CN106012584B - A kind of alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric - Google Patents
A kind of alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric Download PDFInfo
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- CN106012584B CN106012584B CN201610437609.4A CN201610437609A CN106012584B CN 106012584 B CN106012584 B CN 106012584B CN 201610437609 A CN201610437609 A CN 201610437609A CN 106012584 B CN106012584 B CN 106012584B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/003—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated using vat or sulfur dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/028—Material containing basic nitrogen using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8219—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and amide groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a kind of alkali bath method colouring methods of 56 fibers of polyamide fibre/cotton blended spinning face fabric.This method comprises the following steps: being dyed using reducing dye or reactive dye to 56 fibers of polyamide fibre/cotton blended spinning face fabric；56 fibers of the polyamide fibre/cotton blended spinning face fabric is the blended yarn weaved fabric of polyamide fibre 56 and cotton fiber.In the alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric of the present invention, with Covalent bonding together, fastness is better than what acid bath was combined with ionic bond for reactive dye and polyamide fibre 56, and dyeing temperature is lower than common staining method.Low temperature dyeing can reduce the damage to fabric.Reactive dye and pure cotton fabric be also with Covalent bonding together, it is consistent with 56 fiber dyeing method of polyamide fibre.
Description
Technical field
The present invention relates to a kind of alkali bath method colouring methods of 56 fibers of polyamide fibre/cotton blended spinning face fabric.
Background technique
Nylon fabric is the first synthetic fibers occurred in the world, its various types, but is all contained in molecular structure
One identical amide groups, it is polycaprolactam that general common kind, which has polyamide fibre -6, and nylon-66 is that hexamethylene diamine and adipic acid are poly-
It closes, polyamide fibre 56 is a kind of novel Fypro, and different using petroleum from polyamide fibre 66, the raw material that it is used is raw
Raw material, by biological engineering method, fermentation prepares pentanediamine from each kind of starch and stalk cellulose, due to high-volume, it is low at
This, therefore can replace hexamethylene diamine.Biology base fiber has green, environmental-friendly, raw material renewable and biodegradable etc. excellent
Characteristic helps to solve the serious resource that is faced of current global economy social development and energy shortage and environmental pollution
The problems such as.
Various fibers, whether natural fiber or staple fibre and synthetic fibers all respectively possess some good points, and respectively have weak points.It
Right fiber such as cotton hygroscopicity is all relatively good, and comfortable and easy to wear, the general wearability of synthetic fibers is good, and strength is high, but hygroscopicity is poor, thoroughly
Gas is bad.Polyamide fibre 56 has many excellent characteristics, and intensity is higher than terylene close to polyamide fibre 66, and density is lower than terylene；Hygroscopicity
Height, antistatic property are good；Pliability is close to wool；Glass transition temperature is lower than polyamide fibre 66, and 56 crystallinity of polyamide fibre is relatively lower than polyamide fibre-
66,56 glass transition temperature of polyamide fibre is 46 DEG C, and polyamide fibre 66 is 52 DEG C and is far below terylene, it is ensured that lower temperature resistance under cold conditions；It is soft
It is soft, wearability is good etc..The generally upper dye temperature of polyamide fibre 66 is 40-98 DEG C, and the dyeing fabric temperature of 56 fiber of polyamide fibre can be reduced to 40-
80℃。
It is polyamide fibre 56 and pure cotton is blended, so that it may which that the characteristics of sufficiently using various fibers learns from other's strong points to offset one's weaknesses, enhance the clothes of fabric
Use performance.The disclosure of the relevant technologies is had no with 56 fiber of polyamide fibre and pure cotton blended yarn weaved fabric alkali bath method colouring method.
Summary of the invention
The object of the present invention is to provide a kind of alkali bath method colouring methods of 56 fibers of polyamide fibre/cotton blended spinning face fabric.
The alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric provided by the present invention, includes the following steps:
56 fibers of polyamide fibre/cotton blended spinning face fabric is dyed using reducing dye or reactive dye；
56 fibers of the polyamide fibre/cotton blended spinning face fabric is the blended yarn weaved fabric of polyamide fibre 56 and cotton fiber.
In above-mentioned colouring method, when being dyed using the reactive dye, specifically comprise the following steps:
1) dye liquor is prepared, the dye liquor is prepared to obtain by K-type reactive dye and sodium sulphate；
2) 56 fibers of the polyamide fibre/cotton blended spinning face fabric and the dye liquor are sequentially added to overflow dyeing machine；Heat the dye
Alkaline matter is added into the overflow dyeing machine and adjusts pH value to after 9~10, after of continuing rising after temperature rises to 50~60 DEG C for color machine
Temperature is to 80 DEG C, and heat preservation continues dyeing 30~60 minutes and realizes to the dyeing of 56 fibers of polyamide fibre/cotton blended spinning face fabric.
In the dye liquor, quality-volumetric concentration of the K-type reactive dye can be 20~80g/L, concretely 20g/L,
Quality-volumetric concentration of the sodium sulphate can be 30~50g/L, concretely 40g/L.
In above-mentioned colouring method, the alkaline matter can be sodium carbonate.
When being dyed using the reactive dye, due to the reactive dye and 56 fibers of polyamide fibre/cotton blended fabric
It is dyed in alkalinity bath, is Covalent bonding together between dyestuff and fiber, therefore every color fastness is equal in addition to chlorine-resistant floats index error
It is relatively good.
In above-mentioned colouring method, when being dyed using the reducing dye, specifically comprise the following steps:
56 fibers of the polyamide fibre/cotton blended spinning face fabric is padded in reducing dye suspended substance, is dried after taking-up；Then
Continue to be padded in reducing solution, then successively through decatize, washing, aoxidize and soap i.e. realize to 56 fibers of polyamide fibre/cotton blended spinning face fabric
Dyeing；
The reducing dye suspended substance refers to the dispersion liquid for being dispersed in water the reducing dye, the reduction
The concentration of reducing dye described in dye suspension can be 10~80g/L.
In above-mentioned colouring method, the reducing solution is the aqueous solution of caustic soda and sodium dithionite (sodium hydrosulfite), wherein
Quality-volumetric concentration of the caustic soda is 10~30g/l, concretely 20g/l, quality-volume of the sodium dithionite
Concentration is 20~40g/l, concretely 34g/l.
In above-mentioned colouring method, the temperature of the decatize can be 100 DEG C~110 DEG C, and the time can be 20~150s, specifically
Can under conditions of 102 DEG C decatize 40s；
The oxidant used that aoxidizes can be hydrogen peroxide, and the temperature of the oxidation can be 50 DEG C~60 DEG C, concretely
55℃；
The temperature soaped can be 90 DEG C~100 DEG C, and concretely 95 DEG C, soap and soda ash can be used in described soap
Aqueous solution is as detergent.
In the present invention, the blending ratio of polyamide fibre 56 described in 56 fibers of the polyamide fibre/cotton blended spinning face fabric can be 10~85%, such as
50% or 85%.
Fabric after reducing dye dyeing it is bright-colored, chromatography is more complete, and color fastness is excellent, especially soaps and day
It is excellent to shine fastness.
The alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric provided by the invention has the advantages that
Since nylon 56 and common polyamide have apparent difference, the crystal transfer of nylon 56 is irreversible；Polyamide fibre
56 be a kind of typical even-odd polyamide, and all possible intermolecular hydrogen bonding cannot be generated when strand, which has, is all-trans conformation and is made
With.The optical microscopy carried out in the case where waiting mild non-isothermal condition research shows that the spherocrystal of nylon 56 and having conventional laminated structure
Idol-idol polyamide fibre have different optical properties.
Due to caused by the difference of crystallization aspect, in terms of acid and alkali-resistance, the performance of nylon 56 and common nylon 6, nylon66 fiber
It compares, differs larger.Under identical treatment conditions, the fibre strength reduction of nylon 56 is more, causes to study more nylon 6
The dyeing of nylon 56 can not be fitted entirely into nylon66 fiber dyeing.And the dyeing of pure cotton fabric under alkaline condition is then
Conventional colouring method, so 56 fiber of polyamide fibre can be realized smoothly with pure cotton blended yarn weaved fabric alkali bath method colouring method.
In the alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric of the present invention, reactive dye and polyamide fibre 56 with
Covalent bonding together, fastness are better than what acid bath was combined with ionic bond, and dyeing temperature is lower than common staining method.Low temperature dyeing can
Reduce the damage to fabric.Reactive dye and pure cotton fabric be also with Covalent bonding together, it is consistent with 56 fiber dyeing method of polyamide fibre.
Specific embodiment
Experimental method used in following embodiments is conventional method unless otherwise specified.
The materials, reagents and the like used in the following examples is commercially available unless otherwise specified.
K-type reactive dye: reactive brilliant red 3B is purchased from Hensel Mann.
Reducing dye: the black FBL of wheat siron is purchased from Hensel Mann.
Embodiment 1, K-type reactive dyeing
56 fibers of polyamide fibre/cotton blended spinning face fabric dyeing is applicable in the reactive dye of high temperature modification K.
20D × 20D × 56 fibers of 350T polyamide fibre/cotton blended spinning face fabric (56 fiber blend ratio of polyamide fibre is 50%) is packed into overflow
In overflow dyeing machine, adjust coolant-temperature gage in overflow dyeing machine and recycled in 40 DEG C of bootings, when dyeing by reactive brilliant red 3B reactive dye (20g/L) and
The dye liquor that sodium sulphate (40g/L) is made into is added in overflow dyeing machine 1 DEG C/1 minute to 60 DEG C addition sodium carbonate (20g/l) of slowly heating up and adjusts
PH value is saved 80 DEG C and to keep the temperature to after 10, continuing to heat up by 1 DEG C/min and continue dyeing 60 minutes.It is post-processed after qualified to color.
Every color fastness index of fabric after the present embodiment dyes is as shown in table 1.
Every fastness reaches requirement after dyeing it can be seen from data in table 1.
The dyeing of embodiment 2, reducing dye
45 × 45/130 × 70 56 fibers of polyamide fibre/cotton blended spinning face fabric (56 fiber blend ratio of polyamide fibre is 85%), are contaminated with reduction
Material dye polyamide fibre 56 carries out dyeing on continuous pad-dyeing range
Second dipping and rolling reducing dye suspended substance liquid → 90 DEG C of infrared ray drying → room temperature, one immersing and rolling reducing solution (caustic soda with
The aqueous solution of sodium hydrosulfite (sodium dithionite), wherein quality-volumetric concentration of caustic soda is 20g/l, quality-volume of sodium hydrosulfite
Concentration is 34g/l) → 55 DEG C of oxidations of → 102 DEG C decatize 40 seconds → washing, 1g/l → 95 DEG C hydrogen peroxide (30wt%) soap, soap
5g/l, soda ash 3g/l → post-processing.
Every color fastness index of fabric after the present embodiment dyes is as shown in table 1.
Every fastness reaches requirement after dyeing it can be seen from data in table 1.
Table 1 dyes 56 fabric items color fastness index of polyamide fibre
| Name of an article project | Embodiment 1 | Embodiment 2 |
| Dry friction color fastness | 4.5 | 4.5 |
| Wet friction color fastness | 4.5 | 4.5 |
| Color fastness to water | 4.5 | 4.5 |
| Color fastness to chlorine | 4.5 | 4.5 |
| Color fastness to sea water | 5 | 5 |
| Alkaline-resisting PERSPIRATION COLOR FASTNESS | 5 | 5 |
| Colour fasteness to sunlight | 6.5 | 7.5 |
| Fastness to soaping | 4.5 | 5 |
The test method of each index is as follows in table 1:
1, fastness to soaping is tested by national standard GB/T3921.4-1997.
2, dry/wet friction color fastness is executed by GB/3920.
3, resistance to (alkali) PERSPIRATION COLOR FASTNESS is executed by ISO105-E04:2008.
4, chlorine-resistant drift color fastness is executed by ISO105E03:2010.
5, color fastness to sea water is executed by AATCC106-2002.
6, color fastness to water is by JIS (37 ± 2) DEG C × 4h.
7, colour fasteness to sunlight presses ISO105B02-1994.
Claims (4)
1. a kind of alkali bath method colouring method of 56 fibers of polyamide fibre/cotton blended spinning face fabric, includes the following steps:
56 fibers of polyamide fibre/cotton blended spinning face fabric is dyed using reducing dye or reactive dye；
56 fibers of the polyamide fibre/cotton blended spinning face fabric is the blended yarn weaved fabric of polyamide fibre 56 and cotton fiber；
When being dyed using the reactive dye, specifically comprise the following steps:
1) dye liquor is prepared, the dye liquor is prepared to obtain by K-type reactive dye and sodium sulphate；
2) 56 fibers of the polyamide fibre/cotton blended spinning face fabric and the dye liquor are sequentially added to overflow dyeing machine；The overflow dyeing machine is heated,
After temperature rises to 50~60 DEG C, alkaline matter is added into the overflow dyeing machine and adjusts pH value to after 9~10, is continuously heating to 80
DEG C, and heat preservation continues dyeing 30~60 minutes and realizes to the dyeing of 56 fibers of polyamide fibre/cotton blended spinning face fabric；
When being dyed using the reducing dye, specifically comprise the following steps:
56 fabric lining of polyamide fibre is padded in reducing dye suspended substance, is dried after taking-up；It then proceedes to be padded in
In reducing solution, then successively through decatize, washing, aoxidize and soap and realize dyeing to 56 fiber of polyamide fibre；
The reducing dye suspended substance refers to the dispersion liquid for being dispersed in water the reducing dye.
2. colouring method according to claim 1, it is characterised in that: in the dye liquor, the matter of the K-type reactive dye
Amount-volumetric concentration is 20~80g/L, and quality-volumetric concentration of the sodium sulphate is 30~50g/L；
The alkaline matter is sodium carbonate.
3. colouring method according to claim 1, it is characterised in that: the reducing solution is caustic soda and sodium dithionite
Aqueous solution, wherein quality-volumetric concentration of the caustic soda is 10~30g/l, quality-volumetric concentration of the sodium dithionite
For 20~40g/l.
4. colouring method according to claim 1 or 3, it is characterised in that: the temperature of the decatize is 100 DEG C~110 DEG C,
Time is 20~150s；
For the oxidant used that aoxidizes for hydrogen peroxide, the temperature of the oxidation is 50 DEG C~60 DEG C；
The temperature soaped is 90 DEG C~100 DEG C.
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Cited By (1)
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| CN111270533A (en) * | 2020-02-10 | 2020-06-12 | 军事科学院系统工程研究院军需工程技术研究所 | Alkaline pad dyeing method for chinlon 56 fiber and fabric |
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| CN109554939B (en) * | 2017-09-27 | 2021-03-16 | 上海凯赛生物技术股份有限公司 | Indigo dyeing method of polyamide 56 fiber or polyamide 56/cotton blended fabric and product thereof |
| CN108060588A (en) * | 2017-12-11 | 2018-05-22 | 佛山市顺德金纺集团有限公司 | A kind of brocade cotton woven active amide dyestuff one-bath dyeing method |
| CN110344266B (en) * | 2018-04-08 | 2021-05-14 | 上海凯赛生物技术股份有限公司 | One-step dyeing method for cotton/polyamide 56 fiber blended fabric by using reactive dye and acid or neutral dye in one bath |
| CN109183448B (en) * | 2018-09-30 | 2020-12-01 | 绍兴文理学院 | Dyeing process of nylon-cotton fabric |
| CN112011868A (en) * | 2019-05-28 | 2020-12-01 | 上海凯赛生物技术股份有限公司 | Polyamide fiber and cotton blended yarn and preparation method and application thereof |
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| CN111058316A (en) * | 2019-12-31 | 2020-04-24 | 军事科学院系统工程研究院军需工程技术研究所 | Alkaline pad dyeing method for chinlon 56 and cellulose fiber blended fabric |
| CN111058317A (en) * | 2019-12-31 | 2020-04-24 | 军事科学院系统工程研究院军需工程技术研究所 | Alkaline one-bath dip-dyeing method for chinlon 56 and cellulose fiber blended fabric |
| CN111809412A (en) * | 2020-01-09 | 2020-10-23 | 军事科学院系统工程研究院军需工程技术研究所 | Low-temperature one-bath one-step dyeing method for chinlon 56 and protein fiber blended fabric |
| CN111809411A (en) * | 2020-01-22 | 2020-10-23 | 军事科学院系统工程研究院军需工程技术研究所 | Alkaline dip dyeing method for chinlon 56 fiber and fabric |
| CN116005470A (en) * | 2023-01-10 | 2023-04-25 | 浙江三元纺织有限公司 | Chinlon reactive dyeing method |
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