CN105997753A - Method for producing liquid soap by utilizing waste vegetable leaves - Google Patents
Method for producing liquid soap by utilizing waste vegetable leaves Download PDFInfo
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- CN105997753A CN105997753A CN201610588828.2A CN201610588828A CN105997753A CN 105997753 A CN105997753 A CN 105997753A CN 201610588828 A CN201610588828 A CN 201610588828A CN 105997753 A CN105997753 A CN 105997753A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses liquid soap produced by utilizing waste vegetable leaves. The liquid soap is prepared from the following raw materials in parts by weight: 40-50 parts of juice of the vegetable leaves, 10-20 parts of frangipani extract, 10-12 parts of aloe vera gel, 2-4 parts of soapberry fruit extract, 2-4 parts of ginger root extract, 1-3 parts of peppermint essential oil, 6-8 parts of carboxymethylcellulose, 1-3 parts of citric acid, 1-3 parts of sodium citrate, 3-5 parts of a surface active agent and 80-100 parts of water. The liquid soap has high detergency, elegant appearance and an effect of being friendly to the skin; when in use, the liquid soap is fine, smooth and elegant in foam, and pleasant in fragrance; when the liquid soap is used for cleaning, the foam is very easily cleaned, so that water and time are saved; the liquid soap is easy to decompose in the natural world, and does not easily cause the eutrophication of water, thus being environment-friendly.
Description
Technical field
The present invention relates to washing field, a kind of method utilizing useless dish leaf to produce handwashing liquid.
Background technology
In a lot of vegetable places of production, the trade market of vegetable to produce substantial amounts of abandoned vegetable leaf every day, and these abandoned vegetable leaves are relatively low due to the value recycled, and people are little to its technical research recycled, and there is presently no the good treatment technology of formation.Generally people can be with a small amount of waste vegetable leaves pasture, but for large batch of discarded dish leaf, owing to wherein containing putrid and deteriorated dish leaf, it is impossible to directly use waste vegetable leaves pasture, be otherwise easily caused domestic animal sick；Substantial amounts of waste vegetable leaves stacks meeting everywhere because of unmanned recovery, not only wastes, but also causes environmental pollution；Up to the present, various places also neither one well disposes way, mostly falls to topple over toward hole, mountain field nature of leaving as organic waste and rots, and both contaminated airs, again polluted source have a strong impact on living environment and the health of people.In the city that environmental conservation is good, abandoned vegetable leaf is all transported to destructor plant and works as garbage disposal every day, causes the huge waste of resource, human and material resources.Owing to the value of waste vegetable leaves is relatively low, being difficult to cause the attention of people, therefore in the recycling of waste vegetable leaves, the application technology of appearance is little.
Along with raising and the change of living environment of people's living standard, making people more focus on the health of self and surrounding enviroment, thus bring the once leap of Personal hygiene custom, the especially diligent idea washed one's hands is rooted in the hearts of the people step by step.Handwashing liquid is because using health, the convenient succedaneum having become traditional clean hands articles for use, the huge market demand, the most pollution-free, the handwashing liquid of pure natural, safe and sanitary.
Handwashing liquid kind in the market is more, has plenty of the product that pure chemistry synthetic is formed by certain formula, have plenty of in chemical substance, add the product that some medicinal herb componentses or plant extract such as Aloe extraction solution etc. are formed, but on market, also there is no a kind of handwashing liquid utilizing useless dish leaf to make.
Summary of the invention
Based on the problem that presently, there are above-mentioned existence, it is an object of the invention to provide a kind of product consuming and obtaining after useless dish leaf processes, the method that the product utilizing useless dish leaf to obtain after processing produces handwashing liquid, this method is simple, easy to operate, not only process useless dish leaf, also utilize it to create bigger economic benefit.
The present invention realizes by the following technical solutions:
A kind of handwashing liquid utilizing useless dish leaf to produce, including the raw material of following portions by weight: useless vegetable leaf juice 40-50, Flos Plumeriae Acutifoliae extracting solution 10-20, Aloe glue 10-12, Fructus Sapindi Mukouossi fruit extracting solution 2-4, Rhizoma Zingiberis Recens extract 2-4, Peppermint essential oil 1-3, carboxymethyl cellulose 6-8, citric acid 1-3, sodium citrate 1-3, surfactant 3-5, water 80-100.
Described utilization is given up the handwashing liquid that dish leaf produces, including the raw material of following portions by weight: useless vegetable leaf juice 40, Flos Plumeriae Acutifoliae extracting solution 10, Aloe glue 10, Fructus Sapindi Mukouossi fruit 2, Rhizoma Zingiberis Recens extract 2, Peppermint essential oil 1, carboxymethyl cellulose 6, citric acid 1, sodium citrate 1, surfactant 3, water 80.
Described utilization is given up the handwashing liquid that dish leaf produces, including the raw material of following portions by weight: useless vegetable leaf juice 45, Flos Plumeriae Acutifoliae extracting solution 15, Aloe glue 11, Fructus Sapindi Mukouossi fruit 3, Rhizoma Zingiberis Recens extract 3, Peppermint essential oil 2, carboxymethyl cellulose 7, citric acid 2, sodium citrate 2, surfactant 4, water 90.
Described utilization is given up the handwashing liquid that dish leaf produces, including the raw material of following portions by weight: useless vegetable leaf juice 50, Flos Plumeriae Acutifoliae extracting solution 20, Aloe glue 12, Fructus Sapindi Mukouossi fruit 4, Rhizoma Zingiberis Recens extract 4, Peppermint essential oil 3, carboxymethyl cellulose 8, citric acid 3, sodium citrate 3, surfactant 5, water 100.
The preparation method of described useless vegetable leaf juice is: waste vegetable leaves sorts, and is manually sorted out from discarded dish leaf by corrupt dish leaf；nullChoose without going rotten、Unputrefied useless dish leaf，Clean，With disintegrating machine, useless dish leaf is crushed to 0.9～1.2 centimetre，Defibrination is carried out immediately after all crushing uniformly，The abundant defibrination of vegetable that will crush with colloid mill，The granule of defibrination is 0.5～0.6 millimeter，With juice extractor, the serosity of milled is squeezed the juice，Juice extractor stainless steel filtering net separation dish delivery juice and screenings，The dish juice squeezed out leads to steam heating immediately，Limit heating edge air compressor stirs，Blowing compressed air is stopped after boiling，Temperature retention time is 40 minutes，Temperature is at 96-100 DEG C，The feed liquid boiled is centrifuged separating by releasing horizontal centrifugal seperator，Isolate part dish juice float and carry out heat filtering，Dish juice temperature after separation starts when reaching 45-50 DEG C to filter，The juice filtered is through ultra high temperature short time sterilization device 110 ± 5 DEG C，Sterilizing time is 15 seconds，Flowing out temperature is 85 DEG C，Sterilized material is put and is cooled to 60-65 DEG C rapidly to temporary storage tank and concentrates，Vacuum concentration pan concentrates，The Lay juice concentrated carries out the re-pasteurization of 95 DEG C，Release after 3 minutes and concentrate dish juice，It is cooled to 30 DEG C with condensed water，The concentration dish juice that cooling packing is good preserves in-18～-25 DEG C of environment.
The preparation method of described Flos Plumeriae Acutifoliae extracting solution is: shred after Fructus Lycii cleans remove impurity, and water carries 3 times, wherein adds raw material weight 4～the water of 5 times for the first time, decocts 1～2h, and second time adds raw material weight 3～the water of 4 times, decocts 1.5h；Third time adds raw material weight 2～the water of 3 times, decocts 0.5～1h, and collecting decoction, through standing, after centrifugal treating, filtration, obtains filtrate；Described filtrate at 60～75 DEG C, obtains concentrated solution and is Flos Plumeriae Acutifoliae extracting solution after being evaporated to proportion and being 1.1～1.15.
The preparation method of described Fructus Sapindi Mukouossi fruit extracting solution is: being smashed by Fructus Sapindi Mukouossi fruit, add 12 times of water, boil 20 minutes, filter, filtering residue adds 6 times of water boils 10 minutes again, merges twice filtrate and i.e. obtains Fructus Sapindi Mukouossi fruit extracting solution.
The preparation method of described Rhizoma Zingiberis Recens extract is: Rhizoma Zingiberis Recens roguing is cleaned, then cuts into slices, dry, pulverize to 10-30 mesh, obtain Rhizoma Zingiberis Recens powder；By alcohol reflux 2-4 time of the Rhizoma Zingiberis Recens powder 70-80% of gained, each 1-3h, united extraction liquid；The extracting solution of gained is stood 1-2h, filters, be concentrated into the 10-20% of original volume, obtain crude extract；D: by the crude extract of gained respectively with the ethanol extraction of variable concentrations, with resin absorption, separate, concentrate, be dried, obtain finished product Rhizoma Zingiberis Recens extract.
Described surfactant is APG APG-1214 or quaternary surfactant.
Alkyl polyglucoside (APG) itself combines the functional character of traditional nonionic surfactant and anion surfactant, has excellent surface activity and a foaming capacity, strong detergency and without cloud point, without gelatin phenomenon.Compatibility is splendid, has good cooperative effect, does not has zest to skin, nontoxic, fully biodegradable, and environmentally safe is new generation of green surfactant.Alkyl polyglucoside (APG) have been used for washing, emulsifying, surely steep, foam, disperse, thickening, solubilising, the functional product such as moistening and moisturizing.There is purposes widely in washing Industry, cosmetic industry, pesticide, medicine, paper industry, fiber and the various fields such as textile industry, plastics industry, be the substitute products of the conventional surfactants such as LAS, AES.The present invention uses " APG APG-1214 " that Guangzhou Gao Yue Chemical Co., Ltd. produces.
Quaternary surfactant, four hydrogen atoms of ammonium cation [H4N+] a kind of cationic surface active agent entirely replaced by organic group.Researcher in 1935 finds that quaternary ammonium salt has a strongest bactericidal properties, and subsequently, quaternary ammonium salt causes the highest attention of people as the research of antibacterial.The quaternary surfactant that the present invention uses is provided by Hubei Xin Mingtai Chemical Co., Ltd..
Described utilization give up dish leaf produce handwashing liquid, its production method comprises the following steps:
Weigh useless vegetable leaf juice, Flos Plumeriae Acutifoliae extracting solution, Fructus Sapindi Mukouossi fruit extracting solution, Rhizoma Zingiberis Recens extract and water the most by weight and put in beaker, again carboxymethyl cellulose and Aloe glue are added in beaker, the magnetic stirring apparatus of 55-60 DEG C heats 35-40 minute, and make it dissolve with the rotating speed stirring of 300-800r/min, and regulate its viscosity；
2. the pH value of determination step 1. solution, and to regulate its pH with citric acid and sodium citrate be 6～7；
3. adding in beaker by Peppermint essential oil and surfactant, the rotating speed of regulation magnetic stirring apparatus is 1000/minr, and regulation temperature is 50 DEG C, stirs 2 hours so that it is be sufficiently mixed uniformly；
The most ultrasonic 30 minutes, still aging one day, obtain finished product handwashing liquid.
In the raw material that the present invention chooses, active ingredient is analyzed as follows:
Flos Plumeriae Acutifoliae (Classification system:Plumeria rubra L. cv. Acutifolia), another name remote Fructus Gardeniae, egg yolk flower, India jasmine, great Ji Hua, Apocynaceae, egg Pittosporum machaka or dungarunga.Sprig plumpness fleshiness.Ye great, ground paper matter, poly is born in Zhi Ding, and vein is linked to be arteries and veins at nearly leaf margin.Spending several consor in Zhi Ding, corolla tubular, footpath about 5～6cm, 5 split.Outside milky, center foresythia, extremely fragrance.Florescence 5～October.Flos Plumeriae Acutifoliae summer-flowering, delicate fragrance is graceful.After fallen leaves, the trunk bending nature of baldness, its shape is the most beautiful.It is suitable in garden, meadow planting, it is possible to potted plant, can be used as medicine.Originate in America, China's introducing and planting.Plumeria rubra (Plumeria is produced from Egypt
Rubra) and pink Flos Plumeriae Acutifoliae (P.Rubra var.alba) root gets antimicrobial component plumericin (plumericin) etc., there is the strongest antifungic action, Grain-positive and negative bacteria and tubercule bacillus are had obvious inhibition.Plumieride also has significant inhibitory action to Grain-negative and positive bacteria.
Fructus Sapindi Mukouossi (Classification system:Sapindus mukorossi Gaertn.), another name: wood is suffered from sub (Compendium of Materia Medica), oil suffers from bitter trouble tree (Hainan) of son (Sichuan), yellow mesh tree, mesh wave tree (Taiwan), You Luoshu, fruit of washing one's hands, name elsewhere: rub mesh, false Arillus Longan, Devil Frown etc. with the hands.Fructus Sapindi Mukouossi deciduous tree, branch carries out, leaf alternate；Without stipule；There is handle；Panicle, top is raw and side is raw；Flower polygamy, corolla light green, there is short pawl；Floral disc cup-shaped；It is raw that filigree has fine, soft fur, medicine back, and hermaphrodite flower stamen is little, and filigree has fur.Drupe is spherical, yellow or brown color time ripe.Seed is spherical, black, florescence 6～July.Really phase 9～October.Originate in various places and South East Asia Mainland various places, India and Japan on the south Yangtze River in China basin.Peel contains Saponin, can be for soap, and timber can do boxboard and wooden comb etc..Root, browse, seed: bitter, micro-pungent, cold.Slightly poisonous.Heat clearing away is eliminated the phlegm, eliminating stagnated food and killing intestinal worms.For diphtheria, laryngopharynx swelling and pain, tonsillitis, cough, pertussis, dyspepsia malnutrition due to parasitic infestation；Outer for trichomonas vaginitis.Kernel: pungent is flat.Removing food stagnancy wards off evil.For infantile malnutrition, ascariasis, flatulence in abdomen, halitosis.The scourability of Fructus Sapindi Mukouossi fruit, spumescence is best in all plants containing Saponin.
Rhizoma Zingiberis Recens be Zingiberaceae herbaceos perennial Rhizoma Zingiberis Recens (Zingiber officinale Roscoe) fresh rhizome, high 40～100cm.Kind has: number Rhizoma Zingiberis Recens Qingzhou Globba racemosa Smith of Qingzhou bamboo root Jiang Shan agriculture.Another name has race, hundred peppery clouds, hook dress to refer to, because of ground boy pungent, hot and cold, fresh ginger, processed with honey Rhizoma Zingiberis Recens.The rhizome (Rhizoma Zingiberis) of Rhizoma Zingiberis Recens, cork (Cortex Zingiberis), leaf (Folium Zingiberis) all can be used as medicine.Rhizoma Zingiberis Recens have in Chinese medicine and pharmacy dissipate, preventing or arresting vomiting, the effect such as cough-relieving.Ginger extract all has obvious inhibiting effect to staphylococcus aureus, Staphylococcus albus, Bacillus typhi, bacterium sonnei, bacillus pyocyaneus, and its effect is dependence with concentration.Especially the inhibitory action with staphylococcus aureus and Staphylococcus albus is the strongest. officinale root extract with
HBsAg the effect 1～P/N value of HBsAg can be made for 3 hours to be remarkably decreased, but its rate of descent is not further added by after more than 3 hours. gingerade preserved material has strong bactericidal action to Bacillus typhi and vibrio cholera in vitro. in vitro trichophyton there is is inhibitory action. zingiberol in race stem and gingerol have to be killed Mollusca and kills bilharzial effect, can be used for treating schistosomicide.
Carboxymethyl cellulose, English name:Carboxymethyl Cellulose, native cellulose is to be distributed polysaccharide the widest, that content is most in nature, originates the abundantest.The modification technology of current fibre element is concentrated mainly on etherificate and esterification two aspects.Carboxymethylation reaction is the one of etherification technology.Cellulose obtains carboxymethyl cellulose (CMC) after carboxy methylation; its aqueous solution has the effects such as thickening, film forming, gluing, water tariff collection, colloid protection, emulsifying and suspension; it is widely used in the industries such as oil, food, medicine, textile and paper, is one of most important cellulose ethers.
Aloe glue is a kind of product extracted from natural herbs " Aloe " with " freeze-stable method " technology, have no side effect, fester incised wound, scratch, suppurating sore, scald, skin pruritus, comedo, black speck, mosquito bite, toothache, labial angle, operative scar etc. has obvious assosting effect, there is good anti-inflammation and sterilization effect, safe and reliable.
Peppermint essential oil, mint flavored clearly cools off oneself, and the mind rouses oneself.Cure mainly: cleaning throat and moistening larynx, elimination halitosis have good effect, and have unique curative effect of body and mind of releiving.It it is one of quintessence oil introduction quintessence oil ten kinds with abecedarian's indispensability.Effect to skin: shrink blood capillary, gets rid of vivotoxin, improve eczema, tinea, releive itch, inflammation and burning, soft skin, eliminate blackhead, be of value to oiliness hair quality and skin quality.
Citric acid is a kind of important organic acid, has another name called citric acid, clear crystal, and often the water of crystallization Han a part, odorless, have the strongest tart flavour, soluble in water.Its calcium salt is more soluble than in hot water in cold water, and this character is commonly used to be identified and isolated from citric acid.Control suitable temperature during crystallization and can obtain anhydrous citric acid.At industry, grocery trade, cosmetic industry etc. has extremely many purposes.
Sodium citrate (English name:sodium citrate), to call sodium citrate, be a kind of organic compound, outward appearance is that white is to clear crystal.Odorless, has refrigerant salty pungent.Stablizing in room temperature and air, micro-in humid air have dissolubility, produces air slaking phenomenon in hot-air.It is heated to 150 DEG C and loses water of crystallization.Soluble in water, dissolve in glycerol, be insoluble in alcohols and other organic solvents, cross thermal decomposition, the most micro-have deliquescence, and micro-in hot-air have air slaking, and its solution ph is about 8.Sodium citrate is used as acidity regulator, flavoring agent, stabilizer in food, beverage industry；Anticoagulant, apophlegmatisant and diuretic it is used as in medical industry；In detergent industry, alternative sodium tripolyphosphate is as the auxiliary agent of non-toxic detergent；Be additionally operable to brewage, injection, photographic chemical and plating etc..
The invention have the benefit that
1, the present invention is that the product obtained after the process of useless dish leaf is produced handwashing liquid, can be disposed by dish leaf, turn waste into wealth, not only realize the utilization of waste material, also utilize it to create bigger economic benefit；
2, the handwashing liquid that the present invention produces has high detergency ability, graceful outward appearance and effect of parent's skin, and during use, foam exquisiteness is graceful, pleasant aroma, during cleaning, foam is the most clean, and water-saving saves time, and the handwashing liquid of the present invention easily decomposes at nature, do not easily cause body eutrophication, environmental protection；
3, the handwashing liquid of the present invention is not merely for wash hands, also has the function of skin moistening skin protection, after using this product to wash one's hands; feel is very salubrious, feels more moist, and it is lasting to wash rear lingering fragrance; can protect after with and effectively prevent antibacterial in growing on hand, the health of protection people；
4, the present invention uses chemical addition agent hardly, mainly containing plant component, has the effects such as gentle decontamination, disinfection, moistening skin-care, is suitable for various people, and human body skin health is had no stimulation by life-time service.
Detailed description of the invention
Embodiment 1
A kind of handwashing liquid utilizing useless dish leaf to produce, including the raw material of following portions by weight: useless vegetable leaf juice 40, Flos Plumeriae Acutifoliae extracting solution 10, Aloe glue 10, Fructus Sapindi Mukouossi fruit 2, Rhizoma Zingiberis Recens extract 2, Peppermint essential oil 1, carboxymethyl cellulose 6, citric acid 1, sodium citrate 1, surfactant 3, water 80.
The preparation method of described useless vegetable leaf juice is: waste vegetable leaves sorts, and is manually sorted out from discarded dish leaf by corrupt dish leaf；nullChoose without going rotten、Unputrefied useless dish leaf，Clean，With disintegrating machine, useless dish leaf is crushed to 0.9～1.2 centimetre，Defibrination is carried out immediately after all crushing uniformly，The abundant defibrination of vegetable that will crush with colloid mill，The granule of defibrination is 0.5～0.6 millimeter，With juice extractor, the serosity of milled is squeezed the juice，Juice extractor stainless steel filtering net separation dish delivery juice and screenings，The dish juice squeezed out leads to steam heating immediately，Limit heating edge air compressor stirs，Blowing compressed air is stopped after boiling，Temperature retention time is 40 minutes，Temperature is at 96-100 DEG C，The feed liquid boiled is centrifuged separating by releasing horizontal centrifugal seperator，Isolate part dish juice float and carry out heat filtering，Dish juice temperature after separation starts when reaching 45-50 DEG C to filter，The juice filtered is through ultra high temperature short time sterilization device 110 ± 5 DEG C，Sterilizing time is 15 seconds，Flowing out temperature is 85 DEG C，Sterilized material is put and is cooled to 60-65 DEG C rapidly to temporary storage tank and concentrates，Vacuum concentration pan concentrates，The Lay juice concentrated carries out the re-pasteurization of 95 DEG C，Release after 3 minutes and concentrate dish juice，It is cooled to 30 DEG C with condensed water，The concentration dish juice that cooling packing is good preserves in-18～-25 DEG C of environment.
The preparation method of described Flos Plumeriae Acutifoliae extracting solution is: shred after Fructus Lycii cleans remove impurity, and water carries 3 times, wherein adds raw material weight 4～the water of 5 times for the first time, decocts 1～2h, and second time adds raw material weight 3～the water of 4 times, decocts 1.5h；Third time adds raw material weight 2～the water of 3 times, decocts 0.5～1h, and collecting decoction, through standing, after centrifugal treating, filtration, obtains filtrate；Described filtrate at 60～75 DEG C, obtains concentrated solution and is Flos Plumeriae Acutifoliae extracting solution after being evaporated to proportion and being 1.1～1.15.
The preparation method of described Fructus Sapindi Mukouossi fruit extracting solution is: being smashed by Fructus Sapindi Mukouossi fruit, add 12 times of water, boil 20 minutes, filter, filtering residue adds 6 times of water boils 10 minutes again, merges twice filtrate and i.e. obtains Fructus Sapindi Mukouossi fruit extracting solution.
The preparation method of described Rhizoma Zingiberis Recens extract is: Rhizoma Zingiberis Recens roguing is cleaned, then cuts into slices, dry, pulverize to 10-30 mesh, obtain Rhizoma Zingiberis Recens powder；By alcohol reflux 2-4 time of the Rhizoma Zingiberis Recens powder 70-80% of gained, each 1-3h, united extraction liquid；The extracting solution of gained is stood 1-2h, filters, be concentrated into the 10-20% of original volume, obtain crude extract；D: by the crude extract of gained respectively with the ethanol extraction of variable concentrations, with resin absorption, separate, concentrate, be dried, obtain finished product Rhizoma Zingiberis Recens extract.
Described surfactant is APG APG-1214 or quaternary surfactant.
Described utilization give up dish leaf produce handwashing liquid, its production method comprises the following steps:
Weigh useless vegetable leaf juice, Flos Plumeriae Acutifoliae extracting solution, Fructus Sapindi Mukouossi fruit extracting solution, Rhizoma Zingiberis Recens extract and water the most by weight and put in beaker, again carboxymethyl cellulose and Aloe glue are added in beaker, the magnetic stirring apparatus of 55-60 DEG C heats 35-40 minute, and make it dissolve with the rotating speed stirring of 300-800r/min, and regulate its viscosity；
2. the pH value of determination step 1. solution, and to regulate its pH with citric acid and sodium citrate be 6～7；
3. adding in beaker by Peppermint essential oil and surfactant, the rotating speed of regulation magnetic stirring apparatus is 1000/minr, and regulation temperature is 50 DEG C, stirs 2 hours so that it is be sufficiently mixed uniformly；
The most ultrasonic 30 minutes, still aging one day, obtain finished product handwashing liquid.
Embodiment 2
A kind of handwashing liquid utilizing useless dish leaf to produce, including the raw material of following portions by weight: useless vegetable leaf juice 45, Flos Plumeriae Acutifoliae extracting solution 15, Aloe glue 11, Fructus Sapindi Mukouossi fruit 3, Rhizoma Zingiberis Recens extract 3, Peppermint essential oil 2, carboxymethyl cellulose 7, citric acid 2, sodium citrate 2, surfactant 4, water 90.
The preparation method of described useless vegetable leaf juice is: waste vegetable leaves sorts, and is manually sorted out from discarded dish leaf by corrupt dish leaf；nullChoose without going rotten、Unputrefied useless dish leaf，Clean，With disintegrating machine, useless dish leaf is crushed to 0.9～1.2 centimetre，Defibrination is carried out immediately after all crushing uniformly，The abundant defibrination of vegetable that will crush with colloid mill，The granule of defibrination is 0.5～0.6 millimeter，With juice extractor, the serosity of milled is squeezed the juice，Juice extractor stainless steel filtering net separation dish delivery juice and screenings，The dish juice squeezed out leads to steam heating immediately，Limit heating edge air compressor stirs，Blowing compressed air is stopped after boiling，Temperature retention time is 40 minutes，Temperature is at 96-100 DEG C，The feed liquid boiled is centrifuged separating by releasing horizontal centrifugal seperator，Isolate part dish juice float and carry out heat filtering，Dish juice temperature after separation starts when reaching 45-50 DEG C to filter，The juice filtered is through ultra high temperature short time sterilization device 110 ± 5 DEG C，Sterilizing time is 15 seconds，Flowing out temperature is 85 DEG C，Sterilized material is put and is cooled to 60-65 DEG C rapidly to temporary storage tank and concentrates，Vacuum concentration pan concentrates，The Lay juice concentrated carries out the re-pasteurization of 95 DEG C，Release after 3 minutes and concentrate dish juice，It is cooled to 30 DEG C with condensed water，The concentration dish juice that cooling packing is good preserves in-18～-25 DEG C of environment.
The preparation method of described Flos Plumeriae Acutifoliae extracting solution is: shred after Fructus Lycii cleans remove impurity, and water carries 3 times, wherein adds raw material weight 4～the water of 5 times for the first time, decocts 1～2h, and second time adds raw material weight 3～the water of 4 times, decocts 1.5h；Third time adds raw material weight 2～the water of 3 times, decocts 0.5～1h, and collecting decoction, through standing, after centrifugal treating, filtration, obtains filtrate；Described filtrate at 60～75 DEG C, obtains concentrated solution and is Flos Plumeriae Acutifoliae extracting solution after being evaporated to proportion and being 1.1～1.15.
The preparation method of described Fructus Sapindi Mukouossi fruit extracting solution is: being smashed by Fructus Sapindi Mukouossi fruit, add 12 times of water, boil 20 minutes, filter, filtering residue adds 6 times of water boils 10 minutes again, merges twice filtrate and i.e. obtains Fructus Sapindi Mukouossi fruit extracting solution.
The preparation method of described Rhizoma Zingiberis Recens extract is: Rhizoma Zingiberis Recens roguing is cleaned, then cuts into slices, dry, pulverize to 10-30 mesh, obtain Rhizoma Zingiberis Recens powder；By alcohol reflux 2-4 time of the Rhizoma Zingiberis Recens powder 70-80% of gained, each 1-3h, united extraction liquid；The extracting solution of gained is stood 1-2h, filters, be concentrated into the 10-20% of original volume, obtain crude extract；D: by the crude extract of gained respectively with the ethanol extraction of variable concentrations, with resin absorption, separate, concentrate, be dried, obtain finished product Rhizoma Zingiberis Recens extract.
Described surfactant is APG APG-1214 or quaternary surfactant.
Described utilization give up dish leaf produce handwashing liquid, its production method comprises the following steps:
Weigh useless vegetable leaf juice, Flos Plumeriae Acutifoliae extracting solution, Fructus Sapindi Mukouossi fruit extracting solution, Rhizoma Zingiberis Recens extract and water the most by weight and put in beaker, again carboxymethyl cellulose and Aloe glue are added in beaker, the magnetic stirring apparatus of 55-60 DEG C heats 35-40 minute, and make it dissolve with the rotating speed stirring of 300-800r/min, and regulate its viscosity；
2. the pH value of determination step 1. solution, and to regulate its pH with citric acid and sodium citrate be 6～7；
3. adding in beaker by Peppermint essential oil and surfactant, the rotating speed of regulation magnetic stirring apparatus is 1000/minr, and regulation temperature is 50 DEG C, stirs 2 hours so that it is be sufficiently mixed uniformly；
The most ultrasonic 30 minutes, still aging one day, obtain finished product handwashing liquid.
Embodiment 3
A kind of handwashing liquid utilizing useless dish leaf to produce, including the raw material of following portions by weight: useless vegetable leaf juice 50, Flos Plumeriae Acutifoliae extracting solution 20, Aloe glue 12, Fructus Sapindi Mukouossi fruit 4, Rhizoma Zingiberis Recens extract 4, Peppermint essential oil 3, carboxymethyl cellulose 8, citric acid 3, sodium citrate 3, surfactant 5, water 100.
The preparation method of described useless vegetable leaf juice is: waste vegetable leaves sorts, and is manually sorted out from discarded dish leaf by corrupt dish leaf；nullChoose without going rotten、Unputrefied useless dish leaf，Clean，With disintegrating machine, useless dish leaf is crushed to 0.9～1.2 centimetre，Defibrination is carried out immediately after all crushing uniformly，The abundant defibrination of vegetable that will crush with colloid mill，The granule of defibrination is 0.5～0.6 millimeter，With juice extractor, the serosity of milled is squeezed the juice，Juice extractor stainless steel filtering net separation dish delivery juice and screenings，The dish juice squeezed out leads to steam heating immediately，Limit heating edge air compressor stirs，Blowing compressed air is stopped after boiling，Temperature retention time is 40 minutes，Temperature is at 96-100 DEG C，The feed liquid boiled is centrifuged separating by releasing horizontal centrifugal seperator，Isolate part dish juice float and carry out heat filtering，Dish juice temperature after separation starts when reaching 45-50 DEG C to filter，The juice filtered is through ultra high temperature short time sterilization device 110 ± 5 DEG C，Sterilizing time is 15 seconds，Flowing out temperature is 85 DEG C，Sterilized material is put and is cooled to 60-65 DEG C rapidly to temporary storage tank and concentrates，Vacuum concentration pan concentrates，The Lay juice concentrated carries out the re-pasteurization of 95 DEG C，Release after 3 minutes and concentrate dish juice，It is cooled to 30 DEG C with condensed water，The concentration dish juice that cooling packing is good preserves in-18～-25 DEG C of environment.
The preparation method of described Flos Plumeriae Acutifoliae extracting solution is: shred after Fructus Lycii cleans remove impurity, and water carries 3 times, wherein adds raw material weight 4～the water of 5 times for the first time, decocts 1～2h, and second time adds raw material weight 3～the water of 4 times, decocts 1.5h；Third time adds raw material weight 2～the water of 3 times, decocts 0.5～1h, and collecting decoction, through standing, after centrifugal treating, filtration, obtains filtrate；Described filtrate at 60～75 DEG C, obtains concentrated solution and is Flos Plumeriae Acutifoliae extracting solution after being evaporated to proportion and being 1.1～1.15.
The preparation method of described Fructus Sapindi Mukouossi fruit extracting solution is: being smashed by Fructus Sapindi Mukouossi fruit, add 12 times of water, boil 20 minutes, filter, filtering residue adds 6 times of water boils 10 minutes again, merges twice filtrate and i.e. obtains Fructus Sapindi Mukouossi fruit extracting solution.
The preparation method of described Rhizoma Zingiberis Recens extract is: Rhizoma Zingiberis Recens roguing is cleaned, then cuts into slices, dry, pulverize to 10-30 mesh, obtain Rhizoma Zingiberis Recens powder；By alcohol reflux 2-4 time of the Rhizoma Zingiberis Recens powder 70-80% of gained, each 1-3h, united extraction liquid；The extracting solution of gained is stood 1-2h, filters, be concentrated into the 10-20% of original volume, obtain crude extract；D: by the crude extract of gained respectively with the ethanol extraction of variable concentrations, with resin absorption, separate, concentrate, be dried, obtain finished product Rhizoma Zingiberis Recens extract.
Described surfactant is APG APG-1214 or quaternary surfactant.
Described utilization give up dish leaf produce handwashing liquid, its production method comprises the following steps:
Weigh useless vegetable leaf juice, Flos Plumeriae Acutifoliae extracting solution, Fructus Sapindi Mukouossi fruit extracting solution, Rhizoma Zingiberis Recens extract and water the most by weight and put in beaker, again carboxymethyl cellulose and Aloe glue are added in beaker, the magnetic stirring apparatus of 55-60 DEG C heats 35-40 minute, and make it dissolve with the rotating speed stirring of 300-800r/min, and regulate its viscosity；
2. the pH value of determination step 1. solution, and to regulate its pH with citric acid and sodium citrate be 6～7；
3. adding in beaker by Peppermint essential oil and surfactant, the rotating speed of regulation magnetic stirring apparatus is 1000/minr, and regulation temperature is 50 DEG C, stirs 2 hours so that it is be sufficiently mixed uniformly；
The most ultrasonic 30 minutes, still aging one day, obtain finished product handwashing liquid.
According to industry standard QB/T2850-2007 antibacterial bacteriostatic type detergent, the handwashing liquid producing the embodiment of the present invention and the most common handwashing liquid carry out fungistatic effect contrast test, and test result is shown in Table 1:
Table 1
Note: in the ordinary course of things, the gross activity thing content of handwashing liquid is carried out by the regulation of ethanol extraction.When body lotion formula for a product contains the surface active agent composition insoluble in ethanol, or when in travelling trader's contract for future delivery book, regulation has gross activity thing content detection result not include water cosolvent (fingernail benzene or the material such as the sulfonate of dimethylbenzene and carbamide), then gross activity thing content is carried out by the regulation of chloroform extraction method.
Visible, with commercially available anti-bacterial hand lotion contrast, the handwashing liquid that the present invention is produced has certain advantage on antibacterial effect, the sterilizing rate of escherichia coli and staphylococcus aureus is reached 99.99% and 100%, and good stability, gross activity thing content meets national standard, and foaming characteristic is better than commercially available handwashing liquid.
Claims (10)
1. one kind utilizes the handwashing liquid that useless dish leaf produces, it is characterized in that, including the raw material of following portions by weight: useless vegetable leaf juice 40-50, Flos Plumeriae Acutifoliae extracting solution 10-20, Aloe glue 10-12, Fructus Sapindi Mukouossi fruit extracting solution 2-4, Rhizoma Zingiberis Recens extract 2-4, Peppermint essential oil 1-3, carboxymethyl cellulose 6-8, citric acid 1-3, sodium citrate 1-3, surfactant 3-5, water 80-100.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterized in that, including the raw material of following portions by weight: useless vegetable leaf juice 40, Flos Plumeriae Acutifoliae extracting solution 10, Aloe glue 10, Fructus Sapindi Mukouossi fruit 2, Rhizoma Zingiberis Recens extract 2, Peppermint essential oil 1, carboxymethyl cellulose 6, citric acid 1, sodium citrate 1, surfactant 3, water 80.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterized in that, including the raw material of following portions by weight: useless vegetable leaf juice 45, Flos Plumeriae Acutifoliae extracting solution 15, Aloe glue 11, Fructus Sapindi Mukouossi fruit 3, Rhizoma Zingiberis Recens extract 3, Peppermint essential oil 2, carboxymethyl cellulose 7, citric acid 2, sodium citrate 2, surfactant 4, water 90.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterized in that, including the raw material of following portions by weight: useless vegetable leaf juice 50, Flos Plumeriae Acutifoliae extracting solution 20, Aloe glue 12, Fructus Sapindi Mukouossi fruit 4, Rhizoma Zingiberis Recens extract 4, Peppermint essential oil 3, carboxymethyl cellulose 8, citric acid 3, sodium citrate 3, surfactant 5, water 100.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterised in that the preparation method of described useless vegetable leaf juice is: waste vegetable leaves sorts, manually corrupt dish leaf is sorted out from discarded dish leaf；nullChoose without going rotten、Unputrefied useless dish leaf，Clean，With disintegrating machine, useless dish leaf is crushed to 0.9～1.2 centimetre，Defibrination is carried out immediately after all crushing uniformly，The abundant defibrination of vegetable that will crush with colloid mill，The granule of defibrination is 0.5～0.6 millimeter，With juice extractor, the serosity of milled is squeezed the juice，Juice extractor stainless steel filtering net separation dish delivery juice and screenings，The dish juice squeezed out leads to steam heating immediately，Limit heating edge air compressor stirs，Blowing compressed air is stopped after boiling，Temperature retention time is 40 minutes，Temperature is at 96-100 DEG C，The feed liquid boiled is centrifuged separating by releasing horizontal centrifugal seperator，Isolate part dish juice float and carry out heat filtering，Dish juice temperature after separation starts when reaching 45-50 DEG C to filter，The juice filtered is through ultra high temperature short time sterilization device 110 ± 5 DEG C，Sterilizing time is 15 seconds，Flowing out temperature is 85 DEG C，Sterilized material is put and is cooled to 60-65 DEG C rapidly to temporary storage tank and concentrates，Vacuum concentration pan concentrates，The Lay juice concentrated carries out the re-pasteurization of 95 DEG C，Release after 3 minutes and concentrate dish juice，It is cooled to 30 DEG C with condensed water，The concentration dish juice that cooling packing is good preserves in-18～-25 DEG C of environment.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterized in that, the preparation method of described Flos Plumeriae Acutifoliae extracting solution is: shred after Fructus Lycii cleans remove impurity, water carries 3 times, wherein add raw material weight 4～the water of 5 times for the first time, decocting 1～2h, second time adds raw material weight 3～the water of 4 times, decocts 1.5h；Third time adds raw material weight 2～the water of 3 times, decocts 0.5～1h, and collecting decoction, through standing, after centrifugal treating, filtration, obtains filtrate；Described filtrate is 1.1～1.15 at 60～75 DEG C through being evaporated to proportion
After, obtain concentrated solution and be Flos Plumeriae Acutifoliae extracting solution.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterised in that the preparation method of described Fructus Sapindi Mukouossi fruit extracting solution is: smashed by Fructus Sapindi Mukouossi fruit, add 12 times of water, boil 20 minutes, filter, filtering residue adds 6 times of water boils 10 minutes again, merges twice filtrate and i.e. obtains Fructus Sapindi Mukouossi fruit extracting solution.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterised in that the preparation method of described Rhizoma Zingiberis Recens extract is: Rhizoma Zingiberis Recens roguing cleaned, then cut into slices, dry, pulverize to 10-30 mesh, obtain Rhizoma Zingiberis Recens powder；By alcohol reflux 2-4 time of the Rhizoma Zingiberis Recens powder 70-80% of gained, each 1-3h, united extraction liquid；The extracting solution of gained is stood 1-2h, filters, be concentrated into the 10-20% of original volume, obtain crude extract；D: by the crude extract of gained respectively with the ethanol extraction of variable concentrations, with resin absorption, separate, concentrate, be dried, obtain finished product Rhizoma Zingiberis Recens extract.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterised in that described surfactant is APG APG-1214 or quaternary surfactant.
Utilize the handwashing liquid that useless dish leaf produces the most according to claim 1, it is characterised in that its production method comprises the following steps:
Weigh useless vegetable leaf juice, Flos Plumeriae Acutifoliae extracting solution, Fructus Sapindi Mukouossi fruit extracting solution, Rhizoma Zingiberis Recens extract and water the most by weight and put in beaker, again carboxymethyl cellulose and Aloe glue are added in beaker, the magnetic stirring apparatus of 55-60 DEG C heats 35-40 minute, and make it dissolve with the rotating speed stirring of 300-800r/min, and regulate its viscosity；
2. the pH value of determination step 1. solution, and to regulate its pH with citric acid and sodium citrate be 6～7；
3. adding in beaker by Peppermint essential oil and surfactant, the rotating speed of regulation magnetic stirring apparatus is 1000/minr, and regulation temperature is 50 DEG C, stirs 2 hours so that it is be sufficiently mixed uniformly；
The most ultrasonic 30 minutes, still aging one day, obtain finished product handwashing liquid.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108434006A (en) * | 2017-02-16 | 2018-08-24 | 天津国际生物医药联合研究院 | A kind of leakage of liquid and preparation method thereof of prevention hand-foot-and-mouth disease |
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