CN106038353A - A cream facial mask containing nanometer graphene and pectin and a preparing method thereof - Google Patents

A cream facial mask containing nanometer graphene and pectin and a preparing method thereof Download PDF

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Publication number
CN106038353A
CN106038353A CN201610263822.8A CN201610263822A CN106038353A CN 106038353 A CN106038353 A CN 106038353A CN 201610263822 A CN201610263822 A CN 201610263822A CN 106038353 A CN106038353 A CN 106038353A
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parts
pectin
mastic
facial film
weight
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CN201610263822.8A
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曾新民
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Zeng Xinmin
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Cosmetics (AREA)

Abstract

A cream facial mask containing nanometer graphene and pectin, having antibacterial effects and capable of removing acne and diminishing inflammation and a preparing method thereof are provided. The facial mask comprises 0.03-0.1 part by weight of the nanometer graphene and 15-18 parts by weight of the pectin. According to the facial mask and the method, the nanometer graphene which is a physical sterilizing component is added, and therefore bacteria do not generate drug resistance, and the facial mask has acne-removing and inflammation-diminishing effects for skin and has good effects on chronic inflammatory whelk for teenagers.

Description

A kind of containing nano-graphene pectin mastic facial film and preparation method thereof
Technical field
The present invention relates to a kind of facial film and preparation method thereof, especially a kind of containing nano-graphene pectin mastic facial film and Preparation method.
Background technology
Product for resolving poxes in the market often contains ethanol, salicylic acid or chloromycetin etc. and illegally adds antibiotic and hormone, People is known from experience generation drug resistance, even life threatening.
Summary of the invention
The invention provides pectin mastic facial film of a kind of antibacterial effect, acne-removing inflammation-diminishing and preparation method thereof.
Realize the pectin mastic facial film of the object of the invention, including by weight proportion: nano-graphene 0.03～0.1 part and fruit Glue 15～18 parts.
Further, also include part by weight: hyaluronate sodium 0.1 part and deionized water 50～54 parts,
Further, part by weight is also included: sea mud 15 parts and allantoin 0.3 part.
Further, part by weight is also included: glycerol 5 parts and Jojoba oil 5 parts.
Further, part by weight is also included: mud pool tortoise beetle ester 0.1 part and mud moor gold ethyl ester 0.1 part.
Further, part by weight is also included: glyceryl stearate and PEG-100 stearate 2.5～3 parts, spermaceti is hard Lipidol 0.5～1.5 parts and stearic acid 1.5 parts.
Further, part by weight is also included: tocopherol Vitamin E 0.5～1.0 parts, 0.1 part of essence.
Realize the object of the invention two the preparation method of pectin mastic facial film, comprise the steps:
(1) preparation of aqueous phase: weight ratio is divided in the deionized water that 0.1 part of hyaluronate sodium joins 50 parts, heating Transparent to 80～85 DEG C of dissolvings, add 15～18 parts of pectin, 15 parts of sea muds, 5 parts of glycerol, 0.1 part of mud pool tortoise beetle ester and 0.3 part Allantoin mixes；
(2) preparation of oil phase: by 2.5～3 parts of glyceryl stearate and PEG-100 stearate, 0.5～1.5 part of spermaceti Stearyl alcohol, 1.5 parts of stearic acid, 5 parts of Jojoba oil, 0.03～0.1 part of nano-graphene and 0.1 part of mud moor gold ethyl ester mixing heating To 80～85 DEG C, fully melt, standby；
(3) preparation of mastic: described aqueous phase and oil phase are mixed, maintains the complete emulsifying in 5 minutes of 80～85 DEG C of homogenizing, cooling To room temperature, ageing, obtain pectin mastic facial film.
Further, the heating-up temperature in described step (1) and step (2) is 80 DEG C.
Further, in described step (3), described aqueous phase and described oil phase are heated to 5 minutes complete breasts of 80 DEG C of homogenizing Change, after be cooled to 45 DEG C, add weight be divided into 0.5～1.0 part of tocopherol Vitamin E, 0.1 part of essence, stir, cold But to room temperature, ageing, obtain mastic facial film.
Having the beneficial effect that of the pectin mastic facial film of the present invention and preparation method thereof:
Pectin mastic facial film of the present invention and preparation method thereof, with the addition of nano-graphene physical sterilization composition, allows antibacterial Drug resistance will not be produced, skin is had good acne-removing inflammation-diminishing effect；Comedo teen-age to chronic inflammation (is also Cuo Skin ulcer) there is good effect.
Use natural pectin can repair the effect of small pox surrounding tissue simultaneously, make chronic inflammatory disease heal, moreover it is possible to whitening nutrition Skin.
This facial film preparation method is simple, economical and efficient, manufacturing cycle are short, and natural pollution-free, product property is stable, emulsifying effect The best.
Detailed description of the invention
Embodiment 1
The preparation method containing nano-graphene pectin mastic facial film of the present embodiment, comprises the following steps:
A) preparation of aqueous phase: weight ratio is divided in the deionized water that 0.1 part of hyaluronate sodium joins 54 parts, is heated to 80-85 DEG C of dissolving is transparent, adds 15 parts of pectin, 15 parts of sea muds, 5 parts of glycerol, 0.1 part of mud pool tortoise beetle ester 0.3 part of allantois of mixing Element mixing；
Hyaluronate sodium at such a temperature, can ensure the abundant sterilizing of product, and solution temperature is less than 80 DEG C, and sterilizing is not Completely, temperature is higher than 85 DEG C, uprises for horsepower requirements, is also easily destroyed the stability of each composition.Natural pectin can be repaired The effect of small pox surrounding tissue, makes chronic inflammatory disease heal, moreover it is possible to whitening nutrition skin；Sea mud, allantoin are to injured skin simultaneously There is the calm effect repairing nutrition；The present invention applies can film in flakes in face about 25 minutes, it is easier to cleaning；
B) preparation of oil phase: by 2.5 parts of glyceryl stearate and PEG-100 stearate, 1 part of cetearyl alcohol, 1.5 parts Stearic acid, 5 parts of Jojoba oil, 0.03 part of nano-graphene and 0.1 part of mud moor gold ethyl ester mixing are heated to 80-85 DEG C, fully melt Change, standby；
Nano-graphene physical sterilization composition, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing to imitate to skin Really, Jojoba oil has a high-temperature stability, and can osmotic absorption and softening skin cutin rapidly, allowing skin become softness has bullet Property；Emulsifying that glyceryl stearate and PEG-100 stearate, cetearyl alcohol and stearic acid have had and lubricant effect.
C) preparation of mastic: described aqueous phase and oil phase are mixed, maintains the complete emulsifying in 5 minutes of 80 degrees Celsius of homogenizing, cooling To 45 DEG C, add weight and be divided into 0.5 part of tocopherol Vitamin E, 0.1 part of essence, be sufficiently stirred for, be cooled to room temperature, ageing, obtain A kind of pectin mastic facial film Han nano-graphene.
Tocopherol Vitamin E has a murder by poisoning from free radical of the anti-oxidation protection body cell, prevention of inflammation dermatoses, Protect the skin from the injury of ultraviolet and pollution, reduce the deposition of cicatrix and pigment；Accelerate the Healing of wound, skin can be made The smooth exquisiteness of skin, the appearance retained youth.
Embodiment 2
The preparation method of the pectin mastic facial film of the present embodiment, comprises the following steps:
A) preparation of aqueous phase: weight ratio is divided in the deionized water that 0.1 part of hyaluronate sodium joins 50 parts, is heated to 80-85 DEG C of dissolving is transparent, adds 18 parts of pectin, 15 parts of sea muds, 5 parts of glycerol, 0.1 part of mud pool tortoise beetle ester 0.3 part of allantois of mixing Element mixing；
B) preparation of oil phase: by 3 parts of glyceryl stearate and PEG-100 stearate, 1 part of cetearyl alcohol, 1.5 parts hard Fat acid, 5 parts of Jojoba oil, 0.05 part of nano-graphene and 0.1 part of mud moor gold ethyl ester mixing are heated to 80-85 DEG C, fully melt, Standby；
C) preparation of mastic: described aqueous phase and oil phase are mixed, maintains the complete emulsifying in 5 minutes of 80 homogenizing, be cooled to 45 DEG C, Add weight and be divided into 1 part of tocopherol Vitamin E, 0.1 part of essence, be sufficiently stirred for, be cooled to room temperature, ageing, obtain a kind of containing receiving Rice Graphene pectin mastic facial film.
Embodiment 2 film more in blocks than embodiment 1 is good.
Embodiment 3
The preparation method of the pectin mastic facial film of the present embodiment the present embodiment is substantially the same manner as Example 2, except for the difference that: Step b is also added into 0.06 part of nano-graphene；
Embodiment 4
The preparation method of the pectin mastic facial film of the present embodiment the present embodiment is substantially the same manner as Example 2, except for the difference that: Step b is also added into 0.1 part of nano-graphene；
Use case:
Use the Contrast on effect case such as following table institute of pectin mastic facial film and preparation method thereof of embodiment 1 and commercially available facial film Show: as shown in the table: (commercially available facial film without the composition of stone nano-graphene, other all in the presence of)
Knowable to above concrete case, obvious containing nano-graphene pectin mastic facial film anti-acne repairing effect, natural stingless Swash, it is possible to be effectively improved the skin problem that comedo brings, whitening anti-acne, nutrition skin can be played simultaneously, repair skin Effect.
Nano-graphene can kill 10 various bacteria such as bacillus pyocyaneus, escherichia coli, this is because nano-graphene this Body is the carbon atom strung, and just as one layer of the most closely knit cloth the thinnest, they tackle the mode of antibacterial 3 kinds: the first is Directly cutting, owing to Graphene is nano level, and antibacterial is micron order, and the former is less 1000 times than the latter, and Graphene is as same The sharpest cutter, directly antibacterial is cut to death；The second is antibacterial hungry to death, and nano level Graphene can be by antibacterial as cloth Wrap up closely, make antibacterial absorb less than nutrition, die of starvation；The third is slowly to wither away, owing to Graphene is the least, carefully Graphene can be gulped down enter " tripe " inner by bacterium, can suffer from diarrhea uncomfortable just as people has eaten foreign body, cause antibacterial slowly to be withered away, exactly because This physical sterilization method of Graphene, allows antibacterial will not produce drug resistance, has good acne-removing inflammation-diminishing effect to skin.
Pectin is a kind of natural polymer, and it is substantially a kind of linear polysaccharide polymer, containing having hundreds to About thousand Anhydrogalactose. aldehydic acid residues, its corresponding average molecular mass is 50000-150000, and skin is had very by it Whitening well, reparation, nutritive validity.
Embodiment described above is only to be described the preferred embodiment of the present invention, the not model to the present invention Enclosing and be defined, under design spirit premise without departing from the present invention, this area ordinary skill technical staff is to the technology of the present invention side Various deformation that case is made and improvement, all should fall in the protection domain that claims of the present invention determines.

Claims (10)

1. a pectin mastic facial film Han nano-graphene, including by weight proportion: nano-graphene 0.03～0.1 part and pectin 15～18 parts.
Pectin mastic facial film the most according to claim 1, it is characterised in that: further, also include part by weight: transparent 0.1 part of matter acid sodium and deionized water 50～54 parts.
Pectin mastic facial film the most according to claim 1, it is characterised in that: also include part by weight: sea mud 15 parts and urine Bursin 0.3 part.
Pectin mastic facial film the most according to claim 1, it is characterised in that: also include part by weight: glycerol 5 parts and lotus lotus Bar oil 5 parts.
Pectin mastic facial film the most according to claim 1, it is characterised in that: also include part by weight: mud moors tortoise beetle ester 0.1 Part and mud moor gold ethyl ester 0.1 part.
Pectin mastic facial film the most according to claim 1, it is characterised in that: also include part by weight: glyceryl stearate With PEG-100 stearate 2.5～3 parts, cetearyl alcohol 0.5～1.5 parts and stearic acid 1.5 parts.
7. according to the arbitrary described pectin mastic facial film of claim 1～6, it is characterised in that: also include part by weight: tocopherol Vitamin E 0.5～1.0 parts, 0.1 part of essence.
8. the preparation method containing nano-graphene pectin mastic facial film, comprises the steps:
(1) preparation of aqueous phase: weight ratio is divided in the deionized water that 0.1 part of hyaluronate sodium joins 50 parts, is heated to 80 ～85 DEG C of dissolvings are transparent, add 15～18 parts of pectin, 15 parts of sea muds, 5 parts of glycerol, 0.1 part of mud pool tortoise beetle ester and 0.3 part of allantois Element mixing；
(2) preparation of oil phase: by 2.5～3 parts of glyceryl stearate and PEG-100 stearate, 0.5～1.5 part of cetearyl alcohol Alcohol, 1.5 parts of stearic acid, 5 parts of Jojoba oil, 0.03～0.1 part of nano-graphene and 0.1 part of mud moor gold ethyl ester mixing are heated to 80 ～85 DEG C, fully melt, standby；
(3) preparation of mastic: described aqueous phase and oil phase are mixed, maintains the complete emulsifying in 5 minutes of 80～85 DEG C of homogenizing, be cooled to room Temperature, ageing, obtain pectin mastic facial film.
The preparation method of pectin mastic facial film the most according to claim 8, it is characterised in that: described step (1) and step (2) heating-up temperature in is 80 DEG C.
The preparation method of pectin mastic facial film the most according to claim 8 or claim 9, it is characterised in that: in described step (3) In, described aqueous phase and described oil phase are heated to the complete emulsifying in 5 minutes of 80 DEG C of homogenizing, after be cooled to 45 DEG C, add weight be divided into 0.5～1.0 part of tocopherol Vitamin E, 0.1 part of essence, stir, be cooled to room temperature, ageing, obtains mastic facial film.
CN201610263822.8A 2016-04-26 2016-04-26 A cream facial mask containing nanometer graphene and pectin and a preparing method thereof Pending CN106038353A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107397689A (en) * 2017-07-12 2017-11-28 贵州九立德生物制药有限公司 A kind of preparation for skin nursing and preparation method thereof
CN108294977A (en) * 2018-01-26 2018-07-20 湖南御茯堂健康管理咨询有限公司 A kind of graphene black jade facial mask
CN108567578A (en) * 2018-07-25 2018-09-25 四川大学 It is used to prepare the lotion and preparation method thereof of facial mask
CN109288691A (en) * 2018-11-02 2019-02-01 广东墨睿科技有限公司 A kind of graphene facial mask and preparation method thereof
IT201800005481A1 (en) * 2018-05-17 2019-11-17 Non-permanent compositions based on graphene for the coloring and strengthening treatment of the hair

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101849894A (en) * 2010-06-11 2010-10-06 上海丽思化工科技有限公司 CO2 sustained release foam mask and preparation method thereof
CN104257527A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Moisturizing facial cleanser and preparation method thereof
CN104382747A (en) * 2014-11-29 2015-03-04 济南班德瑞生物科技有限公司 Mask containing muyu stone
CN105287248A (en) * 2015-11-18 2016-02-03 张建刚 Graphene oxide mask and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101849894A (en) * 2010-06-11 2010-10-06 上海丽思化工科技有限公司 CO2 sustained release foam mask and preparation method thereof
CN104257527A (en) * 2014-10-22 2015-01-07 广东幸美化妆品股份有限公司 Moisturizing facial cleanser and preparation method thereof
CN104382747A (en) * 2014-11-29 2015-03-04 济南班德瑞生物科技有限公司 Mask containing muyu stone
CN105287248A (en) * 2015-11-18 2016-02-03 张建刚 Graphene oxide mask and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107397689A (en) * 2017-07-12 2017-11-28 贵州九立德生物制药有限公司 A kind of preparation for skin nursing and preparation method thereof
CN108294977A (en) * 2018-01-26 2018-07-20 湖南御茯堂健康管理咨询有限公司 A kind of graphene black jade facial mask
IT201800005481A1 (en) * 2018-05-17 2019-11-17 Non-permanent compositions based on graphene for the coloring and strengthening treatment of the hair
WO2019219471A1 (en) 2018-05-17 2019-11-21 Prodotti Gianni S.R.L. Non-permanent graphene-based compositions for hair coloring and strengthening treatment
CN108567578A (en) * 2018-07-25 2018-09-25 四川大学 It is used to prepare the lotion and preparation method thereof of facial mask
CN109288691A (en) * 2018-11-02 2019-02-01 广东墨睿科技有限公司 A kind of graphene facial mask and preparation method thereof

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Application publication date: 20161026