CN105935579A - Vertical reaction equipment - Google Patents
Vertical reaction equipment Download PDFInfo
- Publication number
- CN105935579A CN105935579A CN201610513646.9A CN201610513646A CN105935579A CN 105935579 A CN105935579 A CN 105935579A CN 201610513646 A CN201610513646 A CN 201610513646A CN 105935579 A CN105935579 A CN 105935579A
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- Prior art keywords
- parts
- vertical cylinder
- cast hopper
- charging
- vertical
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
Abstract
Vertical reaction equipment comprises a vertical cylinder, a stirring device, a feeding device, and a material buffering device. Two ends of the vertical cylinder are provided with an upper head and a lower head respectively. The stirring device comprises a supporting seat, a driving motor, a power output shaft, and a stirring paddle. The feeding device comprises a material leakage pipe, a material delivery pipe, a feed pump, a feed pipe, and a plurality of feeding assemblies. The material buffering device comprises a buffering bucket and a cover plate, wherein the buffering bucket has a hollow and truncated cone liked structure with two opened ends. By setting a vertical cylinder, a stirring device, and a feeding device, controlling the adding time, and adding materials into the plurality of feeding assemblies of the feeding device, continuous feeding operation can be achieved, moreover, the feeding operation is simple and convenient, and the feeding efficiency is high.
Description
Technical field
The present invention relates to chemical production equipment field, particularly relate to a kind of vertical response equipment.
Background technology
At present, in material production field, it usually needs use consersion unit, e.g., need to use as vertical
Consersion unit, vertical cylinder consersion unit or vertical vertical cylinder consersion unit are as material generation chemical reaction
Time the container that carried, it is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine and food
Etc. industry.
In some special occasions, typically the region that feeds intake of consersion unit is arranged on floor or platform, i.e.
The dog-house of consersion unit is normally at the top of consersion unit or near the position at top, when needs are to instead
When answering equipment to add liquid material, need to be transported to by material in advance on floor or platform, cause feeding operation
More complicated, feed inefficient.
Additionally, existing consersion unit is in order to ensure the mechanical strength of self, too much throwing typically will not be set
Material mouth, causes existing consersion unit with regard to this, it is more difficult to realize the operation of continuous way charging, the most relatively difficult to achieve same
One time is interior or interval time is shorter interior, adds the operation of various materials.
Summary of the invention
Based on this, it is necessary to provide that a kind of feeding operation is more simple and convenient, charging efficiency is higher and can
Realize the vertical response equipment of continuous way feeding operation.
A kind of vertical response equipment, including:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head；
Agitating device, described agitating device includes supporting seat, driving motor, power output shaft and stirring paddle,
Described support seat is fixedly mounted on described upper cover, and the first end of described power output shaft drives electricity with described
The rotary shaft of machine connects, and the second end of described power output shaft stretches to inside described vertical cylinder, described dynamic
Second end of power output shaft is connected with described stirring paddle, and described driving motor is used for driving described stirring paddle to rotate；
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body
And the multiple assembly that feeds intake, the first end of described material leakage body connects with described upper cover, described material leakage body
Second end connects with the first end of described conveying body, the second end of described conveying body and the described charging pump housing
Discharge end connection, the feed end of the described charging pump housing connects with described charging body, multiple described in feed intake group
Part is arranged at intervals on described charging body successively, and multiple described in feed intake assembly all with described charging body even
Logical, described in the assembly that feeds intake include feed intake body, cast hopper and the valve that feeds intake, described in feed intake the first end of body
Connect with described charging body, described in feed intake the second end of body connect with described cast hopper, described cast hopper
Offer dog-house, described in feed intake valve be arranged at described in feed intake on body；And
Material buffer device, described material buffer device includes that buffering bucket and cover plate, described buffering bucket have two
The structure of the shaped hollow round table of end opening, the bottom opening fixed cover of described buffering bucket is placed on described cast hopper
And the position of the body that feeds intake described in neighbouring, described cover plate has loop configuration, the outer ledge of described cover plate
Being connected with at the open-topped marginal position of described buffering bucket, the inside edge of described cover plate feeds intake with described
Bucket lateral wall connect, the sidewall of described cast hopper offers cushion hole, described cushion hole respectively with described throwing
Hopper and the connection of described buffering bucket.
Wherein in an embodiment, the sidewall of described cast hopper offers some described cushion holes, described slow
Punching radially distributes with the central axis of described cast hopper.
Wherein in an embodiment, equal between the most adjacent two described cushion holes.
Wherein in an embodiment, described cushion hole position is provided with drainage screen.
Wherein in an embodiment, described cast hopper has cirque structure cross section.
Wherein in an embodiment, the connection of the lateral wall of the inside edge of described cover plate and described buffering bucket
Position is provided with sealing strip.
Wherein in an embodiment, it is characterised in that described sealing strip has loop configuration.
Above-mentioned highly effective reaction device is by arranging vertical cylinder, agitating device and feeding device, and controls well
Addition opportunity, then put into materials to multiple assemblies that feed intake of feeding device and can realize continuous way feeding operation
Effect, and feeding operation is more simple and convenient and charging efficiency is higher.
Accompanying drawing explanation
Fig. 1 is the structural representation of the vertical response equipment of an embodiment of the present invention；
Fig. 2 is Fig. 1 enlarged drawing at A；
Fig. 3 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention；
Fig. 4 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention；
Fig. 5 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention；
Fig. 6 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention；
Fig. 7 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention；
Fig. 8 is the partial structurtes schematic diagram of the vertical response equipment of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully.
Accompanying drawing gives the better embodiment of the present invention.But, the present invention can come in many different forms
Realize, however it is not limited to embodiments described herein.On the contrary, provide the purpose of these embodiments to be
Make the disclosure is understood more thorough comprehensively.
It should be noted that when element is referred to as " being fixed on " another element, and it can be directly at another yuan
On part or element placed in the middle can also be there is.When an element is considered as " connection " another element, and it can
To be directly to another element or to may be simultaneously present centering elements.Term as used herein " is hung down
Straight ", " level ", "left", "right" and similar statement for illustrative purposes only, be not offered as
It it is unique embodiment.
Unless otherwise defined, all of technology used herein and scientific terminology and the technology belonging to the present invention
The implication that the technical staff in field is generally understood that is identical.The art used the most in the description of the invention
Language is intended merely to describe the purpose of specific embodiment, it is not intended that in limiting the present invention.Used herein
Term " and/or " include the arbitrary and all of combination of one or more relevant Listed Items.
Such as, a kind of vertical response equipment, including: vertical cylinder, the two ends of described vertical cylinder set respectively
It is equipped with upper cover and low head；Agitating device, described agitating device includes supporting seat, driving motor, power
Output shaft and stirring paddle, described support seat is fixedly mounted on described upper cover, the of described power output shaft
One end is connected with the rotary shaft of described driving motor, and the second end of described power output shaft stretches to described vertical
Inner barrel, the second end of described power output shaft is connected with described stirring paddle, and described driving motor is used for carrying
Dynamic described stirring paddle rotates；Feeding device, described feeding device includes material leakage body, conveying body, charging
The pump housing, charging body and multiple assembly that feeds intake, the first end of described material leakage body connects with described upper cover,
Second end of described material leakage body connects with the first end of described conveying body, the second end of described conveying body
Connecting with the discharge end of the described charging pump housing, the feed end of the described charging pump housing connects with described charging body,
The assembly that feeds intake described in multiple is arranged at intervals on described charging body successively, and multiple described in feed intake assembly all with
Described charging body connects, described in the assembly that feeds intake include feed intake body, cast hopper and the valve that feeds intake, described throwing
First end of material body connect with described charging body, described in feed intake the second end of body and described cast hopper company
Logical, described cast hopper offers dog-house, described in feed intake valve be arranged at described in feed intake on body；And material
Buffer unit, described material buffer device includes that buffering bucket and cover plate, described buffering bucket have both ends open
The structure of shaped hollow round table, the bottom opening fixed cover of described buffering bucket is placed on described cast hopper and neighbouring institute
Stating the position of the body that feeds intake, described cover plate has loop configuration, and the outer ledge of described cover plate is slow with described
Connect at the open-topped marginal position of punching bucket, the inside edge of described cover plate and the outside of described cast hopper
Wall connect, the sidewall of described cast hopper offers cushion hole, described cushion hole respectively with described cast hopper and institute
State buffering bucket connection.
In order to explain above-mentioned vertical response equipment further, such as, another embodiment is vertical
Formula consersion unit is as follows:
Referring to Fig. 1, highly effective reaction device 10 includes vertical cylinder 100, agitating device 200 and charging dress
Putting 300, agitating device 200 and feeding device 300 may be contained within vertical cylinder 100.
Referring to Fig. 1, the two ends of vertical cylinder 100 are respectively arranged with upper cover 110 and low head 120, vertical
Formula cylinder 100 is for the accommodating material added, and gives material mix and blend and the offer occasion that reacts.Example
As, upper cover 110 forms vertical cylinder 100 after being connected with low head 120.And for example, described vertical cylinder is
Integrated formed structure.And for example, described vertical cylinder be installed on outside support during, described upper envelope
The top of externally-located support, the bottom of the externally-located support of described low head.
Referring to Fig. 1, agitating device 200 includes supporting seat 210, driving motor 220, power output shaft 230
And stirring paddle 240, supporting seat 210 and be fixedly mounted on the upper cover 110 of vertical cylinder 100, power exports
First end of axle 230 is connected with the rotary shaft driving motor 220, and the second end of power output shaft 230 stretches into
Internal to vertical cylinder 100, e.g., the second end of power output shaft 230 stretches to vertical cylinder 100 times
End socket 120 is internal, and the second end of power output shaft 230 is connected with stirring paddle 240, e.g., and stirring paddle 240
The low head 120 being positioned at vertical cylinder 100 is internal, drives motor 220 to be used for driving power output shaft 230
Rotate, and then drive the stirring paddle 240 fixed with power output shaft 230 to rotate.When the vertical cylinder of needs
When material in 100 is stirred married operation, control to drive motor 220 to drive power output shaft 230 to rotate,
And then drive stirring paddle 240 to rotate, utilize the flow-disturbing effect of stirring paddle 240, preferably stirring can be played
Immixture, and then married operation can be stirred with the material in vertical cylinder 100.
See also Fig. 1 and Fig. 2, feeding device 300 include material leakage body 310, conveying body 320,
The charging pump housing 330, charging body 340 and multiple assembly 350 that feeds intake, upper cover 110, material leakage body 310,
Conveying body 320, the charging pump housing 330, charging body 340 and the assembly 350 that feeds intake are sequentially connected with, and for example,
Upper cover 110, material leakage body 310, conveying body 320, the charging pump housing 330, charging body 340 and throwing
Material assembly 350 is sequentially communicated.
Referring to Fig. 1, the first end of material leakage body 310 connects with upper cover 110, the of material leakage body 310
Two ends connect with the first end of conveying body 320, the second end of conveying body 320 and the charging pump housing 330
Discharge end connects, and the feed end of the charging pump housing 330 connects with charging body 340, multiple assemblies 350 that feed intake
It is arranged at intervals at successively on charging body 340, and multiple assembly 350 that feeds intake all connects with charging body 340,
When needs add material in vertical cylinder 100, only need to put into material to the assembly 350 that feeds intake can complete
Whole feeding operation, feeding operation is more simple and convenient and charging efficiency is higher, and without additionally arranging floor
Or these regions that feed intake such as platform, it is achieved that exempt from the effect of high-order charging, say, that when to the assembly that feeds intake
During 350 input material, draft based on the charging pump housing 330, the material adding the assembly 350 that feeds intake can enter to
In charging body 340, afterwards, material enters in conveying body 320, so by the charging pump housing 330 again
After, material is entered in material leakage body 310 by conveying body 320 again, and finally, material is again by material leakage body
In 310 upper covers 110 entering to vertical cylinder 100, and then enter in whole vertical cylinder 100, this
Time, complete whole feeding operation, i.e. only need to put into the assembly 350 that feeds intake or add material and can complete whole
Feeding operation, feeding operation is simple and convenient and charging efficiency is higher.Additionally, due to material leakage body 310, conveying
Body 320 and the existence of charging body 340, can be arranged far from vertical cylinder 100 by the assembly 350 that feeds intake
Region, such as, due to material leakage body 310, conveying body 320 and charging body 340 existence, permissible
The assembly 350 that feeds intake is arranged and is convenient on the ground of dosing operation or is arranged in weighing area, so, can
To realize exempting from the effect that a high position feeds intake and exempts from feeding platform.
Referring to Fig. 2, the assembly 350 that feeds intake includes feed intake body 351, cast hopper 352 and the valve 353 that feeds intake,
Feed intake body 351 the first end with charging body 340 connect, the second end of the body 351 that feeds intake and cast hopper
352 connections, cast hopper 352 offers dog-house 354, and the valve 353 that feeds intake is arranged at and feeds intake on body 351.
Such as, described feeding device arranges the assembly that feeds intake described in three, as such, it is possible to be simultaneously introduced three kinds of materials,
And then realize the effect of continuous way feeding operation, certainly, described in the feed intake number of assembly be not limited to three,
For example, it is also possible to be adjusted according to practical situation, e.g., feed intake described in each assembly one_to_one corresponding one seed ginseng
Add the material of reaction.
When in the needs same time or interval time shorter in, add various materials to vertical cylinder 100 is internal
Time, now, it being simultaneously introduced the kind of material as required, correspondence opens a number of valve 353 that feeds intake,
Then, to the dog-house 354 of multiple cast hoppers 352 corresponding input various materials, the charging pump housing 330 is opened,
Based on charging the pump housing 330 swabbing action, material along cast hopper 352-feed intake body 351-feed body 340-
The charging path of charging pump housing 330-conveying body 320-material leakage body 310-vertical cylinder 100 enters to vertical
In cylinder 100, now, whole feeding operation is completed.
When needs are to vertical cylinder 100 a kind of material of internal addition, now, open a cast hopper 352
Dog-house 354 and corresponding put into this material, and close remaining valve 353 that feeds intake, material is along cast hopper
352-feed intake body 351-charging body 340-charging pump housing 330-conveying body 320-material leakage body 310-vertical
The charging path of cylinder 100 enters in vertical cylinder 100, now, completes whole feeding operation.
Above-mentioned highly effective reaction device 10 by arranging vertical cylinder 100, agitating device 200 and feeding device 300,
And control addition opportunity well, then put into material to multiple assemblies 350 that feed intake of feeding device 300 can be real
The effect of existing continuous way feeding operation, and feeding operation is more simple and convenient and charging efficiency is higher.
In order to preferably close described cast hopper, with reduce the material in described cast hopper evaporate into the external world amount,
Such as, referring to Fig. 3, described highly effective reaction device also includes that locking device 400, locking device 400 include
Rotary shaft 410 and closing door 420, described rotary shaft rotates the limit of the described dog-house being arranged at cast hopper 352
Edge position, described closing door and described rotary shaft are fixing to be connected, described closing door be used for closing described in feed intake
Mouthful, the edge of described closing door is provided with sealing ring, and described sealing ring supports with the edge of described dog-house；
And for example, described dog-house has the cross section of circular configuration；And for example, described closing door has circular discoid knot
Structure；And for example, described sealing ring has circular annular form structure；And for example, described closing door is away from described rotary shaft
Position be provided with balancing weight；And for example, described sealing ring is provided with sealing towards the side opening of described dog-house
Groove, the edge of described dog-house is embedded at inside described seal groove；And for example, described seal groove has ring junction
Structure, so, utilizes the closing door 420 of locking device 400 can preferably close described cast hopper, to subtract
Material in few described cast hopper evaporates into the amount in the external world.
In order to preferably put into material in described cast hopper, such as, referring to Fig. 4, described highly effective reaction fills
Putting and also include material injection device 500, described material injection device 500 includes that sealing plate 510, first injects
Body 520 and second injects body 530, and described sealing plate covers on the described dog-house of cast hopper 352,
And being used for closing described dog-house, the described first the first end injecting body connects with described sealing plate, and
Described first inject body the first end connect with described cast hopper, described first injection body the second end and
Described second the first end injecting body is flexibly connected, and the described second the second end injecting body is used for and outside
The connection of material injection device, e.g., connect with outside charging bucket, described charging bucket is equipped with material；Again
As, the lateral wall of the described first the second end injecting body offers external screw thread, and described second injects body
The medial wall of the second end offers female thread, described female thread and described external thread bolt connection；And for example, described
The junction of one the second end and the described second the first end injecting body injecting body is provided with hoop component；
And for example, described hoop component includes clip body and connects screw rod, and described clip body is arranged at described first
Inject the second end of body and the junction of the described second the first end injecting body, the two of described connection screw rod
End two ends with described clip body respectively are spirally connected；And for example, described clip body has arcuate structure；And for example,
Being provided with reinforcement on described clip body, described reinforcement is extended to described by one end of described clip body
The other end of clip body；And for example, described reinforcement has a semicircular structure cross section, so, only need by
Outside material injection device connects with the described second the second end injecting body can complete dosing operation, from
And preferably can put into material in described cast hopper.
It is appreciated that when adding the material of excess to described cast hopper, it is possible to cause described cast hopper to send out
The problem of raw flash, in order to make described cast hopper preferably buffer material, with the problem reducing flash
Occurring, such as, refer to Fig. 5, described highly effective reaction device also includes material buffer device 600, described thing
Material buffer unit 600 includes buffering bucket 610 and cover plate 620, and described buffering bucket 610 has the sky of both ends open
The structure that the heart is round table-like, the bottom opening fixed cover of described buffering bucket 610 be placed on described cast hopper 352 and
Feed intake described in Lin Jin the position of body, and described cover plate has a loop configuration, the outer ledge of described cover plate with
Connect at the open-topped marginal position of described buffering bucket, the inside edge of described cover plate and described cast hopper
Lateral wall connect, the sidewall of described cast hopper offers cushion hole, and described cushion hole feeds intake with described respectively
Bucket and the connection of described buffering bucket, material can by described cushion hole described buffering bucket and described cast hopper it
Between flow, to play the effect of buffering；And for example, the sidewall of described cast hopper offers some described cushion holes,
Described cushion hole radially distributes with the central axis of described cast hopper；And for example, the most adjacent two described slow
Equal between punching；And for example, described cushion hole position is provided with drainage screen；And for example, described cast hopper
There is cirque structure cross section；And for example, the lateral wall of the inside edge of described cover plate and described buffering bucket
Sealing strip it is provided with at link position；And for example, described sealing strip has loop configuration, so, utilizes material
Buffer unit 600 can make described cast hopper preferably buffer material, sends out reducing the problem of flash
Raw.
In order to preferably carry the logistics flowed out in described material leakage body, and then minimizing material falls to described
The problem of the material sputtering produced in vertical cylinder, such as, refers to Fig. 6, and described highly effective reaction device also wraps
Including material bogey 700, described material bogey 700 includes loading plate 710 and connecting plate 720, institute
State loading plate to be connected with the medial wall of described upper cover, and described loading plate arranged towards described material leakage body,
Acute angle, described connecting plate is formed between bearing of trend and the central axis of described vertical cylinder of described loading plate
The first end be connected with the medial wall of described upper cover, the second end of described connecting plate is connected with described loading plate,
Described loading plate 710 is provided with flow-disturbing projection 711 towards the side of described material leakage body 310；And for example, described
It is protruding that loading plate is provided with some flow-disturbings；And for example, some described flow-disturbing projection rectangular array are distributed in described
In carrying；And for example, described flow-disturbing projection has hemispherical structure；And for example, described loading plate is near institute
The position stating low head is gradually obliquely installed；And for example, described connecting plate has the cross section of trapezium structure；
And for example, described loading plate is further opened with liquid leakage tank towards the side of described material leakage body, so, passes through material
The loading plate 710 of bogey 700 is to the carrying of material and buffering effect, it is possible to reduce material drops to institute
State the flow velocity within vertical cylinder, and the effect of dispersed material can also be played, so can preferably carry from
The logistics flowed out in described material leakage body, spatters reducing in material falls to described vertical cylinder the material produced
The problem penetrated.
In order to make the material flowed out in described material leakage body carry out preferably scatter operation, the most whole reaction
During, the mixed effect of each material, such as, refer to Fig. 7, described highly effective reaction device also includes material
Dispersal device 800, it is internal that described material dispersing device 800 is placed in described vertical cylinder 10, described material
Dispersal device 800 includes connector drum 810 and dispersion framework 820, and the first end of described connector drum is with described
First end connection of material leakage body, described dispersion framework has hollow structure, forms distribution cavity, institute in it
The second end stating connector drum is connected with described dispersion framework, and the second end of described connector drum is with described
Distribution cavity connects, and described dispersion framework 820 offers some described point away from one end of described connector drum
Dissipating the dispersion hole 821 of cavity connection, described dispersion hole is arranged towards described low head 120, and e.g., material is by respectively
Described dispersion hole 821 falls to inside described vertical cylinder；And for example, described dispersion framework has the circle of hollow
Tubular construction；And for example, some described dispersion hole are distributed with the central axis circular array of described dispersion framework；
And for example, described dispersion hole has the cross-sectional structure of regular polygon；And for example, described dispersion hole has positive six limits
The cross-sectional structure of shape structure；And for example, the first end of described connector drum and the first end of described material leakage body
It is spirally connected；And for example, described connector drum has rounded cylindrical structure, so, utilizes described material dispersing device
The material flowed out in described material leakage body can be made to carry out preferably scatter operation, the most whole course of reaction
In, the mixed effect of each material.
It is pointed out that each material being stirred married operation inside described vertical cylinder carries out chemical combination
During reaction, and most combination reaction is all exothermic reaction, and the productivity that the speed of reaction and product generate is also
Liberated heat when needing dependent reaction, is used for improving reaction rate and productivity.Additionally, in whipping process,
Material can be done work by described agitating device, and i.e. material is during being mutually mixed agitation, shows as outwardly
Releasing the material that heat, especially toughness are stronger, its exothermic phenomenon becomes apparent from, therefore, based on above-mentioned feelings
Condition, relies on the combination reaction of higher temperature for some, as depended on reaction self-heat generation and stirring heat production
Combination reaction, and need not extra heater for the reaction that it heats, it is especially desirable to guarantee institute
State the heat-insulating property of vertical cylinder.Further, in order to for some acid materials, therefore, to assure that described vertical
The medial wall of formula cylinder, the medial wall of the described vertical cylinder i.e. directly contacted with acid material possesses higher
Resistance to acid attack performance, for prolonging the raw service life of described vertical cylinder and being normally carried out of reaction.Further,
The lateral wall of described vertical cylinder is owing to often contacting with corrosive materials, e.g., and the form such as gaseous state or liquid
Corrosive materials contacts, it is therefore desirable to possess preferable decay resistance, described vertical for preferably protecting
Cylinder.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described vertical cylinder, such as, please
Refering to Fig. 8, described vertical cylinder, e.g., the sidewall of described vertical cylinder includes the resistance to acid attack being cascading
Layer 130, heat-insulation layer 140, supporting layer 150, weight coating 160 and protective layer 170, described resistance to acid attack layer position
In the medial wall of described vertical cylinder, and described resistance to acid attack layer is direct and material, e.g., and acid material contact,
Described protective layer is positioned at the lateral wall of described vertical cylinder, and the most described protective layer is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts～88
Part, titanium 30 parts～34 parts, chromium 20 parts～25 parts, antimony 2.5～3.4 parts, copper part 2.3～3.4 parts, 1.5 parts of zinc
～2.7 parts, aluminum 0.9～1.4 parts, 0.15 part～0.27 part of carbon, silicon 0.25 part～0.46 part, boron 0.12 part～0.18
Part, cobalt 0.04 part～0.09 part, 0.001 part～0.03 part of phosphorus, sulfur 0.001 part～0.03 part, 0.02 part of strontium～0.03
Part, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002 part.
Use ferrum 75 parts～88 parts, titanium 30 parts～34 parts and 20 parts～25 parts basic bases as resistance to acid attack layer of chromium
Plinth element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding
Antimony 2.5～3.4 parts, copper 2.3 parts～3.4 parts, 1.5 parts～2.7 parts of zinc, aluminum 0.9～1.4 parts, cobalt 0.04 part～0.09
Part, 0.02 part～0.03 part of strontium, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002
Part compounds, additionally it is possible to optimize the properties of described resistance to acid attack layer further, especially can be further
Optimize the resistance to acid attack performance of described resistance to acid attack layer such that it is able to better against the acid etching of material, be used for into one
Step improves the service life of described vertical cylinder and guarantees being normally carried out of reaction.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts～80
Part, titanium 33 parts～34 parts, chromium 24 parts～25 parts, antimony 2.7～3.4 parts, copper 2.7 parts～3.4 parts, 1.8 parts of zinc
～2.5 parts, aluminum 1.1～1.4 parts, 0.18 part～0.27 part of carbon, silicon 0.27 part～0.46 part, boron 0.13 part～0.18
Part, cobalt 0.04 part～0.09 part, 0.001 part～0.03 part of phosphorus, sulfur 0.001 part～0.03 part, 0.02 part of strontium～0.03
Part, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts,
Titanium 33 parts, chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon
0.46 part, boron 0.18 part, cobalt 0.04 part, 0.03 part of phosphorus, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04
Part, scandium 0.01 part and 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts～22
Part, white cotton 8～20 parts, rock wool 8 parts～15 parts, glass fibre 7 parts～9 parts, Lauxite 10 parts～20
Part, polyacrylamide 3.5 parts～4.5 parts, basalt fibre 1 part～3 parts, rubber foam 3～5 parts, hydrogen-oxygen
Change 1 part～2 parts of magnesium, aminopropyl triethoxysilane 1 part～2 parts, aluminium oxide 1 part～2 parts, the tertiary fourth of 3,5-bis-
Base-4-HBA methyl ester 1 part～2 parts, polypropylene fiber 3～4 parts, thiorubber. 1 part～2 parts and dodecane
Base sodium sulfate 0.2～0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when described
During material generation exothermic reaction within vertical cylinder, and after transferring heat to described resistance to acid attack layer, based on
Described heat-insulation layer has good heat insulation and heat-insulating property, can limit heat and be further transmitted through described vertical cylinder
Body, and then avoid heat to be transferred directly in external environment, it is ensured that the material within described vertical cylinder exists
Suitably react at temperature, for improving the productivity of reaction rate and product.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts
～21 parts, white cotton 17～20 parts, rock wool 10 parts～15 parts, glass fibre 7 parts～9 parts, Lauxite 10
Part～20 parts, polyacrylamide 3.5 parts～4.5 parts, basalt fibre 1 part～2.5 parts, rubber foam 3.5～5
Part, 1.5 parts～2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1.5 parts～2 parts, aluminium oxide 1 part～2 parts,
3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part～1.4 parts, polypropylene fiber 3.3～4 parts, thiorubber. 1 part
～2 parts and sodium lauryl sulphate 0.2～0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts,
White cotton 17～20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts,
Basalt fibre 2.1 parts, rubber foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2
Part, aluminium oxide 1.8 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1.4 parts, polypropylene fiber 4 parts, poly-
Sulphur rubber 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts～98 parts,
0.4 part～0.95 part of manganese, molybdenum 0.1 part～0.5 part, titanium 0.01 part～0.05 part, 0.02 part～0.1 part of aluminum, carbon
0.06 part～0.25 part, silicon 0.1 part～0.3 part, 0.05 part～0.1 part of phosphorus, boron 0.001 part～0.01 part, hafnium
0.05 part～0.5 part, scandium 0.05 part～0.3 part, chromium 0.05 part～0.3 part, 0.01 part～0.05 part of nickel, cerium 0.01
Part～0.05 part, thorium 0.01 part～0.05 part and zirconium 0.01 part～0.05 part.
It is appreciated that to make described vertical cylinder possess preferable heat-insulating property, needs to introduce described insulation
Layer, and the mechanical strength of described heat-insulation layer is poor, strong in order to strengthen the integrally-built machinery of described vertical cylinder
Degree, needs to introduce described supporting layer so that it is directly contact with described heat-insulation layer, is used for improving described vertical cylinder
The integrally-built mechanical strength of body, to reach the purpose of safety in production.Based on above-mentioned situation, this is necessary for wanting
Described supporting layer is asked to possess higher mechanical strength and anti-deformation nature, by using each group of as above mass parts
Part, the most described supporting layer contains hafnium 0.05 part～0.5 part, scandium 0.05 part～0.3 part, chromium 0.05 part～0.3
Part, 0.01 part～0.05 part of nickel, cerium 0.01 part～0.05 part, thorium 0.01 part～0.05 part and zirconium 0.01 part～0.05
Part, the mechanical strength of conventional iron alloy can be improved so that it is mechanical strength and anti-deformation nature are more excellent,
Disclosure satisfy that requirement.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts～98
Part, 0.55 part～0.95 part of manganese, molybdenum 0.35 part～0.5 part, titanium 0.01 part～0.05 part, 0.02 part of aluminum～0.1
Part, 0.17 part～0.25 part of carbon, silicon 0.1 part～0.25 part, 0.05 part～0.1 part of phosphorus, boron 0.008 part～0.01
Part, hafnium 0.1 part～0.5 part, scandium 0.1 part～0.3 part, chromium 0.1 part～0.3 part, 0.02 part～0.05 part of nickel,
Cerium 0.02 part～0.05 part, thorium 0.02 part～0.05 part and zirconium 0.02 part～0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, manganese
0.75 part, molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus,
Boron 0.008 part, hafnium 0.5 part, scandium 0.2 part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part
With 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts～95 parts of tungsten,
30 parts～60 parts of nickel, ferrum 15 parts～40 parts, chromium 1.5 parts～10 parts, 1.5 parts～10 parts of lead, copper 1 part～6
Part and molybdenum 0.5 part～5 parts.
It is appreciated that in producing course of reaction, needs the material in described vertical cylinder is carried out intensity relatively
High stirring operation, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid institute
The integrally-built quality stating vertical cylinder kicks the beam, and then reduces the external impacts impact on described vertical cylinder,
I.e. can reduce described vertical cylinder and concussion or displacement problem occur.The each component using as above mass parts is permissible
Described weight coating is made to possess excellent counterweight performance, it is possible to effectively to increase described vertical cylinder integrally-built
Weight so that it is identical or adaptive with the weight of traditional vertical cylinder, such that it is able to improve in production process
Security performance.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts of tungsten～95
Part, 30 parts～45 parts of nickel, ferrum 27 parts～40 parts, chromium 1.5 parts～2.3 parts, 1.5 parts～3.3 parts of lead, copper 1
Part～5.5 parts and molybdenum 0.5 part～4.9 parts.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, nickel
38 parts, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts～80 parts,
Lithium 16～18 parts, 18 parts～25 parts of nickel, molybdenum 3.5 parts～4 parts, chromium 2 parts～5 parts, cobalt 1 part～5 parts, vanadium 1
Part～5 parts, 1 part～2 parts of manganese, 0.8 part～2.5 parts of iridium, niobium 0.5 part～2.5 parts, scandium 0.3 part～2.5 parts,
0.2 part～2.5 parts of strontium, caesium 0.2 part～2.5 parts, 0.2 part～2.5 parts of tungsten and titanium 0.2 part～2.5 parts.
Be appreciated that the lateral wall of described vertical cylinder owing to often contacting with corrosive materials, e.g., gaseous state
Or the corrosive materials contact of the form such as liquid, it is therefore desirable to possess preferable decay resistance, for more preferably
Described vertical cylinder is protected on ground.By each component of as above mass parts, described protective layer can be made to possess well
Corrosion Protection, and then preferably protect described vertical cylinder, for extending the use of described vertical cylinder
Life-span.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts～70
Part, lithium 16 parts～16.5 parts, nickel 18～21 parts, molybdenum 3.5 parts～3.9 parts, chromium 2 parts～4.4 parts, cobalt 1 part
～3.9 parts, vanadium 1 part～4.5 parts, 1 part～1.7 parts of manganese, 0.8 part～2.3 parts of iridium, niobium 0.5 part～2.2 parts, scandium
0.3 part～2.3 parts, 0.2 part～2.3 parts of strontium, caesium 0.2 part～2.4 parts, 0.2 part～2.1 parts of tungsten and titanium 0.2 part～1.9
Part.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium
16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, iridium 2.3
Part, niobium 2.2 parts, scandium 2.3 parts, 2.3 parts of strontium, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described vertical cylinder further, e.g., the structure of the sidewall of described vertical cylinder, such as,
The thickness ratio of described resistance to acid attack layer, described heat-insulation layer, described supporting layer, described weight coating and described protective layer
For (1～1.5): (15～20): (5～5.5): (8～9.8): (0.5～1.2)；And for example, described weight coating and institute
State the thickness of protective layer than for 1:15:5:9.5:1.1.
It should be noted that other embodiments of the present invention also include the technical characteristic phase in the various embodiments described above
Combination can be formed mutually, and the highly effective reaction device that can implement.
It should be noted that other embodiments of the present invention also include the technical characteristic phase in the various embodiments described above
Combination can be formed mutually, and the vertical response equipment that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, the most right
The all possible combination of each technical characteristic in above-described embodiment is all described, but, if these skills
There is not contradiction in the combination of art feature, is all considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed
Carefully, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that, for this
For the those of ordinary skill in field, without departing from the inventive concept of the premise, it is also possible to make some changes
Shape and improvement, these broadly fall into protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be with
Claims are as the criterion.
Claims (7)
1. a vertical response equipment, it is characterised in that including:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head；
Agitating device, described agitating device includes supporting seat, driving motor, power output shaft and stirring paddle,
Described support seat is fixedly mounted on described upper cover, and the first end of described power output shaft drives electricity with described
The rotary shaft of machine connects, and the second end of described power output shaft stretches to inside described vertical cylinder, described dynamic
Second end of power output shaft is connected with described stirring paddle, and described driving motor is used for driving described stirring paddle to rotate；
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body
And the multiple assembly that feeds intake, the first end of described material leakage body connects with described upper cover, described material leakage body
Second end connects with the first end of described conveying body, the second end of described conveying body and the described charging pump housing
Discharge end connection, the feed end of the described charging pump housing connects with described charging body, multiple described in feed intake group
Part is arranged at intervals on described charging body successively, and multiple described in feed intake assembly all with described charging body even
Logical, described in the assembly that feeds intake include feed intake body, cast hopper and the valve that feeds intake, described in feed intake the first end of body
Connect with described charging body, described in feed intake the second end of body connect with described cast hopper, described cast hopper
Offer dog-house, described in feed intake valve be arranged at described in feed intake on body；And
Material buffer device, described material buffer device includes that buffering bucket and cover plate, described buffering bucket have two
The structure of the shaped hollow round table of end opening, the bottom opening fixed cover of described buffering bucket is placed on described cast hopper
And the position of the body that feeds intake described in neighbouring, described cover plate has loop configuration, the outer ledge of described cover plate
Being connected with at the open-topped marginal position of described buffering bucket, the inside edge of described cover plate feeds intake with described
Bucket lateral wall connect, the sidewall of described cast hopper offers cushion hole, described cushion hole respectively with described throwing
Hopper and the connection of described buffering bucket.
Vertical response equipment the most according to claim 1, it is characterised in that the sidewall of described cast hopper
Offering some described cushion holes, described cushion hole radially distributes with the central axis of described cast hopper.
Vertical response equipment the most according to claim 2, it is characterised in that the most adjacent two described slow
Equal between punching.
Vertical response equipment the most according to claim 3, it is characterised in that described cushion hole position
It is provided with drainage screen.
Vertical response equipment the most according to claim 1, it is characterised in that described cast hopper has circle
Loop configuration cross section.
Vertical response equipment the most according to claim 1, it is characterised in that the inner side edge of described cover plate
Edge is provided with sealing strip at the link position of the lateral wall of described buffering bucket.
Vertical response equipment the most according to claim 6, it is characterised in that described sealing strip has ring
Shape structure.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610513646.9A CN105935579B (en) | 2016-06-30 | 2016-06-30 | Vertical response equipment |
| CN201810619551.4A CN108479677B (en) | 2016-06-30 | 2016-06-30 | Vertical reaction equipment for preventing materials from being added into sputtering |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610513646.9A CN105935579B (en) | 2016-06-30 | 2016-06-30 | Vertical response equipment |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810619551.4A Division CN108479677B (en) | 2016-06-30 | 2016-06-30 | Vertical reaction equipment for preventing materials from being added into sputtering |
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| CN105935579A true CN105935579A (en) | 2016-09-14 |
| CN105935579B CN105935579B (en) | 2018-07-20 |
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| CN201610513646.9A Expired - Fee Related CN105935579B (en) | 2016-06-30 | 2016-06-30 | Vertical response equipment |
| CN201810619551.4A Active CN108479677B (en) | 2016-06-30 | 2016-06-30 | Vertical reaction equipment for preventing materials from being added into sputtering |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810619551.4A Active CN108479677B (en) | 2016-06-30 | 2016-06-30 | Vertical reaction equipment for preventing materials from being added into sputtering |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204768663U (en) * | 2015-05-29 | 2015-11-18 | 惠州市建科实业有限公司 | Agitated reactor |
| CN205948884U (en) * | 2016-06-30 | 2017-02-15 | 惠州市格雷戈里科技有限公司 | Vertical response device |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010179923A (en) * | 2009-02-03 | 2010-08-19 | Sumitomo Chemical Co Ltd | Storage container |
| CN201447180U (en) * | 2009-06-23 | 2010-05-05 | 罗明坚 | Mensurable conveying device of dye powder measuring hopper |
| CN203196640U (en) * | 2013-04-28 | 2013-09-18 | 寿光市新海化工有限公司 | Reaction kettle |
| CN104477536A (en) * | 2014-12-17 | 2015-04-01 | 江阴市盛园铜材有限公司 | Buffer hopper |
-
2016
- 2016-06-30 CN CN201610513646.9A patent/CN105935579B/en not_active Expired - Fee Related
- 2016-06-30 CN CN201810619551.4A patent/CN108479677B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204768663U (en) * | 2015-05-29 | 2015-11-18 | 惠州市建科实业有限公司 | Agitated reactor |
| CN205948884U (en) * | 2016-06-30 | 2017-02-15 | 惠州市格雷戈里科技有限公司 | Vertical response device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108479677A (en) | 2018-09-04 |
| CN105935579B (en) | 2018-07-20 |
| CN108479677B (en) | 2020-11-24 |
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