速冷冻离心机中离心25分钟，去除杂质后置于85℃真空箱抽真空3小时，即制得挥发油B，备用；
S6、将麝香1重量份，马齿苋3重量份，丹参4重量份，辣蓼草3重量份，百部9重量份，藿香3重量份，狼毒4重量份，栀子3重量份，板蓝根18重量份，酸枣仁3重量份洗净烘干，一起投入超微粉碎机中粉碎至30目，然后加去离子水浸泡5小时，加水量为所浸泡原料药质量的7倍，搅拌分散调匀，制得中药混合物，备用；
S7、将步骤S6制得的中药混合物于80℃煎煮2小时，收集蒸馏液，并加入乙醚萃取，蒸馏液与乙醚的体积比为2.5:1，取上层油相，然后加无水硫酸钠0.1重量份进行干燥处理，即制得挥发油C，备用；
S8、将步骤S5和S7所制挥发油B和挥发油C混合调匀制得混合油，再边搅拌边依次加入薄荷精油、玫瑰精油、番红花精油和杜松精油，充分搅拌45分钟，静置30分钟，过滤除杂，即得中药精油，其中，所述混合油与薄荷精油、玫瑰精油、番红花精油和杜松精油的质量比为2：0.5：0.4：0.6：0.5；
S9、将步骤S8制得的中药精油与步骤S1制得的混合物A，在70℃下，在搅拌机中集中搅拌混合15分钟，得到预混料，然后在预混料中加入二氧化铈、活性矿物质粉以及改性芳香胺固化剂，在65℃下，集中搅拌35分钟后，然后浇铸在基层的外表面，固化脱模，即得功能涂层。
在一较佳实施例中，在步骤S8中的中药精油还包括以下重量份的组分：表面活性剂1.7份、避蚊胺0.2份、丁酸丁酯1份、桉树油1.2份、醋酸氯已定0.5份、脂肪醇聚氧乙烯醚硫酸钠1份和苯甲酸钠0.2份。
一种LED灯具，所述LED灯具包括LED照明组件、底座以及通过上述方法制备的灯罩A。
实施例2：
纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，所述的LED灯罩包括灯罩壳体A，所述灯罩壳体A包括基层1和功能涂层2，所述基层1和功能涂层2自内而外依次排列，所述功能涂层2完全包覆灯罩基层1的外表面，所述功能涂层2由下列组份按照重量份数组成：
环保树脂19重量份；阻燃剂5重量份；改性芳香胺固化剂3重量份；纳米荧光粉0.15重量份；汽巴艳佳固754光引发剂2重量份；聚醚胺催化剂0.6重量份；羟乙基纤维素2.5重量份；二氧化铈0.15重量份；活性矿物质粉1重量份；中药精油1重量份；其中，所述环保树脂为环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的混合物，所述环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的质量比为1.5:1，所述阻燃剂为多聚磷酸铵、三聚氰胺以及膨胀型石墨的混合物，所述多聚磷酸铵、三聚氰胺以及膨胀型石墨的质量比1.5:1.2:1，所述的纳米荧光粉为Ce和YAG的混合物，所述纳米荧光粉的粒径≤13μm，所述的活性矿物质粉为锗石、萤石、电气石、六环石按重量比2.5：3：3.7：2的混合物，其中电气石为镁电气石和锂电气石按重量比5：3的混合物，所述活性矿物质粉的粒径≤13μm，所述功能涂层通过如下步骤制备而成：
S1、将所需重量份数的环保树脂、阻燃剂、纳米荧光粉、羟乙基纤维素、汽巴艳佳固754光引发剂以及聚醚胺催化剂置于搅拌机中，在75℃下集中高速搅拌调匀，搅拌时间为25分钟，待混合均匀后从搅拌机中取出，即制得混合物A，备用；
S2、将物料打破碗花花65-重量份，大青叶20重量份，贯众4重量份，普洱茶6重量份，丁香罗勒1.5重量份，柴胡13重量份，芦荟1重量份，黄柏3重量份，连翘1重量份，白芍药3重量份去杂质，一起置于-20℃的真空釜2.5小时，然后再置于微波干燥机进行预处理，其中干燥时间为35分钟，微波功率为17kw；
S3、将步骤S2处理后的物料一起投入超微粉碎机中粉碎至60目，制得原料药粉末，备用；
S4、将步骤S3中制得的原料药粉末投入超临界二氧化碳萃取装置的萃取釜中，调节萃取压力28MPa，萃取温度45℃，二氧化碳流量为1100L/h，动态萃取2小时，直接在分离釜出口用三角瓶收集粗油，备用；
S5、将步骤S4中制得的粗油置于5℃环境中冷冻70分钟，再将冷冻后的粗油置于转速为17000r/min的高速冷冻离心机中离心25分钟，去除杂质后置于85℃真空箱抽真空3小时，即制得挥发油B，备用；
S6、将麝香0.6重量份，马齿苋4重量份，丹参3重量份，辣蓼草4重量份，百部7重量份，藿香4重量份，狼毒3重量份，栀子4重量份，板蓝根15重量份，酸枣仁4重量份洗净烘干，一起投入超微粉碎机中粉碎至30目，然后加去离子水浸泡5小时，加水量为所浸泡原料药质量的7倍，搅拌分散调匀，制得中药混合物，备用；
S7、将步骤S6制得的中药混合物于80℃煎煮2小时，收集蒸馏液，并加入乙醚萃取，蒸馏液与乙醚的体积比为2.5:1，取上层油相，然后加无水硫酸钠0.2重量份进行干燥处理，即制得挥发油C，备用；
S8、将步骤S5和S7所制挥发油B和挥发油C混合调匀制得混合油，再边搅拌边依次加入薄荷精油、玫瑰精油、番红花精油和杜松精油，充分搅拌45分钟，静置30分钟，过滤除杂，即得中药精油，其中，所述混合油与薄荷精油、玫瑰精油、番红花精油和杜松精油的质量比为2：0.5：0.4：0.6：0.5；
S9、将步骤S8制得的中药精油与步骤S1制得的混合物A，在75℃下，在搅拌机中集中搅拌混合15分钟，得到预混料，然后在预混料中加入二氧化铈、活性矿物质粉以及改性芳香胺固化剂，在75℃下，集中搅拌35分钟后，然后浇铸在基层的外表面，固化脱模，即得功能涂层。
其余同实施例1。
本发明实施例1和实施例2的测试指标如下：
（1）气味检查：感官，无刺激性异味。
（2）驱蚊效果测试。
依据现有技术中的普通灯具与上述实施例1和实施例2的驱蚊效果进行对比测试，测试数据请见表1。
结论：本发明实施例1和实施例2均能起到较好的驱蚊作用，与市场上普通灯具
相比较，本发明具有非常明显的驱蚊效果。
（3）负离子检测。
采用负离子测试仪器，主要是针对木材、矿石、陶瓷材料、负离子粉末与相关制成商品（如负离子衣物、项链、毛毯）等所释放出的负离子数量做出测量，测试结果见表2。
结论：本发明实施例1、实施例2可以持续释放空气负离子，与现有技术中的普通灯具相比较，本发明具有非常明显的优势。
Claims (2)
1.纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，其特征在于：所述的LED灯罩包括灯罩壳体（A），所述灯罩壳体（A）包括基层（1）和功能涂层（2），所述基层（1）和功能涂层（2）自内而外依次排列，所述功能涂层（2）完全包覆灯罩基层（1）的外表面，所述功能涂层（2）由下列组份按照重量份数组成：
环保树脂15-25重量份；阻燃剂3-6重量份；改性芳香胺固化剂2-3.5重量份；纳米荧光粉0.1-0.2重量份；汽巴艳佳固754光引发剂1.5-3重量份；聚醚胺催化剂0.5-0.7重量份；羟乙基纤维素2-3重量份；二氧化铈0.1-0.15重量份；活性矿物质粉0.75-1.3重量份；中药精油0.6-1.1重量份；其中，所述环保树脂为环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的混合物，所述环氧大豆油丙烯酸酯和双酚A型E51环氧树脂的质量比为1.5:1，所述阻燃剂为多聚磷酸铵、三聚氰胺以及膨胀型石墨的混合物，所述多聚磷酸铵、三聚氰胺以及膨胀型石墨的质量比1.5:1.2:1，所述的纳米荧光粉为Ce和YAG的混合物，所述纳米荧光粉的粒径≤13μm，所述的活性矿物质粉为锗石、萤石、电气石、六环石按重量比2.5：3：3.7：2的混合物，其中电气石为镁电气石和锂电气石按重量比5：3的混合物，所述活性矿物质粉的粒径≤13μm，所述功能涂层通过如下步骤制备而成：
S1、将所需重量份数的环保树脂、阻燃剂、纳米荧光粉、羟乙基纤维素、汽巴艳佳固754光引发剂以及聚醚胺催化剂置于搅拌机中，在65-85℃下集中高速搅拌调匀，搅拌时间为15-30分钟，待混合均匀后从搅拌机中取出，即制得混合物A，备用；
S2、将物料打破碗花花65-85重量份，大青叶15-20重量份，贯众4-6重量份，普洱茶4-6重量份，丁香罗勒1.5-2.5重量份，柴胡1-3重量份，芦荟1-3重量份，黄柏1-3重量份，连翘1-3重量份以及白芍药1-3重量份去杂质，一起置于-20℃的真空釜2-3小时，然后再置于微波干燥机进行预处理，其中干燥时间为30-40分钟，微波功率为17kw；
S3、将步骤S2处理后的物料一起投入超微粉碎机中粉碎至60目，制得原料药粉末，备用；
S4、将步骤S3中制得的原料药粉末投入超临界二氧化碳萃取装置的萃取釜中，调节萃取压力28MPa，萃取温度45℃，二氧化碳流量为1100L/h，动态萃取2小时，直接在分离釜出口用三角瓶收集粗油，备用；
S5、将步骤S4中制得的粗油置于5℃环境中冷冻70分钟，再将冷冻后的粗油置于转速为17000r/min的高速冷冻离心机中离心25分钟，去除杂质后置于85℃真空箱抽真空3小时，即制得挥发油B，备用；
S6、将麝香0.6-1重量份，马齿苋3-4重量份，丹参3-4重量份，辣蓼草3-4重量份，百部7-9重量份，藿香3-4重量份，狼毒3-4重量份，栀子3-4重量份，板蓝根15-18重量份以及酸枣仁3-4重量份洗净烘干，一起投入超微粉碎机中粉碎至30目，然后加去离子水浸泡5小时，加水量为所浸泡原料药质量的7倍，搅拌分散调匀，制得中药混合物，备用；
S7、将步骤S6制得的中药混合物于80℃煎煮2小时，收集蒸馏液，并加入乙醚萃取，蒸馏液与乙醚的体积比为2.5:1，取上层油相，然后加无水硫酸钠0.1-0.25重量份进行干燥处理，即制得挥发油C，备用；
S8、将步骤S5和S7所制挥发油B和挥发油C混合调匀制得混合油，再边搅拌边依次加入薄荷精油、玫瑰精油、番红花精油和杜松精油，充分搅拌45分钟，静置30分钟，过滤除杂，即得中药精油，其中，所述混合油与薄荷精油、玫瑰精油、番红花精油和杜松精油的质量比为2：0.5：0.4：0.6：0.5；
S9、将步骤S8制得的中药精油与步骤S1制得的混合物A，在70-80℃下，在搅拌机中集中搅拌混合15分钟，得到预混料，然后在预混料中加入二氧化铈、活性矿物质粉以及改性芳香胺固化剂，在65-85℃下，集中搅拌35分钟后，然后浇铸在所述的基层的外表面，固化脱模，即得功能涂层。
2.根据权利要求1所述的纳米荧光粉与活性矿物质粉复配的环保灯罩的制备方法，其特征在于：在步骤S8中的中药精油还包括以下重量份的组分：表面活性剂1.7份、避蚊胺0.2份、丁酸丁酯1份、桉树油1.2份、醋酸氯已定0.5份、脂肪醇聚氧乙烯醚硫酸钠1份和苯甲酸钠0.2份。
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