CN105968940A - Preparation method of black ceramic ink - Google Patents
Preparation method of black ceramic ink Download PDFInfo
- Publication number
- CN105968940A CN105968940A CN201610331652.2A CN201610331652A CN105968940A CN 105968940 A CN105968940 A CN 105968940A CN 201610331652 A CN201610331652 A CN 201610331652A CN 105968940 A CN105968940 A CN 105968940A
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- weight ratio
- pigment
- ink
- preparation
- black ceramic
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a preparation method of black ceramic ink and aims at providing the preparation method of the black ceramic ink, which has a bright color and is simple to maintain. The method disclosed by the invention comprises the following steps: preparing a pigment raw material, mixing a solvent to prepare a pigment solution, carrying out water-bath constant-temperature vibration and mixing, mixing a binding agent, a dispersant and a surfactant, carrying out water-bath constant-temperature vibration and mixing, standing and cooling, precipitating and sieving. The black ceramic ink is mainly used for ceramic manufacturers.
Description
Technical field
The present invention relates to a kind of ceramic ink, particularly relate to the preparation method of a kind of black ceramic ink.
Background technology
Ceramic tile is that we carry out one of main construction material of house decoration, and China produces going through of ceramic
History is long, enjoys great prestige in the world, and in English, the English " China " of China is exactly to have porcelain.And ceramic tile
Being one of ceramic spin-off, traditional ceramic tile uses high temperature sintering, and its surface uses glaze coating, sintering
Rear natural birth raw glaze material color, but glaze color is single, if using special glaze or special technological process
Produce ceramic tile, the problem that color is single can be changed, but special glaze or its restrictive condition of technological process are more,
And production cost height is difficult to use on a large scale.Therefore along with industrial expansion, inkjet printing is used in the modern times
Mode realize the decorative pattern of ceramic tile surface.Its technological process is simple, and reproducibility makes it use on a large scale.
But traditional ceramic ink performance is weak, production technology is simple, and easily blocking shower nozzle makes later maintenance cost high,
The life-span of printer is affected.
Summary of the invention
The invention discloses the preparation method of a kind of black ceramic ink, in order to solve the deficiencies in the prior art.
For solving the problems referred to above, the technical solution of the present invention is:
The preparation method of a kind of black ceramic ink, its method is: a, use pigment crude are used hot stove
Sintering, uses atomizer mill grind as fine powder after cooling, then pigment fine powder is passed through the thin of 0.05-0.5 μm
Sieve to obtain pigment powder, in not entering back into atomizer mill by the raw material of screening, repeat fine grinding；
B, adding in solvent by pigment powder, prepare pigment solution, the weight ratio of pigment is 5-35%, solvent
Weight ratio is 65%-95%；
C, pigment solution adding constant temperature water bath vibration mixing in water-bath vibrating machine, temperature controlled water baths is 35 DEG C
-45℃；
D, bonding agent, dispersant, three kinds of adjuvants of surfactant are added to the mixed pigment solution that vibrates
Prepare ink solution, the pH value of ink solution is 5-8, wherein bonding agent weight ratio be 1%-5%, point
The weight ratio of powder is 2%-8%, and the weight ratio of surfactant is 0.5%-3%；
E, mixing of being vibrated by constant temperature water bath in mixed ink solution addition water-bath vibrating machine, water-bath controls temperature
Degree is 35 DEG C-45 DEG C so that it is be sufficiently mixed.
F, will be sufficiently mixed after ink solution stand cooling make it fully react and precipitate；
G, will fully react and precipitate after ink solution sieve, control sieve mesh number be 0.05-0.5 μm, from
And prepare finished product ink.
Further, described pigment crude is iron compound, and the weight ratio added in its step b is 15%.
Further, described solvent is ester or alcohol organic solvent, and the weight ratio added in its step b is 85%.
Further, described bonding agent is silicon dioxide or siliceous compound, the weight added in its step d
Amount ratio is 5%.
Further, described surfactant is aliphatic hydrocarbon, and the weight ratio added in its step d is 1.5%.
Further, described dispersant be fatty glyceride or fatty acid Pyrusussuriensis smooth, add in its step d
Weight ratio be 3%.
The invention has the beneficial effects as follows: the above-mentioned ceramic ink produced, it is possible to print at most of potteries
Apply on machine, and later maintenance is easy, is not susceptible to clogging so that the life-span of printer is able to
Extending, and then saved fund, color is beautiful, and printing effect is outstanding.
Detailed description of the invention
Below the detailed description of the invention of the present invention is described in further detail.
The method of the present invention is: a, use pigment crude are used hot stove to sinter, and use fine grinding after cooling
Machine is ground as fine powder, then by the dusting cover of 0.05-0.5 μm, pigment fine powder is screened to obtain pigment powder, does not leads to
The raw material crossing screening enters back into repetition fine grinding in atomizer mill；
B, adding in solvent by pigment powder, prepare pigment solution, the weight ratio of pigment is 5-35%, solvent
Weight ratio is 65%-95%；
C, pigment solution adding constant temperature water bath vibration mixing in water-bath vibrating machine, temperature controlled water baths is 35 DEG C
-45℃；
D, bonding agent, dispersant, three kinds of adjuvants of surfactant are added to the mixed pigment solution that vibrates
Prepare ink solution, the pH value of ink solution is 5-8, wherein bonding agent weight ratio be 1%-5%, point
The weight ratio of powder is 2%-8%, and the weight ratio of surfactant is 0.5%-3%；
E, mixing of being vibrated by constant temperature water bath in mixed ink solution addition water-bath vibrating machine, water-bath controls temperature
Degree is 35 DEG C-45 DEG C so that it is be sufficiently mixed.
F, will be sufficiently mixed after ink solution stand cooling make it fully react and precipitate；
G, will fully react and precipitate after ink solution sieve, control sieve mesh number be 0.05-0.5 μm, from
And prepare finished product ink.
Further, described pigment crude is iron compound, and the weight ratio added in its step b is 15%.
Further, described solvent is ester or alcohol organic solvent, and the weight ratio added in its step b is 85%.
Further, described bonding agent is silicon dioxide or siliceous compound, the weight added in its step d
Amount ratio is 5%.
Further, described surfactant is aliphatic hydrocarbon, and the weight ratio added in its step d is 1.5%.
Further, described dispersant be fatty glyceride or fatty acid Pyrusussuriensis smooth, add in its step d
Weight ratio be 3%.
In use, the ceramic ink produced by this method is used in the usual way, its later maintenance
Easily, it is not susceptible to clogging so that the life-span of printer is extended, and then saves fund, color
Color reduction is beautiful, and printing effect is outstanding.
Above-mentioned detailed description of the invention is the preferred embodiments of the present invention, can not limit the invention, its
His any change made without departing from technical scheme or the substitute mode of other equivalence, all wrap
Within being contained in protection scope of the present invention.
Claims (6)
1. a preparation method for black ceramic ink, its method is: a, use pigment crude are used
Hot stove sinters, and uses atomizer mill grind as fine powder after cooling, then pigment fine powder is passed through 0.05-0.5 μm
Dusting cover screen to obtain pigment powder, repeat fine grinding in not entering back into atomizer mill by the raw material of screening；
B, adding in solvent by pigment powder, prepare pigment solution, the weight ratio of pigment is 5-35%, solvent
Weight ratio is 65%-95%；
C, pigment solution adding constant temperature water bath vibration mixing in water-bath vibrating machine, temperature controlled water baths is 35 DEG C
-45℃；
D, bonding agent, dispersant, three kinds of adjuvants of surfactant are added to the mixed pigment solution that vibrates
Prepare ink solution, the pH value of ink solution is 5-8, wherein bonding agent weight ratio be 1%-5%, point
The weight ratio of powder is 2%-8%, and the weight ratio of surfactant is 0.5%-3%；
E, mixing of being vibrated by constant temperature water bath in mixed ink solution addition water-bath vibrating machine, water-bath controls temperature
Degree is 35 DEG C-45 DEG C so that it is be sufficiently mixed.
F, will be sufficiently mixed after ink solution stand cooling make it fully react and precipitate；
G, will fully react and precipitate after ink solution sieve, control sieve mesh number be 0.05-0.5 μm, from
And prepare finished product ink.
The preparation method of black ceramic ink the most according to claim 1, it is characterised in that: described
Pigment crude is iron compound, and the weight ratio added in its step b is 15%.
The preparation method of black ceramic ink the most according to claim 1, it is characterised in that: described
Solvent is ester or alcohol organic solvent, and the weight ratio added in its step b is 85%.
The preparation method of black ceramic ink the most according to claim 1, it is characterised in that: described
Bonding agent is silicon dioxide or siliceous compound, and the weight ratio added in its step d is 5%.
The preparation method of black ceramic ink the most according to claim 1, it is characterised in that: described
Surfactant is aliphatic hydrocarbon, and the weight ratio added in its step d is 1.5%.
The preparation method of black ceramic ink the most according to claim 1, it is characterised in that: described
Dispersant be fatty glyceride or fatty acid Pyrusussuriensis smooth, the weight ratio added in its step d is 3%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610331652.2A CN105968940A (en) | 2016-05-17 | 2016-05-17 | Preparation method of black ceramic ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610331652.2A CN105968940A (en) | 2016-05-17 | 2016-05-17 | Preparation method of black ceramic ink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105968940A true CN105968940A (en) | 2016-09-28 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610331652.2A Withdrawn CN105968940A (en) | 2016-05-17 | 2016-05-17 | Preparation method of black ceramic ink |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105968940A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020793A (en) * | 2007-03-14 | 2007-08-22 | 四川蓝雅精工科技发展有限公司 | Prepn process of titania-silica color glaze pigment-filler for ceramic |
| CN101717274A (en) * | 2009-12-19 | 2010-06-02 | 江门市道氏标准制釉股份有限公司 | Brown pigment for ceramic ink jet printing and preparation method thereof |
| CN103509409A (en) * | 2012-06-18 | 2014-01-15 | 苏州忠辉蜂窝陶瓷有限公司 | Preparation method of ceramic ink used in ink jet printer |
| CN103555066A (en) * | 2013-10-30 | 2014-02-05 | 澧县新鹏陶瓷有限公司 | Colored glaze mixed type ink for ceramic ink-jet printing and preparation method thereof |
| CN103642317A (en) * | 2013-12-20 | 2014-03-19 | 佛山市三水区康立泰无机合成材料有限公司 | Low temperature ceramic inkjet ink |
-
2016
- 2016-05-17 CN CN201610331652.2A patent/CN105968940A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020793A (en) * | 2007-03-14 | 2007-08-22 | 四川蓝雅精工科技发展有限公司 | Prepn process of titania-silica color glaze pigment-filler for ceramic |
| CN101717274A (en) * | 2009-12-19 | 2010-06-02 | 江门市道氏标准制釉股份有限公司 | Brown pigment for ceramic ink jet printing and preparation method thereof |
| CN103509409A (en) * | 2012-06-18 | 2014-01-15 | 苏州忠辉蜂窝陶瓷有限公司 | Preparation method of ceramic ink used in ink jet printer |
| CN103555066A (en) * | 2013-10-30 | 2014-02-05 | 澧县新鹏陶瓷有限公司 | Colored glaze mixed type ink for ceramic ink-jet printing and preparation method thereof |
| CN103642317A (en) * | 2013-12-20 | 2014-03-19 | 佛山市三水区康立泰无机合成材料有限公司 | Low temperature ceramic inkjet ink |
Non-Patent Citations (2)
| Title |
|---|
| 夏征农等: "《大辞海 第26卷 数理化力学卷》", 31 December 2015, 上海辞书出版社 * |
| 藏广州等: "《最新印刷技术实用手册 丝网印刷技术分册 上》", 30 November 2003, 合肥：安徽音像出版社 * |
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| PB01 | Publication | ||
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| WW01 | Invention patent application withdrawn after publication | ||
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Application publication date: 20160928 |