CN106040149A - Reaction device - Google Patents

Reaction device Download PDF

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Publication number
CN106040149A
CN106040149A CN201610513659.6A CN201610513659A CN106040149A CN 106040149 A CN106040149 A CN 106040149A CN 201610513659 A CN201610513659 A CN 201610513659A CN 106040149 A CN106040149 A CN 106040149A
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CN
China
Prior art keywords
parts
charging
vertical cylinder
connects
feeding
Prior art date
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Granted
Application number
CN201610513659.6A
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Chinese (zh)
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CN106040149B (en
Inventor
吴玲玲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Petrochemical Caojing Machinery Manufacturing Co ltd
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Huizhou Gregory Technology Co Ltd
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Priority to CN201610513659.6A priority Critical patent/CN106040149B/en
Publication of CN106040149A publication Critical patent/CN106040149A/en
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Publication of CN106040149B publication Critical patent/CN106040149B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/008Feed or outlet control devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236Metal based
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)
  • Injection Moulding Of Plastics Or The Like (AREA)

Abstract

The invention relates to a reaction device which comprises a vertical drum, a stirring device, a feeding device and a material injecting device, wherein an upper sealing head and a lower sealing head are respectively arranged at the two ends of the vertical drum; the stirring device comprises a supporting base, a driving motor, a power output shaft and a stirring paddle; the feeding device comprises a leaking tube, a conveying tube, a feeding pump, a feeding tube and a plurality of feeding components; the material injecting device comprises a sealing plate, a first injecting tube and a second injecting tube. The efficient reaction device is provided with the vertical drum, the stirring device and the feeding device, the feeding moment is controlled and the materials are fed into the feeding components of the feeding device, so that the effect of continuous feeding operation is realized; the feeding operation is simple and convenient; the feeding efficiency is higher.

Description

Consersion unit
Technical field
The present invention relates to chemical production equipment field, particularly relate to a kind of consersion unit.
Background technology
At present, in material production field, it usually needs use consersion unit, e.g., need to use such as vertical response equipment, The container carried when vertical cylinder consersion unit or vertical vertical cylinder consersion unit are as material generation chemical reaction, it is wide General it is applied to the industries such as oil, chemical industry, rubber, pesticide, dyestuff, medicine and food.
In some special occasions, typically the region that feeds intake of consersion unit is arranged on floor or platform, i.e. reaction sets Standby dog-house is normally at the top of consersion unit or near the position at top, when needs add liquid object to consersion unit During material, need to be transported to by material in advance on floor or platform, cause feeding operation more complicated, feed inefficient.
Additionally, existing consersion unit is in order to ensure the mechanical strength of self, too much dog-house typically will not be set, just This causes existing consersion unit, it is more difficult to realize the operation of continuous way charging, in the same time the most relatively difficult to achieve or interval time In shorter, add the operation of various materials.
Summary of the invention
Based on this, it is necessary to a kind of feeding operation of offer is more simple and convenient, charging efficiency is higher and the company of being capable of The consersion unit of continuous formula feeding operation.
A kind of consersion unit, including:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, described agitating device includes supporting seat, driving motor, power output shaft and stirring paddle, described support Seat is fixedly mounted on described upper cover, and the first end of described power output shaft is connected with the rotary shaft of described driving motor, institute The second end stating power output shaft stretches to inside described vertical cylinder, the second end of described power output shaft and described stirring paddle Connecting, described driving motor is used for driving described stirring paddle to rotate;
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body and multiple throwing Material assembly, the first end of described material leakage body connects with described upper cover, the second end of described material leakage body and described conveying pipeline First end connection of body, the second end of described conveying body connects with the discharge end of the described charging pump housing, the described charging pump housing Feed end connects with described charging body, multiple described in the assembly that feeds intake be arranged at intervals at successively on described charging body, and multiple The described assembly that feeds intake all connects with described charging body, described in the assembly that feeds intake include feed intake body, cast hopper and the valve that feeds intake, institute The first end stating the body that feeds intake connects with described charging body, described in feed intake the second end of body connect with described cast hopper, institute State cast hopper and offer dog-house, described in feed intake valve be arranged at described in feed intake on body;And
Material injection device, described material injection device include sealing plate, first inject body and second inject body, institute State sealing plate to cover on described dog-house, and be used for closing described dog-house, described first inject body the first end with Described sealing plate connects, and the described first the first end injecting body connects with described cast hopper, and described first injects body Second end is flexibly connected with the described second the first end injecting body.
Wherein in an embodiment, the lateral wall of the described first the second end injecting body offers external screw thread, described The medial wall of the second the second end injecting body offers female thread, described female thread and described external thread bolt connection.
Wherein in an embodiment, described first injects the second end and described second first end injecting body of body Junction be provided with hoop component.
Wherein in an embodiment, described hoop component includes clip body and connects screw rod, and described clip body sets It is placed in described first and injects the second end of body and the junction of the described second the first end injecting body, described connection screw rod Two ends with described clip body respectively, two ends are spirally connected.
Wherein in an embodiment, described clip body has arcuate structure.
Wherein in an embodiment, described clip body being provided with reinforcement, described reinforcement is by described clip originally One end of body extends to the other end of described clip body.
Wherein in an embodiment, described reinforcement has semicircular structure cross section.
Above-mentioned highly effective reaction device by arranging vertical cylinder, agitating device and feeding device, and control well add fashionable Machine, then the effect of continuous way feeding operation, and feeding operation can be realized to multiple assemblies input materials that feed intake of feeding device More simple and convenient and charging efficiency higher.
Accompanying drawing explanation
Fig. 1 is the structural representation of the consersion unit of an embodiment of the present invention;
Fig. 2 is Fig. 1 enlarged drawing at A;
Fig. 3 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention;
Fig. 4 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention;
Fig. 5 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention;
Fig. 6 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention;
Fig. 7 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention;
Fig. 8 is the partial structurtes schematic diagram of the consersion unit of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully.In accompanying drawing Give the better embodiment of the present invention.But, the present invention can realize in many different forms, however it is not limited to herein Described embodiment.On the contrary, providing the purpose of these embodiments is to make to understand the disclosure more Add thorough comprehensive.
It should be noted that when element is referred to as " being fixed on " another element, and it can be directly on another element Or element placed in the middle can also be there is.When an element is considered as " connection " another element, and it can be to be directly connected to To another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", " left ", For illustrative purposes only, being not offered as is unique embodiment for " right " and similar statement.
Unless otherwise defined, all of technology used herein and scientific terminology and the technical field belonging to the present invention The implication that technical staff is generally understood that is identical.The term used the most in the description of the invention is intended merely to describe tool The purpose of the embodiment of body, it is not intended that in limiting the present invention.Term as used herein " and/or " include one or more Arbitrary and all of combination of relevant Listed Items.
Such as, a kind of consersion unit, including vertical cylinder, the two ends of described vertical cylinder be respectively arranged with upper cover and Low head;Agitating device, described agitating device includes supporting seat, driving motor, power output shaft and stirring paddle, described support seat Being fixedly mounted on described upper cover, the first end of described power output shaft is connected with the rotary shaft of described driving motor, described Second end of power output shaft stretches to inside described vertical cylinder, and the second end of described power output shaft is with described stirring paddle even Connecing, described driving motor is used for driving described stirring paddle to rotate;Feeding device, described feeding device includes material leakage body, conveying Body, the charging pump housing, charging body and multiple assembly that feeds intake, the first end of described material leakage body connects with described upper cover, institute First end of the second end and described conveying body of stating material leakage body connects, the second end of described conveying body and described charge pump Body discharge end connection, the feed end of the described charging pump housing connects with described charging body, multiple described in feed intake assembly successively between Every being arranged on described charging body, and multiple described in the assembly that feeds intake all connect with described charging body, described in feed intake assembly bag Include the body that feeds intake, cast hopper and the valve that feeds intake, described in feed intake the first end of body connect with described charging body, described commissioning pipe Second end of body connects with described cast hopper, and described cast hopper offers dog-house, described in feed intake valve be arranged at described in feed intake On body;And material injection device, described material injection device include sealing plate, first inject body and second inject body, Described sealing plate covers on described dog-house, and is used for closing described dog-house, and described first injects the first end of body Connecting with described sealing plate, and the described first the first end injecting body connects with described cast hopper, described first injects body The second end with described second inject body the first end be flexibly connected.
In order to explain above-mentioned consersion unit further, such as, the consersion unit of another embodiment is as follows:
Referring to Fig. 1, highly effective reaction device 10 includes vertical cylinder 100, agitating device 200 and feeding device 300, stirring Device 200 and feeding device 300 may be contained within vertical cylinder 100.
Referring to Fig. 1, the two ends of vertical cylinder 100 are respectively arranged with upper cover 110 and low head 120, vertical cylinder 100 For the material of accommodating addition, and give material mix and blend and the offer occasion that reacts.Such as, upper cover 110 and low head Vertical cylinder 100 is formed after 120 connections.And for example, described vertical cylinder is formed in one structure.And for example, in described vertical cylinder Be installed on outside support during, the top of the externally-located support of described upper cover, the externally-located support of described low head Bottom.
Referring to Fig. 1, agitating device 200 includes supporting seat 210, driving motor 220, power output shaft 230 and stirring paddle 240, support seat 210 and be fixedly mounted on the upper cover 110 of vertical cylinder 100, the first end of power output shaft 230 and driving electricity The rotary shaft of machine 220 connects, and it is internal that the second end of power output shaft 230 stretches to vertical cylinder 100, e.g., and power output shaft 230 The second end to stretch to the low head 120 of vertical cylinder 100 internal, the second end of power output shaft 230 is with stirring paddle 240 even Connecing, e.g., the low head 120 that stirring paddle 240 is positioned at vertical cylinder 100 is internal, drives motor 220 to be used for driving power output shaft 230 rotate, and then drive the stirring paddle 240 fixed with power output shaft 230 to rotate.Thing in needing vertical cylinder 100 When material is stirred married operation, controls to drive motor 220 to drive power output shaft 230 to rotate, and then drive stirring paddle 240 turns Dynamic, utilize the flow-disturbing effect of stirring paddle 240, can play and preferably stir immixture, and then can be with in vertical cylinder 100 Material be stirred married operation.
Seeing also Fig. 1 and Fig. 2, feeding device 300 includes material leakage body 310, conveying body 320, the charging pump housing 330, charging body 340 and multiple assembly 350 that feeds intake, upper cover 110, material leakage body 310, conveying body 320, the charging pump housing 330, charging body 340 and the assembly 350 that feeds intake be sequentially connected with, and for example, upper cover 110, material leakage body 310, conveying body 320, The charging pump housing 330, charging body 340 and the assembly 350 that feeds intake are sequentially communicated.
Referring to Fig. 1, the first end of material leakage body 310 connects with upper cover 110, and the second end of material leakage body 310 is with defeated First end connection of material body 320, the second end of conveying body 320 connects with the discharge end of the charging pump housing 330, and feed the pump housing The feed end of 330 connects with charging body 340, and multiple assemblies 350 that feed intake are arranged at intervals on charging body 340 successively, and many The individual assembly 350 that feeds intake all connects with charging body 340, when needs add material in vertical cylinder 100, and only need to be to the group that feeds intake Part 350 puts into material can complete whole feeding operation, and feeding operation is more simple and convenient and charging efficiency is higher, and without volume Outer these regions that feed intake such as floor or platform are set, it is achieved that exempt from the effect of high-order charging, say, that when to the assembly that feeds intake During 350 input material, draft based on the charging pump housing 330, the material adding the assembly 350 that feeds intake can enter to the body 340 that feeds In, afterwards, material enters in conveying body 320 by the charging pump housing 330 again, and then, material is entered by conveying body 320 again To material leakage body 310, finally, material is entered in the upper cover 110 of vertical cylinder 100 again by material leakage body 310, Jin Erjin Enter to whole vertical cylinder 100, now, complete whole feeding operation, i.e. only need to put into the assembly 350 that feeds intake or add material Can complete whole feeding operation, feeding operation is simple and convenient and charging efficiency is higher.Additionally, due to material leakage body 310, conveying Body 320 and the existence of charging body 340, can be arranged far from the region of vertical cylinder 100 by the assembly 350 that feeds intake, such as, Due to material leakage body 310, conveying body 320 and the existence of charging body 340, the assembly 350 that feeds intake can be arranged and be convenient for On the ground of dosing operation or be arranged in weighing area, so, it is possible to achieve exempt from the effect that a high position feeds intake and exempts from feeding platform.
Referring to Fig. 2, the assembly 350 that feeds intake includes feed intake body 351, cast hopper 352 and the valve 353 that feeds intake, and feed intake body First end of 351 connects with charging body 340, and the second end of the body 351 that feeds intake connects with cast hopper 352, and cast hopper 352 is offered Having dog-house 354, the valve 353 that feeds intake is arranged at and feeds intake on body 351.Such as, described feeding device arranges and feeds intake described in three Assembly, as such, it is possible to be simultaneously introduced three kinds of materials, and then realizes the effect of continuous way feeding operation, certainly, described in feed intake assembly Number be not limited to three, for example, it is also possible to be adjusted according to practical situation, e.g., each described in feed intake assembly one a pair Should a kind of material participating in reaction.
When in the needs same time or interval time shorter in, to vertical cylinder 100 is internal add various materials time, this Time, it being simultaneously introduced the kind of material as required, a number of valve 353 that feeds intake of corresponding unlatching, then, to multiple cast hoppers The dog-house 354 of 352 is corresponding puts into various materials, opens the charging pump housing 330, swabbing action based on the charging pump housing 330, material Along cast hopper 352-feed intake body 351-charging body 340-charging pump housing 330-conveying body 320-material leakage body 310-stand The charging path of formula cylinder 100 enters in vertical cylinder 100, now, completes whole feeding operation.
When needs are to vertical cylinder 100 a kind of material of internal addition, now, open the dog-house of a cast hopper 352 354 and corresponding put into these materials, and close remaining valve 353 that feeds intake, material adds along the cast hopper 352-body 351-that feeds intake The charging path of material body 340-charging pump housing 330-conveying body 320-material leakage body 310-vertical cylinder 100 enters to vertical In cylinder 100, now, whole feeding operation is completed.
Above-mentioned highly effective reaction device 10 is by arranging vertical cylinder 100, agitating device 200 and feeding device 300, and controls Make addition opportunity, then put into material to multiple assemblies 350 that feed intake of feeding device 300 and can realize continuous way feeding operation Effect, and feeding operation is more simple and convenient and charging efficiency is higher.
In order to preferably close described cast hopper, with reduce the material in described cast hopper evaporate into the external world amount, such as, Referring to Fig. 3, described highly effective reaction device also includes that locking device 400, locking device 400 include rotary shaft 410 and closing door 420, described rotary shaft rotates and is arranged at the marginal position of described dog-house of cast hopper 352, described closing door and described rotation Rotating shaft is fixing to be connected, and described closing door is used for closing described dog-house, and the edge of described closing door is provided with sealing ring, described close Seal supports with the edge of described dog-house;And for example, described dog-house has the cross section of circular configuration;And for example, described closing Door has circular pan-like structure;And for example, described sealing ring has circular annular form structure;And for example, described closing door is away from described rotation The position of rotating shaft is provided with balancing weight;And for example, described sealing ring is provided with seal groove towards the side opening of described dog-house, described The edge of dog-house is embedded at inside described seal groove;And for example, described seal groove has loop configuration, so, utilizes and closes dress The closing door 420 putting 400 can preferably close described cast hopper, with reduce the material in described cast hopper evaporate into the external world Amount.
In order to preferably put into material in described cast hopper, such as, referring to Fig. 4, described highly effective reaction device also wraps Including material injection device 500, described material injection device 500 includes that sealing plate 510, first injects body 520 and second and injects Body 530, described sealing plate covers on the described dog-house of cast hopper 352, and is used for closing described dog-house, and described One the first end injecting body connects with described sealing plate, and described first injects the first end of body with described cast hopper even Logical, the described first the second end injecting body is flexibly connected with the described second the first end injecting body, described second ascending pipe Second end of body is for connecting with outside material injection device, e.g., connects with outside charging bucket, and described charging bucket is equipped with Material;And for example, the lateral wall of the described first the second end injecting body offers external screw thread, and described second injects the second of body The medial wall of end offers female thread, described female thread and described external thread bolt connection;And for example, described first injects the second of body End is provided with hoop component with the junction of the described second the first end injecting body;And for example, described hoop component includes clip Body and connection screw rod, described clip body is arranged at the described first the second end injecting body and injects body with described second The junction of the first end, two ends with described clip body respectively, the two ends of described connection screw rod are spirally connected;And for example, described clip is originally Body has arcuate structure;And for example, described clip body being provided with reinforcement, described reinforcement is by one end of described clip body Extend to the other end of described clip body;And for example, described reinforcement has a semicircular structure cross section, so, and only need to be by outward The material injection device in portion connects with the described second the second end injecting body can complete dosing operation such that it is able to preferably Material is put in described cast hopper.
It is appreciated that when adding the material of excess to described cast hopper, it is possible to cause described cast hopper generation flash Problem, in order to make described cast hopper preferably material be buffered, with reduce flash problem occur, such as, refer to Fig. 5, described highly effective reaction device also include material buffer device 600, described material buffer device 600 include buffering bucket 610 and Cover plate 620, described buffering bucket 610 has the structure of the shaped hollow round table of both ends open, and the bottom opening of described buffering bucket 610 is solid Surely be placed on described cast hopper 352 and neighbouring described in feed intake the position of body, described cover plate has loop configuration, described lid The outer ledge of plate is connected at the open-topped marginal position of described buffering bucket, the inside edge of described cover plate and described throwing The lateral wall of hopper connects, and the sidewall of described cast hopper offers cushion hole, described cushion hole respectively with described cast hopper and institute Stating buffering bucket connection, material can be flowed between described buffering bucket and described cast hopper by described cushion hole, slow to play The effect of punching;And for example, the sidewall of described cast hopper offers some described cushion holes, and described cushion hole is with in described cast hopper Mandrel line radially distributes;And for example, equal between the most adjacent two described cushion holes;And for example, described cushion hole position It is provided with drainage screen;And for example, described cast hopper has cirque structure cross section;And for example, the inside edge of described cover plate and institute It is provided with sealing strip at the link position of the lateral wall stating buffering bucket;And for example, described sealing strip has loop configuration, so, and profit Described cast hopper can be made preferably material to be buffered with material buffer device 600, to reduce the problem generation of flash.
In order to preferably carry the logistics flowed out in described material leakage body, and then minimizing material falls to described vertical cylinder The problem of the material sputtering of internal generation, such as, refers to Fig. 6, and described highly effective reaction device also includes material bogey 700, described material bogey 700 includes the inner side of loading plate 710 and connecting plate 720, described loading plate and described upper cover Wall connects, and described loading plate is arranged towards described material leakage body, the bearing of trend of described loading plate and described vertical cylinder Forming acute angle between central axis, the first end of described connecting plate is connected with the medial wall of described upper cover, described connecting plate Second end is connected with described loading plate, and described loading plate 710 is provided with flow-disturbing projection towards the side of described material leakage body 310 711;And for example, described loading plate is provided with some flow-disturbings projection;And for example, some described flow-disturbing projection rectangular array are distributed in institute State in carrying;And for example, described flow-disturbing projection has hemispherical structure;And for example, described loading plate is near described low head Position is gradually obliquely installed;And for example, described connecting plate has the cross section of trapezium structure;And for example, described loading plate is towards institute The side stating material leakage body is further opened with liquid leakage tank, so, is held material by the loading plate 710 of material bogey 700 Carry and buffering effect, it is possible to reduce material drops to the flow velocity within described vertical cylinder, and can also play the effect of dispersed material Really, and then can preferably carry the logistics flowed out in described material leakage body, fall to described vertical cylinder reducing material The problem of the material sputtering of interior generation.
In order to make the material flowed out in described material leakage body carry out preferably scatter operation, the most whole course of reaction In, the mixed effect of each material, such as, refer to Fig. 7, described highly effective reaction device also includes material dispersing device 800, described It is internal that material dispersing device 800 is placed in described vertical cylinder 10, described material dispersing device 800 include connector drum 810 and Dispersion framework 820, the first end of described connector drum connects with the first end of described material leakage body, during described dispersion framework has Hollow structure, forms distribution cavity in it, the second end of described connector drum is connected with described dispersion framework, and described connecting cylinder Second end of body connects with described distribution cavity, and described dispersion framework 820 offers some away from one end of described connector drum The dispersion hole 821 of described distribution cavity connection, described dispersion hole is arranged towards described low head 120, and e.g., material is by each described point Dissipate hole 821 to fall to inside described vertical cylinder;And for example, described dispersion framework has the columnar structured of hollow;And for example, some Described dispersion hole is distributed with the central axis circular array of described dispersion framework;And for example, described dispersion hole has regular polygon Cross-sectional structure;And for example, described dispersion hole has the cross-sectional structure of regular hexagon structure;And for example, described connector drum First end is spirally connected with the first end of described material leakage body;And for example, described connector drum has rounded cylindrical structure, so, utilizes Described material dispersing device can make the material flowed out in described material leakage body carry out preferably scatter operation, the most whole instead During Ying, the mixed effect of each material.
It is pointed out that each material being stirred married operation inside described vertical cylinder carries out combination reaction Time, and most combination reaction is all exothermic reaction, when the productivity that the speed of reaction and product generate is also required to dependent reaction Liberated heat, is used for improving reaction rate and productivity.Additionally, in whipping process, material can be done work by described agitating device, I.e. material is during being mutually mixed agitation, shows as outwardly releasing the material that heat, especially toughness are stronger, and it is put Thermal phenomenon becomes apparent from, and therefore, based on above-mentioned situation, relies on the combination reaction of higher temperature for some, as depended on reaction certainly Body heat release and the combination reaction of stirring heat production, and need not extra heater for the reaction that it heats, especially need Guarantee the heat-insulating property of described vertical cylinder.Further, in order to for some acid materials, therefore, to assure that described vertical cylinder The medial wall of body, the medial wall of the described vertical cylinder i.e. directly contacted with acid material possesses higher resistance to acid attack performance, uses The service life of vertical cylinder described in Yu Yansheng and being normally carried out of reaction.Further, the lateral wall of described vertical cylinder by In often contacting with corrosive materials, e.g., the corrosive materials contact of the form such as gaseous state or liquid, it is therefore desirable to possess preferably Decay resistance, for preferably protecting described vertical cylinder.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described vertical cylinder, such as, refer to Fig. 8, Described vertical cylinder, e.g., the sidewall of described vertical cylinder includes the resistance to acid attack layer 130 being cascading, heat-insulation layer 140, props up Support layer 150, weight coating 160 and protective layer 170, described resistance to acid attack layer is positioned at the medial wall of described vertical cylinder, and described resistance to Directly and material, e.g., acid material contact, described protective layer is positioned at the lateral wall of described vertical cylinder, the most described guarantor to acid etching layer Sheath is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts~88 parts, titanium 30 Part~34 parts, chromium 20 parts~25 parts, antimony 2.5~3.4 parts, copper part 2.3~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 Part, 0.15 part~0.27 part of carbon, silicon 0.25 part~0.46 part, boron 0.12 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.
Use ferrum 75 parts~88 parts, titanium 30 parts~34 parts and chromium 20 parts~25 parts as basis, the basis unit of resistance to acid attack layer Element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding antimony 2.5~3.4 parts, copper 2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 parts, cobalt 0.04 part~0.09 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 part compound, additionally it is possible to optimize further The properties of described resistance to acid attack layer, especially can optimize the resistance to acid attack performance of described resistance to acid attack layer further such that it is able to Better against the acid etching of material, for improving the service life of described vertical cylinder further and guaranteeing normally entering of reaction OK.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts~80 parts, titanium 33 parts~34 parts, chromium 24 parts~25 parts, antimony 2.7~3.4 parts, copper 2.7 parts~3.4 parts, 1.8 parts~2.5 parts of zinc, aluminum 1.1~1.4 Part, 0.18 part~0.27 part of carbon, silicon 0.27 part~0.46 part, boron 0.13 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts, titanium 33 parts, Chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon 0.46 part, boron 0.18 part, cobalt 0.04 part, phosphorus 0.03 part, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04 part, scandium 0.01 part and 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts~22 parts, white Cotton 8~20 parts, rock wool 8 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 parts~ 4.5 parts, basalt fibre 1 part~3 parts, rubber foam 3~5 parts, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1 Part~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~2 parts, polypropylene fiber 3~4 parts, Thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when described vertical cylinder During the material generation exothermic reaction in internal portion, and after transferring heat to described resistance to acid attack layer, have good based on described heat-insulation layer Good heat insulation and heat-insulating property, can limit heat and be further transmitted through described vertical cylinder, and then avoid heat to be transferred directly to In external environment, it is ensured that the material within described vertical cylinder reacts at a suitable temperature, it is used for improving reaction speed Rate and the productivity of product.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts~21 parts, White cotton 17~20 parts, rock wool 10 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 Part~4.5 parts, basalt fibre 1 part~2.5 parts, rubber foam 3.5~5 parts, 1.5 parts~2 parts of magnesium hydroxide, aminopropyl three second TMOS 1.5 parts~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~1.4 parts, third Synthetic fibre fiber 3.3~4 parts, thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts, white cotton 17 ~20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts, basalt fibre 2.1 parts, rubber Foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2 parts, aluminium oxide 1.8 parts, 3,5-di-t-butyl-4-hydroxyl Essence of Niobe 1.4 parts, polypropylene fiber 4 parts, thiorubber. 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts~98 parts, manganese 0.4 Part~0.95 part, molybdenum 0.1 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.06 part~0.25 part of carbon, Silicon 0.1 part~0.3 part, 0.05 part~0.1 part of phosphorus, boron 0.001 part~0.01 part, hafnium 0.05 part~0.5 part, scandium 0.05 part~ 0.3 part, chromium 0.05 part~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part.
It is appreciated that to make described vertical cylinder possess preferable heat-insulating property, needs to introduce described heat-insulation layer, and institute The mechanical strength stating heat-insulation layer is poor, in order to strengthen the integrally-built mechanical strength of described vertical cylinder, needs to introduce described Support layer so that it is directly contact with described heat-insulation layer, be used for improving the integrally-built mechanical strength of described vertical cylinder, to reach peace The full purpose produced.Based on above-mentioned situation, this is necessary for requiring that described supporting layer possesses higher mechanical strength and anti-deformation behavior Can, by using each component of as above mass parts, the most described supporting layer contain hafnium 0.05 part~0.5 part, scandium 0.05 part~ 0.3 part, chromium 0.05 part~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part, the mechanical strength of conventional iron alloy can be improved so that it is mechanical strength and anti-deformation nature are more excellent, Disclosure satisfy that requirement.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts~98 parts, manganese 0.55 part~0.95 part, molybdenum 0.35 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.17 part of carbon~ 0.25 part, silicon 0.1 part~0.25 part, 0.05 part~0.1 part of phosphorus, boron 0.008 part~0.01 part, hafnium 0.1 part~0.5 part, scandium 0.1 Part~0.3 part, chromium 0.1 part~0.3 part, 0.02 part~0.05 part of nickel, cerium 0.02 part~0.05 part, thorium 0.02 part~0.05 part and Zirconium 0.02 part~0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, 0.75 part of manganese, Molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus, boron 0.008 part, hafnium 0.5 part, scandium 0.2 Part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part and 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts~95 parts of tungsten, 30 parts of nickel ~60 parts, ferrum 15 parts~40 parts, chromium 1.5 parts~10 parts, 1.5 parts~10 parts of lead, copper 1 part~6 parts and molybdenum 0.5 part~5 parts.
It is appreciated that in producing course of reaction, needs the material in described vertical cylinder is carried out higher the stirring of intensity Mix operation, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid the entirety of described vertical cylinder The quality of structure kicks the beam, and then reduces the external impacts impact on described vertical cylinder, i.e. can reduce described vertical cylinder and send out Raw concussion or displacement problem.The each component using as above mass parts can make described weight coating possess excellent counterweight performance, energy Enough effectively increase the integrally-built weight of described vertical cylinder so that it is identical or adaptive with the weight of traditional vertical cylinder, Such that it is able to the security performance in raising production process.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts~95 parts of tungsten, nickel 30 Part~45 parts, ferrum 27 parts~40 parts, chromium 1.5 parts~2.3 parts, 1.5 parts~3.3 parts of lead, copper 1 part~5.5 parts and molybdenum 0.5 part~ 4.9 part.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, 38 parts of nickel, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts~80 parts, lithium 16~ 18 parts, 18 parts~25 parts of nickel, molybdenum 3.5 parts~4 parts, chromium 2 parts~5 parts, cobalt 1 part~5 parts, vanadium 1 part~5 parts, 1 part~2 parts of manganese, iridium 0.8 part~2.5 parts, niobium 0.5 part~2.5 parts, scandium 0.3 part~2.5 parts, 0.2 part~2.5 parts of strontium, caesium 0.2 part~2.5 parts, tungsten 0.2 part~2.5 parts and titanium 0.2 part~2.5 parts.
Be appreciated that the lateral wall of described vertical cylinder owing to often contacting with corrosive materials, e.g., gaseous state or liquid etc. The corrosive materials contact of form, it is therefore desirable to possess preferable decay resistance, for preferably protecting described vertical cylinder. By each component of as above mass parts, described protective layer can be made to possess good Corrosion Protection, and then preferably protect institute State vertical cylinder, for extending the service life of described vertical cylinder.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts~70 parts, lithium 16 Part~16.5 parts, nickel 18~21 parts, molybdenum 3.5 parts~3.9 parts, chromium 2 parts~4.4 parts, cobalt 1 part~3.9 parts, vanadium 1 part~4.5 parts, 1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, niobium 0.5 part~2.2 parts, scandium 0.3 part~2.3 parts, 0.2 part~2.3 parts of strontium, caesium 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium 0.2 part~1.9 parts.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium 16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, 2.3 parts of iridium, niobium 2.2 parts, scandium 2.3 parts, strontium 2.3 Part, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described vertical cylinder further, e.g., the structure of the sidewall of described vertical cylinder, such as, described acidproof The thickness ratio of erosion layer, described heat-insulation layer, described supporting layer, described weight coating and described protective layer is (1~1.5): (15~20): (5~5.5): (8~9.8): (0.5~1.2);And for example, the thickness of described weight coating and described protective layer is than for 1:15:5:9.5: 1.1。
It should be noted that other embodiments of the present invention also include that the technical characteristic in the various embodiments described above be combined with each other Can be formed, and the highly effective reaction device that can implement.
It should be noted that other embodiments of the present invention also include that the technical characteristic in the various embodiments described above be combined with each other Can be formed, and the consersion unit that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, not to above-mentioned reality The all possible combination of each technical characteristic executed in example is all described, but, as long as the combination of these technical characteristics is not deposited In contradiction, all it is considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed, but Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that, for the ordinary skill people of this area For Yuan, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these broadly fall into the present invention's Protection domain.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (7)

1. a consersion unit, it is characterised in that including:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, described agitating device includes supporting seat, driving motor, power output shaft and stirring paddle, and described support seat is solid Dingan County is contained on described upper cover, and the first end of described power output shaft is connected with the rotary shaft of described driving motor, described dynamic Second end of power output shaft stretches to inside described vertical cylinder, and the second end of described power output shaft is with described stirring paddle even Connecing, described driving motor is used for driving described stirring paddle to rotate;
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body and multiple group that feeds intake Part, the first end of described material leakage body connects with described upper cover, the second end of described material leakage body and described conveying body First end connection, the second end of described conveying body connects with the discharge end of the described charging pump housing, the charging of the described charging pump housing End connects with described charging body, multiple described in the assembly that feeds intake be arranged at intervals at successively on described charging body, and multiple described in The assembly that feeds intake all connects with described charging body, described in the assembly that feeds intake include feed intake body, cast hopper and the valve that feeds intake, described throwing First end of material body connects with described charging body, described in feed intake the second end of body connect with described cast hopper, described throwing Hopper offers dog-house, described in feed intake valve be arranged at described in feed intake on body;And
Material injection device, described material injection device include sealing plate, first inject body and second inject body, described close Shrouding covers on described dog-house, and is used for closing described dog-house, and described first injects the first end of body with described Sealing plate connects, and the described first the first end injecting body connects with described cast hopper, and described first injects the second of body Hold and be flexibly connected with the described second the first end injecting body.
Consersion unit the most according to claim 1, it is characterised in that described first injects the lateral wall of the second end of body Offering external screw thread, the medial wall of the described second the second end injecting body offers female thread, described female thread with described outside Screw thread is spirally connected.
Consersion unit the most according to claim 2, it is characterised in that described first injects second end and described the of body The junction of two the first ends injecting body is provided with hoop component.
Consersion unit the most according to claim 3, it is characterised in that described hoop component includes clip body and connects spiral shell Bar, described clip body is arranged at described first and injects the second end of body and the connection of the described second the first end injecting body Place, two ends with described clip body respectively, the two ends of described connection screw rod are spirally connected.
Consersion unit the most according to claim 4, it is characterised in that described clip body has arcuate structure.
Consersion unit the most according to claim 4, it is characterised in that be provided with reinforcement on described clip body, described Reinforcement is extended to the other end of described clip body by one end of described clip body.
Consersion unit the most according to claim 6, it is characterised in that described reinforcement has semicircular structure cross section.
CN201610513659.6A 2016-06-30 2016-06-30 Consersion unit Expired - Fee Related CN106040149B (en)

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