CN106040144A - Efficient reaction device - Google Patents

Efficient reaction device Download PDF

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Publication number
CN106040144A
CN106040144A CN201610509748.3A CN201610509748A CN106040144A CN 106040144 A CN106040144 A CN 106040144A CN 201610509748 A CN201610509748 A CN 201610509748A CN 106040144 A CN106040144 A CN 106040144A
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China
Prior art keywords
air
blowing
parts
kettle
reaction device
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Granted
Application number
CN201610509748.3A
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Chinese (zh)
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CN106040144B (en
Inventor
吴玲玲
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Gaomi Jiantao Chemical Co ltd
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Huizhou Gregory Technology Co Ltd
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Priority to CN201610509748.3A priority Critical patent/CN106040144B/en
Publication of CN106040144A publication Critical patent/CN106040144A/en
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Publication of CN106040144B publication Critical patent/CN106040144B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • B01F33/402Mixers using gas or liquid agitation, e.g. with air supply tubes comprising supplementary stirring elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236Metal based
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention relates to an efficient reaction device which comprises a kettle body, a stirring component, an air-blowing mixing component and a material separating component, wherein an upper sealing head and a lower sealing head are respectively arranged at the two ends of the kettle body; the stirring component comprises a mounting frame, a stirring motor, a stirring shaft and a stirring paddle; the air-blowing mixing component comprises an exhaust pipe, an air-blowing pump, an air feeding pipe, a fixing frame and an air blowing plate; the exhaust pipe is respectively communicated with the upper sealing head and the air-blowing pump; the air feeding pipe is respectively communicated with the air-blowing pump and the lower sealing head; the air feeding pipe is communicated with an air blowing chamber of the air blowing plate; an air blowing hole is formed on the air blowing plate; the material separating component is located in the kettle body; the material separating component comprises a connecting pipe and a separating pipe; under the synergistic effect of the stirring component and the air-blowing mixing component, the efficient reaction device can achieve better material mixing effect; besides, the condition of the sticky material adhering to the stirring paddle can be reduced by the air shock of the air-blowing mixing component to the stirring paddle.

Description

Highly effective reaction device
Technical field
The present invention relates to chemical machinery technical field, particularly relate to a kind of highly effective reaction device.
Background technology
At present, in material production field, it usually needs use reaction unit, e.g., need to use still reaction device to make The container carried during by material generation chemical reaction, its be widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine and The industries such as food.
Common, in order to accelerate the hybrid reaction process of material, need material is stirred operation, reach to improve material Mixing homogeneity and improve material and contact with each other the effect of degree.Therefore, stirring is often installed in traditional reaction unit Device, agitating device generally comprises power drive assem, shaft and the stirring paddle being sequentially connected with, and stirring paddle stretches to material In, by power drive assem, shaft provided power, and then drive stirring paddle that material is stirred.
But, still there is the problem that mixing effect is poor in traditional reaction unit, additionally, bigger for some viscosity Material, e.g., the material of resinae, it also occur that the problem that materials from bonding is on stirring paddle.
Summary of the invention
Based on this, it is necessary to provide a kind of mixed effect preferably and viscous material can be reduced and stick on stirring paddle Highly effective reaction device.
A kind of highly effective reaction device, including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head;
Mixing component, described mixing component includes installing rack, stirring motor, shaft and stirring paddle, and described installing rack is solid Dingan County is contained on described upper cover, and the first end of described shaft is connected with the rotary shaft of described stirring motor, described shaft The second end stretch to inside described kettle, the second end of described shaft is connected with described stirring paddle, described stirring motor use Rotate in driving described stirring paddle;
Air-blowing electric hybrid module, described air-blowing electric hybrid module include bleeding body, the air-blowing pump housing, body of supplying gas, fixed mount and Air-blowing plate body, described in bleed the first end of body connect with described upper cover, described in bleed the second end of body and described air-blowing The inlet end connection of the pump housing, described in the first end of body of supplying gas connect with the outlet side of the described air-blowing pump housing, described fixed mount peace Being contained on the medial wall of described low head, described air-blowing plate body fixes with described fixed mount, and described air-blowing plate body is placed in In described kettle, described air-blowing plate body has arcuate structure, and in it, hollow is arranged, and is provided with air-blowing chamber in described air-blowing plate body Body, described in supply gas the second end of body be connected with described air-blowing plate body, and described in supply gas the second end of body and described air-blowing Cavity connects, and on described air-blowing plate body, the sidewall towards described stirring paddle offers some air-blowing holes, and some described air-blowing holes are equal Connect with described air-blowing cavity, and between the bearing of trend in described air-blowing hole and the central axis of described kettle, form acute angle;And
Material intercepts assembly, and described material intercepts assembly and is positioned at inside described kettle, and described material intercepts assembly and includes even Adapter body and intercept body, the first end of described connection pipe body is spirally connected with the first end of body of bleeding, the of described connection pipe body Two ends are spirally connected with the first end of described obstruct body, and the second end of described obstruct body is arranged towards described shaft, described resistance The bearing of trend of pipe body forms angle with the central axis of described kettle, and described obstruct body is towards the side of described stirring paddle To being gradually obliquely installed.
Wherein in an embodiment, described connection pipe body has round tubular structure, the first end of described connection pipe body Lateral wall offer the first external screw thread, the lateral wall of the second end of described connection pipe body offers the second external screw thread, described in take out The medial wall of the first end of trachea body offers the first female thread, and the medial wall of the first end of described obstruct body offers second Female thread, described first female thread and described first external thread bolt connection, described second female thread and described second external thread bolt connection.
Wherein in an embodiment, described connecting tube is positioned at the pipe diameter size of its first end equal to being positioned at its second end Pipe diameter size.
Wherein in an embodiment, the medial wall of described obstruct body is provided with some projections.
Wherein in an embodiment, some described protruding circular array are distributed in the medial wall of described obstruct body On.
Wherein in an embodiment, the end of described projection has semicircle spherical structure.
Wherein in an embodiment, the first end of described obstruct body and the position that is spirally connected of the second end of described connection pipe body The place of putting is provided with sealant layer.
Above-mentioned highly effective reaction device by arranging kettle, mixing component and air-blowing electric hybrid module, and at mixing component and Under the synergism of air-blowing electric hybrid module, it is possible to reach preferable material mixed effect, additionally, by air-blowing electric hybrid module to stirring Mix the gas shock of oar, it is possible to reduce viscous material and stick to the situation generation of stirring paddle.
Accompanying drawing explanation
Fig. 1 is the structural representation of the highly effective reaction device of an embodiment of the present invention;
Fig. 2 is Fig. 1 enlarged drawing at A;
Fig. 3 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention;
Fig. 4 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention;
Fig. 5 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention;
Fig. 6 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention;
Fig. 7 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention;
Fig. 8 is the partial structurtes schematic diagram of the highly effective reaction device of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully.In accompanying drawing Give the better embodiment of the present invention.But, the present invention can realize in many different forms, however it is not limited to herein Described embodiment.On the contrary, providing the purpose of these embodiments is to make to understand the disclosure more Add thorough comprehensive.
It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, and it can be directly separately On one element or element placed in the middle can also be there is.When an element is considered as " connection " another element, and it is permissible It is directly to another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", "left", "right" and similar statement for illustrative purposes only, being not offered as is unique embodiment.
Unless otherwise defined, all of technology used herein and scientific terminology and the technical field belonging to the present invention The implication that technical staff is generally understood that is identical.The term used the most in the description of the invention is intended merely to describe tool The purpose of the embodiment of body, it is not intended that in limiting the present invention.Term as used herein " and/or " include one or more Arbitrary and all of combination of relevant Listed Items.
Such as, a kind of highly effective reaction device, including: kettle, the two ends of described kettle are respectively arranged with upper cover and lower envelope Head;Mixing component, described mixing component includes installing rack, stirring motor, shaft and stirring paddle, and described installing rack fixedly mounts On described upper cover, the first end of described shaft is connected with the rotary shaft of described stirring motor, the second of described shaft End stretches to inside described kettle, and the second end of described shaft is connected with described stirring paddle, and described stirring motor is used for driving Described stirring paddle rotates;Air-blowing electric hybrid module, described air-blowing electric hybrid module includes bleeding body, the air-blowing pump housing, body of supplying gas, solid Determine frame and air-blowing plate body, described in bleed the first end of body connect with described upper cover, described in bleed the second end of body and institute State the inlet end connection of the air-blowing pump housing, described in the first end of body of supplying gas connect with the outlet side of the described air-blowing pump housing, described solid Determining frame to be arranged on the medial wall of described low head, described air-blowing plate body fixes with described fixed mount, and described air-blowing plate body Being placed in described kettle, described air-blowing plate body has arcuate structure, and in it, hollow is arranged, and is provided with drum in described air-blowing plate body Air cavity, described in supply gas the second end of body be connected with described air-blowing plate body, and described in supply gas the second end of body with described Air-blowing cavity connects, and on described air-blowing plate body, the sidewall towards described stirring paddle offers some air-blowing holes, some described air-blowing Air-blowing cavity connection described in Kong Junyu, and formed sharp between the bearing of trend in described air-blowing hole and the central axis of described kettle Angle;And material intercepts assembly, described material intercepts assembly and is positioned at inside described kettle, and described material intercepts assembly and includes connecting tube Body and obstruct body, the first end of described connection pipe body is spirally connected with the first end of body of bleeding, the second end of described connection pipe body Being spirally connected with the first end of described obstruct body, the second end of described obstruct body is arranged towards described shaft, described obstructing tube The central axis of the bearing of trend of body and described kettle forms angle, and described obstruct body towards described stirring paddle direction by Gradually it is obliquely installed.
In order to further above-mentioned highly effective reaction device be explained, such as, the highly effective reaction of another embodiment Device is as follows:
Referring to Fig. 1, highly effective reaction device 10 includes kettle 100, mixing component 200 and air-blowing electric hybrid module 300, stirring Assembly 200 and air-blowing electric hybrid module 300 may be contained within kettle 100.
Referring to Fig. 1, the two ends of kettle 100 are respectively arranged with upper cover 110 and low head 120, and kettle 100 is used for housing The material added, and material mix and blend and the offer occasion that reacts are provided.Such as, after upper cover 110 is connected with low head 120 Form kettle 100.And for example, described kettle is formed in one structure.And for example, in the process being installed on outside support of described kettle In, the top of the externally-located support of described upper cover, the bottom of the externally-located support of described low head.
Referring to Fig. 1, mixing component 200 includes installing rack 210, stirring motor 220, shaft 230 and stirring paddle 240, Installing rack 210 is fixedly mounted on the upper cover 110 of kettle 100, the first end of shaft 230 and the rotation of stirring motor 220 Axle connects, and it is internal that the second end of shaft 230 stretches to kettle 100, and e.g., the second end of shaft 230 stretches to kettle 100 Low head 120 is internal, and the second end of shaft 230 is connected with stirring paddle 240, and e.g., stirring paddle 240 is positioned at the lower envelope of kettle 100 120 internal, and stirring motor 220 is used for driving shaft 230 to rotate, and then drives and the fixing stirring paddle 240 of shaft 230 Rotate.When needing the material in kettle 100 is stirred married operation, control stirring motor 220 and drive shaft 230 turns Dynamic, and then drive stirring paddle 240 to rotate, utilize the flow-disturbing effect of stirring paddle 240, can play and preferably stir immixture, And then the material in kettle 100 can be stirred married operation.
Seeing also Fig. 1 and Fig. 2, air-blowing electric hybrid module 300 includes bleed body 310, the air-blowing pump housing 320, snorkel Body 330, fixed mount 340 and air-blowing plate body 350, body 310 of bleeding, the air-blowing pump housing 320, supply gas body 330 and air-blowing plate body 350 Being sequentially connected with, fixed mount 340 medial wall with air-blowing plate body 350 and kettle 100 respectively is connected.
Referring to Fig. 2, the first end of body 310 of bleeding connects with the upper cover 110 of kettle 100, the of body 310 of bleeding Two ends connect with the inlet end of the air-blowing pump housing 320, and the first end of body 330 of supplying gas connects with the outlet side of the air-blowing pump housing 320, drum Air-pump 320, and is blasted the air suction in the upper cover 110 of kettle 100 to supplying gas further by body 310 of bleeding In body 330.
Referring to Fig. 2, fixed mount 340 is arranged on the medial wall of low head 120 of kettle 100, and air-blowing plate body 350 is with solid Determine frame 340 to fix, and air-blowing plate body 350 is placed in low head 120 inside of kettle 100.Air-blowing plate body 350 has arc knot Structure, the inner hollow of air-blowing plate body 350 arranges, is provided with air-blowing cavity 351 in air-blowing plate body 350.Supply gas the second of body 330 End is connected with air-blowing plate body 350, and the second end of body 330 of supplying gas connects with air-blowing cavity 321.Court on air-blowing plate body 350 Sidewall to stirring paddle 240 offers some air-blowing holes 352, and some air-blowing holes 352 all connect with air-blowing cavity 351, and air-blowing Acute angle is formed between bearing of trend and the central axis of kettle 100 in hole 352.
It should be noted that when mixing component 200 is stirred operation to the material in kettle 100, now, open drum Air-pump 320, is extracted out the air of the upper cover 110 of kettle 100 by the air-blowing pump housing 320 and body 310 of bleeding, and again leads to Cross the air-blowing pump housing 320 to blast to supplying gas in body 330 from the air that the upper cover of kettle 100 is extracted out, and blast further to The air-blowing cavity 321 of air-blowing plate body 350 is internal, finally, then by the some air-blowing holes 352 connected with air-blowing cavity 321 by air-flow Blast to the material of low head 120 being positioned at kettle 100, so, in conjunction with the mixing component 200 stirring operation to material, By air-blowing electric hybrid module 300, the material in stirring is blasted the air in kettle 100 again, it is possible to improve flow-disturbing effect further Really, and during air-blowing, it is possible to strengthen the exposure level between each material, for improving the mixing effect of material further Really, it is used for improving reaction efficiency.
Additionally, due to air-blowing hole 352 is towards stirring 240 setting, and in the bearing of trend in air-blowing hole 352 and kettle 100 Forming acute angle between mandrel line, so, air-blowing hole 352 can spray gases at high pressure to the stirring paddle 240 in rotating, and is used for washing away Stick to the viscous material of stirring paddle 240, or wash away the viscous material of adhesive tendencies, stick on stirring paddle 240 as washed away The material of resinae, and then viscous material can be reduced stick to the situation of stirring paddle 240 and occur.
Above-mentioned highly effective reaction device 10 by arranging kettle 100, mixing component 200 and air-blowing electric hybrid module 300, and Under the synergism of mixing component 200 and air-blowing electric hybrid module 300, it is possible to reach preferable material mixed effect, additionally, pass through The air-blowing electric hybrid module 300 gas shock to stirring paddle 240, it is possible to minimizing viscous material sticks to the situation of stirring paddle 240 and sends out Raw.
The problem being sputtered onto in described exhaust tube body to reduce the material within described kettle occurs, and then can reduce Described air-blowing electric hybrid module is occurred by the problem of feed blocking, such as, refers to Fig. 3, and described highly effective reaction device also includes thing Material intercepts assembly 400, and material intercepts assembly 400 and is positioned at inside described kettle, and described material intercepts assembly 400 and includes intercepting body 410 and connection pipe body 420, the first end of described connection pipe body 420 is spirally connected with the first end of body 310 of bleeding, described connecting tube Second end of body 420 is spirally connected with the first end of described obstruct body 410, and the second end of described obstruct body is towards described shaft Arranging, the bearing of trend of described obstruct body forms angle with the central axis of described kettle, and described obstruct body is towards institute The direction stating stirring paddle is gradually obliquely installed.Described connection pipe body has round tubular structure, the first end of described connection pipe body Lateral wall offer the first external screw thread, the lateral wall of the second end of described connection pipe body offers the second external screw thread, described in take out The medial wall of the first end of trachea body offers the first female thread, and the medial wall of the first end of described obstruct body offers second Female thread, described first female thread and described first external thread bolt connection, described second female thread and described second external thread bolt connection; And for example, described connecting tube is positioned at the pipe diameter size of its first end equal to the pipe diameter size being positioned at its second end;And for example, described obstruct The medial wall of body is provided with some projections;And for example, some described protruding circular array are distributed in the interior of described obstruct body On sidewall;And for example, the end of described projection has semicircle spherical structure;And for example, the first end of described obstruct body and described company The position that is spirally connected of the second end of adapter body is provided with sealant layer, so, utilizes described obstruct body to enter the material of sputtering Row intercepts or stops, it is possible to reduce the problem generation that the material within described kettle is sputtered onto in described exhaust tube body, Jin Erke Occurred by the problem of feed blocking with the described air-blowing electric hybrid module of minimizing.
The problem being sputtered onto in described exhaust tube body to reduce the material within described kettle occurs, and then can reduce Described air-blowing electric hybrid module is occurred by the problem of feed blocking, such as, refers to Fig. 4, and described highly effective reaction device also includes thing Material filter assemblies 500, described material filtering assembly 500 includes framework 510 and drainage screen 520, and described framework has both ends open Hollow structure, the first end opening of described framework is connected with the medial wall of described upper cover, and the first of described framework 510 End opening connects with the first end of described body 310 of bleeding, and described filtering screen is located at the opening position of the second end of described framework Put place.The first end of body of bleeding is provided with some buckles, if the edge of opening position of the first end of described framework is provided with Dry button bit, button bit described in each described buckle one_to_one corresponding and fastens;And for example, described buckle is provided with the portion of setting, described button Position is provided with and sets hole, described in the portion of setting be embedded at described in set in hole;And for example, described drainage screen includes drainage screen body and consolidates Determining ring body, the edge of described drainage screen body is connected with the medial wall of described fixing ring body, the lateral wall of described fixing ring body with Connect at second end opening marginal position of described framework;And for example, the medial wall of described framework is provided with some reinforcements;Again As, described reinforcement is extended to the second end of described framework by the first end of described framework;And for example, described reinforcement has spiral Shape structure, so, utilizes filtration or the iris action of described drainage screen, it is possible to reduce the material within described kettle and be sputtered onto Problem in described exhaust tube body occurs, and then can reduce described air-blowing electric hybrid module and occurred by the problem of feed blocking.
In order to preferably collect the material entered in described air-blowing electric hybrid module, to alleviate feed blocking problem, such as, Referring to Fig. 5, described highly effective reaction device also includes that material recycle assembly 600, described material recycle assembly 600 include recovery tube Body 610 and hold tank body 620, described in supply gas and offer leakage mouth 331 on body 330, the first end of described recovery body 610 with Described leakage mouth 331 connects, described in hold tank body be the hollow structure with one end open, formed in it and hold cavity, described The second end reclaiming body is connected with the described aperture position holding tank body at, and the second end of described recovery body and described Sheng Put cavity connection.Described recovery body has round tubular structure;And for example, to offer drain oblique in the medial wall of described recovery body Face, described drain inclined-plane is obliquely installed to the central axis near described recovery body;And for example, described drain inclined-plane offers Drainage trough, described drainage trough is extended to the direction of the second end of described recovery body by the first end of described recovery body; And for example, hold tank body described in and offer liquid outlet away from the end of described recovery body;And for example, described material recycle assembly also wraps Including adapter body, described adapter body connects with described liquid outlet;And for example, at described adapter body position, it is provided with valve, this Sample, by reclaiming body 610 and holding tank body 620, it is possible to preferably collect the material entering in described air-blowing electric hybrid module, Supply gas as described in enter to the material of tubular body, to alleviate feed blocking problem.
In order to improve stirring and mixing effect further, and the problem that minimizing viscous material sticks on described stirring paddle is sent out Raw, such as, refer to Fig. 6, described highly effective reaction device also includes assisting mixing component 700, and described auxiliary mixing component 700 wraps Including mounting bar 710 and broken stream wedge 720, described mounting bar 710 has installed surface 711 and a binding face 712, described installed surface 711 with The lateral wall of described stirring paddle 240 connects, and described binding face 712 is connected with the bottom of described broken stream wedge 720, described broken stream wedge The 720 broken stream curved surfaces 721 with two arc-shaped curved surface structures, described broken stream curved surface 721 by the bottom of described broken stream wedge 720 to institute The direction, tip stating brokenly stream wedge is extended, and two described broken stream curved surfaces divide axisymmetricly with the central axis of described broken stream wedge Cloth.Described broken stream curved surface has arc-shaped curved surface structure;And for example, described broken stream curved surface offers brokenly chute, and described broken chute is by institute The bottom stating brokenly stream wedge is extended to the direction, tip of described broken stream wedge;And for example, described broken chute has triangular structure Cross section;And for example, described installed surface is provided with some installation raised lines, and it is recessed that the lateral wall of described stirring paddle offers some installations Groove, each described installation raised line one_to_one corresponding is embedded at installation inside grooves described in;And for example, described installation raised line has rectangle The cross section of structure;And for example, described installed surface arranges at least three described installation raised lines, so, utilizes the broken of broken stream wedge 720 Stream curved surface 721 can preferably cater to the high pressure draught that described air-blowing hole bloats, and e.g., plays and high pressure draught plays guiding work With, so, it is possible to improve further stirring and mixing effect, and the problem that minimizing viscous material sticks on described stirring paddle is sent out Raw.
In order to reduce the material vortex phenomenon when stirring married operation, and improve flow-disturbing effect further, be used for carrying High stirring and mixing effect, such as, refers to Fig. 7, and described highly effective reaction device also includes that baffling assembly 800, baffling assembly 800 wrap Include the medial wall of the described low head 120 of some baffling bodies of rod 810, the first end of the described baffling body of rod 810 and described kettle 100 Connecting, the second end of the described baffling body of rod 810 is connected away from the side in described air-blowing hole with described air-blowing plate body 350, and adjacent It is provided with interval between two described baffling bodies of rod;And for example, the described baffling body of rod has hollow-core construction;And for example, described rod baffle Body has the cross section of regular polygon structure;And for example, the described baffling body of rod has the cross section of regular hexagon structure;And for example, institute State and on the sidewall of the baffling body of rod, offer some through holes;And for example, some described through holes with the central axis of the described baffling body of rod in Radial distribution;And for example, described upper cover offers the services aperture that connect internal with described kettle, so, utilizes some institutes State the baffling body of rod 810 material in whipping process is stopped, e.g., the material under centrifugal action is stopped, energy Enough reduce the material vortex phenomenon when stirring married operation, and improve flow-disturbing effect further, be used for improving stirring mixing Effect.
When it is pointed out that being stirred each material of married operation inside described kettle carries out combination reaction, and Most combination reaction is all exothermic reaction, and the productivity that the speed of reaction and product generate is also required to releasing during dependent reaction Heat, is used for improving reaction rate and productivity.Additionally, in whipping process, material can be done work by described mixing component, i.e. material During being mutually mixed agitation, show as outwardly releasing the material that heat, especially toughness are stronger, its exothermic phenomenon Become apparent from, therefore, based on above-mentioned situation, rely on the combination reaction of higher temperature for some, as depended on reaction self-heat generation With the combination reaction of stirring heat production, and need not extra heater for the reaction that it heats, it is especially desirable to guarantee The heat-insulating property of described kettle.Further, in order to for some acid materials, therefore, to assure that the medial wall of described kettle, i.e. The medial wall of the described kettle directly contacted with acid material possesses higher resistance to acid attack performance, for prolonging making of raw described kettle With being normally carried out of life-span and reaction.Further, the lateral wall of described kettle is owing to often contacting with corrosive materials, e.g., The corrosive materials contact of the form such as gaseous state or liquid, it is therefore desirable to possess preferable decay resistance, for preferably protecting Described kettle.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described kettle, such as, refer to Fig. 8, described Kettle, e.g., resistance to acid attack layer 130 that the sidewall of described kettle includes being cascading, heat-insulation layer 140, supporting layer 150, counterweight Layer 160 and protective layer 170, described resistance to acid attack layer is positioned at the medial wall of described kettle, and described resistance to acid attack layer is direct and material, As, acid material contact, described protective layer is positioned at the lateral wall of described kettle, and the most described protective layer is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts~88 parts, titanium 30 Part~34 parts, chromium 20 parts~25 parts, antimony 2.5~3.4 parts, copper part 2.3~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 Part, 0.15 part~0.27 part of carbon, silicon 0.25 part~0.46 part, boron 0.12 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.
Use ferrum 75 parts~88 parts, titanium 30 parts~34 parts and chromium 20 parts~25 parts as basis, the basis unit of resistance to acid attack layer Element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding antimony 2.5~3.4 parts, copper 2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 parts, cobalt 0.04 part~0.09 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 part compound, additionally it is possible to optimize further The properties of described resistance to acid attack layer, especially can optimize the resistance to acid attack performance of described resistance to acid attack layer further such that it is able to Better against the acid etching of material, for improving the service life of described kettle further and guaranteeing being normally carried out of reaction.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts~80 parts, titanium 33 parts~34 parts, chromium 24 parts~25 parts, antimony 2.7~3.4 parts, copper 2.7 parts~3.4 parts, 1.8 parts~2.5 parts of zinc, aluminum 1.1~1.4 Part, 0.18 part~0.27 part of carbon, silicon 0.27 part~0.46 part, boron 0.13 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts, titanium 33 parts, Chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon 0.46 part, boron 0.18 part, cobalt 0.04 part, phosphorus 0.03 part, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04 part, scandium 0.01 part and 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts~22 parts, white Cotton 8~20 parts, rock wool 8 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 parts~ 4.5 parts, basalt fibre 1 part~3 parts, rubber foam 3~5 parts, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1 Part~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~2 parts, polypropylene fiber 3~4 parts, Thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when in described kettle During the material generation exothermic reaction in portion, and after transferring heat to described resistance to acid attack layer, have good based on described heat-insulation layer Heat insulation and heat-insulating property, can limit heat and be further transmitted through described kettle, and then avoid heat to be transferred directly to external environment In, it is ensured that the material within described kettle reacts at a suitable temperature, for improving the product of reaction rate and product Rate.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts~21 parts, White cotton 17~20 parts, rock wool 10 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 Part~4.5 parts, basalt fibre 1 part~2.5 parts, rubber foam 3.5~5 parts, 1.5 parts~2 parts of magnesium hydroxide, aminopropyl three second TMOS 1.5 parts~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~1.4 parts, third Synthetic fibre fiber 3.3~4 parts, thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts, white cotton 17 ~20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts, basalt fibre 2.1 parts, rubber Foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2 parts, aluminium oxide 1.8 parts, 3,5-di-t-butyl-4-hydroxyl Essence of Niobe 1.4 parts, polypropylene fiber 4 parts, thiorubber. 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts~98 parts, manganese 0.4 Part~0.95 part, molybdenum 0.1 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.06 part~0.25 part of carbon, Silicon 0.1 part~0.3 part, 0.05 part~0.1 part of phosphorus, boron 0.001 part~0.01 part, hafnium 0.05 part~0.5 part, scandium 0.05 part~ 0.3 part, chromium 0.05 part~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part.
It is appreciated that to make described kettle possess preferable heat-insulating property, needs to introduce described heat-insulation layer, and described guarantor The mechanical strength of temperature layer is poor, in order to strengthen the integrally-built mechanical strength of described kettle, needs to introduce described supporting layer so that it is Directly contact with described heat-insulation layer, be used for improving the integrally-built mechanical strength of described kettle, to reach the purpose of safety in production. Based on above-mentioned situation, this is necessary for requiring that described supporting layer possesses higher mechanical strength and anti-deformation nature, by using such as Improving quality each component of part, the most described supporting layer contains hafnium 0.05 part~0.5 part, scandium 0.05 part~0.3 part, chromium 0.05 part ~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part, The mechanical strength of conventional iron alloy can be improved so that it is mechanical strength and anti-deformation nature are more excellent, it is possible to meet requirement.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts~98 parts, manganese 0.55 part~0.95 part, molybdenum 0.35 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.17 part of carbon~ 0.25 part, silicon 0.1 part~0.25 part, 0.05 part~0.1 part of phosphorus, boron 0.008 part~0.01 part, hafnium 0.1 part~0.5 part, scandium 0.1 Part~0.3 part, chromium 0.1 part~0.3 part, 0.02 part~0.05 part of nickel, cerium 0.02 part~0.05 part, thorium 0.02 part~0.05 part and Zirconium 0.02 part~0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, 0.75 part of manganese, Molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus, boron 0.008 part, hafnium 0.5 part, scandium 0.2 Part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part and 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts~95 parts of tungsten, 30 parts of nickel ~60 parts, ferrum 15 parts~40 parts, chromium 1.5 parts~10 parts, 1.5 parts~10 parts of lead, copper 1 part~6 parts and molybdenum 0.5 part~5 parts.
It is appreciated that in producing course of reaction, needs the material in described kettle carries out the stirring behaviour that intensity is higher Make, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid the integrally-built matter of described kettle Amount kicks the beam, and then reduces the external impacts impact on described kettle, i.e. can reduce described kettle and concussion or displacement problem occur. The each component using as above mass parts can make described weight coating possess excellent counterweight performance, it is possible to effectively increases described still The integrally-built weight of body so that it is identical or adaptive with the weight of traditional kettle, such that it is able to the peace improved in production process Full performance.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts~95 parts of tungsten, nickel 30 Part~45 parts, ferrum 27 parts~40 parts, chromium 1.5 parts~2.3 parts, 1.5 parts~3.3 parts of lead, copper 1 part~5.5 parts and molybdenum 0.5 part~ 4.9 part.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, 38 parts of nickel, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts~80 parts, lithium 16~ 18 parts, 18 parts~25 parts of nickel, molybdenum 3.5 parts~4 parts, chromium 2 parts~5 parts, cobalt 1 part~5 parts, vanadium 1 part~5 parts, 1 part~2 parts of manganese, iridium 0.8 part~2.5 parts, niobium 0.5 part~2.5 parts, scandium 0.3 part~2.5 parts, 0.2 part~2.5 parts of strontium, caesium 0.2 part~2.5 parts, tungsten 0.2 part~2.5 parts and titanium 0.2 part~2.5 parts.
Be appreciated that the lateral wall of described kettle owing to often contacting with corrosive materials, e.g., the form such as gaseous state or liquid Corrosive materials contact, it is therefore desirable to possess preferable decay resistance, for preferably protecting described kettle.By as above Each component of mass parts, can make described protective layer possess good Corrosion Protection, and then preferably protect described kettle, uses The service life extending described kettle.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts~70 parts, lithium 16 Part~16.5 parts, nickel 18~21 parts, molybdenum 3.5 parts~3.9 parts, chromium 2 parts~4.4 parts, cobalt 1 part~3.9 parts, vanadium 1 part~4.5 parts, 1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, niobium 0.5 part~2.2 parts, scandium 0.3 part~2.3 parts, 0.2 part~2.3 parts of strontium, caesium 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium 0.2 part~1.9 parts.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium 16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, 2.3 parts of iridium, niobium 2.2 parts, scandium 2.3 parts, strontium 2.3 Part, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described kettle further, e.g., the structure of the sidewall of described kettle, such as, described resistance to acid attack layer, described The thickness of heat-insulation layer, described supporting layer, described weight coating and described protective layer is than being (1~1.5): (15~20): (5~5.5): (8~9.8): (0.5~1.2);And for example, the thickness of described weight coating and described protective layer is than for 1:15:5:9.5:1.1.
It should be noted that other embodiments of the present invention also include that the technical characteristic in the various embodiments described above be combined with each other Can be formed, and the highly effective reaction device that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, not to above-mentioned reality The all possible combination of each technical characteristic executed in example is all described, but, as long as the combination of these technical characteristics is not deposited In contradiction, all it is considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed, but Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that, for the ordinary skill people of this area For Yuan, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these broadly fall into the present invention's Protection domain.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (7)

1. a highly effective reaction device, it is characterised in that including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head;
Mixing component, described mixing component includes installing rack, stirring motor, shaft and stirring paddle, the fixing peace of described installing rack Being contained on described upper cover, the first end of described shaft is connected with the rotary shaft of described stirring motor, the of described shaft Two ends stretch to inside described kettle, and the second end of described shaft is connected with described stirring paddle, and described stirring motor is used for carrying Dynamic described stirring paddle rotates;
Air-blowing electric hybrid module, described air-blowing electric hybrid module includes bleed body, the air-blowing pump housing, body of supplying gas, fixed mount and air-blowing Plate body, described in bleed the first end of body connect with described upper cover, described in bleed the second end of body and the described air-blowing pump housing Inlet end connection, described in the first end of body of supplying gas connect with the outlet side of the described air-blowing pump housing, described fixed mount is arranged on On the medial wall of described low head, described air-blowing plate body fixes with described fixed mount, and described air-blowing plate body is placed in described In kettle, described air-blowing plate body has arcuate structure, and in it, hollow is arranged, and is provided with air-blowing cavity, institute in described air-blowing plate body The second end stating body of supplying gas is connected with described air-blowing plate body, and described in supply gas body the second end and described air-blowing cavity even Logical, on described air-blowing plate body, the sidewall towards described stirring paddle offers some air-blowing holes, and some described air-blowing holes are all with described Air-blowing cavity connects, and forms acute angle between the bearing of trend in described air-blowing hole and the central axis of described kettle;And
Material intercepts assembly, and described material intercepts assembly and is positioned at inside described kettle, and described material intercepts assembly and includes connecting tube Body and obstruct body, the first end of described connection pipe body is spirally connected with the first end of body of bleeding, the second end of described connection pipe body Being spirally connected with the first end of described obstruct body, the second end of described obstruct body is arranged towards described shaft, described obstructing tube The central axis of the bearing of trend of body and described kettle forms angle, and described obstruct body towards described stirring paddle direction by Gradually it is obliquely installed.
Highly effective reaction device the most according to claim 1, it is characterised in that described connection pipe body has round tubular knot Structure, the lateral wall of the first end of described connection pipe body offers the first external screw thread, the lateral wall of the second end of described connection pipe body Offer the second external screw thread, described in the bleed medial wall of the first end of body offer the first female thread, described obstruct body The medial wall of the first end offers the second female thread, described first female thread and described first external thread bolt connection, in described second Screw thread and described second external thread bolt connection.
Highly effective reaction device the most according to claim 2, it is characterised in that described connecting tube is positioned at the caliber of its first end Size is equal to the pipe diameter size being positioned at its second end.
Highly effective reaction device the most according to claim 1, it is characterised in that if the medial wall of described obstruct body is provided with Dry projection.
Highly effective reaction device the most according to claim 4, it is characterised in that some described protruding circular array are distributed in On the medial wall of described obstruct body.
Highly effective reaction device the most according to claim 5, it is characterised in that the end of described projection has semicircle spherical junctions Structure.
Highly effective reaction device the most according to claim 1, it is characterised in that the first end of described obstruct body and described company The position that is spirally connected of the second end of adapter body is provided with sealant layer.
CN201610509748.3A 2016-06-30 2016-06-30 Highly effective reaction device Expired - Fee Related CN106040144B (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104877889A (en) * 2014-02-28 2015-09-02 北京化工大学 Method and device for fermented coupled steam penetration in-situ separation of volatile organic compounds

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104877889A (en) * 2014-02-28 2015-09-02 北京化工大学 Method and device for fermented coupled steam penetration in-situ separation of volatile organic compounds

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