CN105906450B - A kind of functional living being composite fertilizer and preparation method thereof - Google Patents
A kind of functional living being composite fertilizer and preparation method thereof Download PDFInfo
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- CN105906450B CN105906450B CN201610519763.6A CN201610519763A CN105906450B CN 105906450 B CN105906450 B CN 105906450B CN 201610519763 A CN201610519763 A CN 201610519763A CN 105906450 B CN105906450 B CN 105906450B
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
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Abstract
The invention discloses a kind of functional living being composite fertilizer and preparation method thereof, described functional living being composite fertilizer includes following raw material：PQQ, Aphanamixis plant extracts, microbial bacterial agent, moderate-element nitrogen, phosphorus, potassium and microelements of calcium, magnesium, sulphur, zinc, boron, molybdenum.Aphanamixis plant leaf extract of the invention be by the fresh branches and leaves of Aphanamixis plant by immersion, sterilizing, cleaning, chopping, defibrination, squeeze the juice, concentrate, be vacuum dried, the step such as granulate and be prepared from.Various amino acid, plant good protein, various organic state micro elements, various active enzyme, SOD enzymes and various chelant things are rich in the extract, effective, many mechanism, complementary synergies can be carried out with PQQ, promote plant absorption.Additionally, the Soluble Fiber in plant extracts, can produce solidification with PQQ, further disperse active ingredient, so as to increase the long-acting of fertilizer.
Description
Technical field
The present invention relates to a kind of functional living being composite fertilizer and preparation method thereof, and in particular to a kind of containing PQQ
Biological compound fertilizer and preparation method thereof, belongs to agrochemical technical field.
Background technology
In modern agricultural production, chemical fertilizer plays more and more important effect, and the consumption figure of wherein composite fertilizer is very big, often
Year about tens million of tons.At present, domestic fertilizer enterprises are mainly with nitrogen, phosphorus, potassium as raw material, using physics or chemical synthesis
Method produces three element compound fertilizer or complex fertilizer.But, no matter using physics or chemical method production composite fertilizer, all suffering from
The low shortcoming of composite fertilizer's unitary function, utilization rate.Research shows that China is low because of utilization rate of fertilizer every year, the economic damage for causing
Lose nearly hundred billion yuan.This not only causes a large amount of wastes of resource, and to environment for the survival of mankind such as air, water body soil
Cause severe contamination.Therefore advocate today of energy-saving and emission-reduction energetically in country, in order to mitigate environmental pollution, improve the profit of fertilizer
With rate, develop a kind of new, efficient, environmental protection biological compound fertilizer and have very important significance, this is also industry research and development
With the Main way of tackling key problem.
The sixties in 20th century, it has been found that the special dehydrogenase of a class (D-Glucose dehydrogenase), this special dehydrogenation
The activity of enzyme is independent of nicotinamide nucleotide or flavin nucleotide, but used as a kind of new coenzyme, be present in alcohol dehydrogenase and
In mammalian placenta lysyloxidase.Then, the X-ray such as Salisbury determines its structure, is named as pyrroles's quinoline
Quinoline quinone.PQQ (Pyrroloquinoline quinone, PQQ), chemical constitution is 4,5- dihydro -4,5- titanium dioxides -
1- hydrogen pyrroles (2,3-f) quinone -2,7,9- tricarboxylic acids, in water solubility, molecular mass is 330, mainly as electron acceptor or donor
The oxidation-reduction process of enzymatic is participated in, unique adjacent benzoquinones structure and 3 carboxyls are its important functions in its chemical constitution
Group.PQQ has various physiologically actives to organism as the coenzyme of the 3rd class oxidoreducing enzyme.For example, it can promote plant
And growth of microbial cells, percentage of seedgermination is improved, body Free Radical Level is adjusted, plant is improved to arid, toxicity and radiation
Etc. extreme condition tolerance etc..In addition, functional components of the PQQ as fertilizer, can promote germination and plant growth, carry
Tolerance of the high crop to extreme condition.
Mountain chinaberry is a kind of arbor, is widely distributed in the torrid areas in Asia, such as India, Malaysia, Indonesia and
SOUTHERN CHINA.The southern areas of the provinces and regions such as Guangdong, Guangxi, Yunnan are mainly distributed in China, the shaw of Altitude Regions is born in
In.Its seed, bark, leaf, fruit etc. are widely used India and its surrounding countries are among the people as traditional herbal medicines.Mountain chinaberry
Bark has functions that astringing to arrest bleeding, the various discomforts of the disease, cancer and belly that are usually used in terms of spleen and liver；Its kind of oil
Can be made into the liniment for rheumatism.The pungent bitter of its seed, has and rushes down lower and vermifugal effect, and can be as gastric ulcer.But
It is that research currently for mountain chinaberry in terms of fertilizer is also rarely reported, therefore to Yushan Hill chinaberry extract and mountain chinaberry extract and PQQ
Act synergistically and the research of crops and ozone deplation is significant.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of functional living being composite fertilizer and preparation method thereof, the function
Property biological compound fertilizer using PQQ and Aphanamixis plant extracts as biological compound fertilizer Synergistic feature into
Point, solve the low shortcoming of existing composite fertilizer's unitary function, utilization rate.
To achieve these goals, the technical solution adopted in the present invention is：
A kind of functional living being composite fertilizer, including following raw material：PQQ, Aphanamixis plant extracts, microorganism
Microbial inoculum, moderate-element nitrogen, phosphorus, potassium and microelements of calcium, magnesium, sulphur, zinc, boron, molybdenum.
Nitrogen in the moderate-element derives from urea, ammonium hydrogen carbonate, ammonium sulfate, ammonium chloride, MAP, phosphorus unit
MAP, double superhosphate, calcium superphosphate, ammonium phosphate, calcium magnesium phosphate or ground phosphate rock are usually come from, potassium element derives from chlorination
Potassium, potassium sulfate or potassium nitrate.
Described functional living being composite fertilizer, including following weight portion raw material：PQQ 0.1-5.0 parts, mountain chinaberry
Genus plants extract 3-12 parts, microbial bacterial agent 2-6 parts, urea 20-30 parts of leaded wastewater 46%, MAP 55-85 parts, chlorine
Change 30-50 parts of potassium；
Also include calcium, the magnesium of 200-600ppm, the sulphur of 50-200ppm, the 500- of above-mentioned raw materials gross weight 300-700ppm
The zinc of 900ppm, the boron of 100-500ppm, the molybdenum of 50-300ppm.
Described Aphanamixis plant is Aphanamixis grandifolia BI, Huashan chinaberry, mountain chinaberry or TaiWan, China mountain chinaberry.
The preparation method of described Aphanamixis plant extracts, comprises the following steps：
(1) immersion sterilizing：The harvesting fresh branches and leaves of Aphanamixis plant, are immersed in salt solution and are sterilized, wherein, salt
Liquid quality fraction is 4-12%, and soak time is 1-4h, and soaking temperature is 10-25 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is concentrated, the volume ratio before and after concentration is 8-12:1, obtain
To the Aphanamixis plant extracts of concentration；
(7) dry：The Aphanamixis plant extracts of concentration is circulated granulation by rolling pelletizer, is obtained final product.
Preferably, the concentration is low temperature concentration, and thickening temperature is less than 50 DEG C.
The temperature of described low temperature defibrination is 0-5 DEG C.
Described microbial bacterial agent is one or more mixed in bacillus subtilis, nitrogen-fixing bacteria, phosphate solubilizing bacteria, photosynthetic bacteria
Compound, living bacteria count is hundred million/g of 20-30 in microbial bacterial agent.
A kind of preparation method of functional living being composite fertilizer, comprises the following steps：
(1) by Urea to molten condition, obtain urea melt, in urea melt add calcium, magnesium, sulphur, zinc, boron,
The corresponding raw material of molybdenum, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 40-50 DEG C, microbial bacterial agent, Aphanamixis plant extracts and pyrroles's quinoline are added
Quinoline quinone, carries out secondary granulation, while carry out normal temperature and air-drying and making particle water content control between 3.5-3.8%, obtains function
Property biological compound fertilizer.
The corresponding raw material of the calcium, magnesium, sulphur, zinc, boron, molybdenum is the material containing corresponding element.Preferably：Calcium was conducted oneself with dignity
Calcium phosphate, calcium superphosphate, calcium magnesium phosphate, magnesium come from calcium magnesium phosphate, and sulphur comes from potassium sulfate, ammonium sulfate, and zinc comes from zinc chloride, and boron comes
From borax, molybdenum comes from sodium molybdate.
Described calcium, magnesium, sulphur, zinc, boron, the grain graininess of the corresponding raw material of molybdenum are 150-300 mesh.
In actual production, PQQ can also be for PQQ salt sterling, PQQ solution, comprising pyrroles
The powder of the fermentation culture medium of quinoline quinone or the PQQ containing fermenting agent.
As needed, functional living being composite fertilizer of the invention can also add other nutrients, such as some plants also
Need the beneficial elements such as silicon, sodium, cobalt.
Beneficial effect
1st, seed is promoted to sprout.Functional components PQQ is with the addition of in functional living being composite fertilizer of the invention,
PQQ is plant growth factor, is capable of the positive energy regulation and control of involved in plant cell growth, promotes cell propagation, improves and plants
Lipase active in son, promotes seed respiratory rate, accelerates seed and sprouts process.
2nd, destruction of the prevention and elimination of disease and pests to seed, improves germination percentage.Be with the addition of in functional living being composite fertilizer of the invention
Aphanamixis plant leaf extract, the extract is rich in limonin active component, with stronger desinsection and insect antifeedant
Activity, can prevent insect pest from gnawing seed, so as to improve germination percentage.
3rd, fertilizer efficiency is improved.Aphanamixis plant leaf extract of the invention is by leaching by the fresh branches and leaves of Aphanamixis plant
Bubble, sterilizing, cleaning, chopping, defibrination, the step such as squeeze the juice, concentrate, being vacuum dried, granulating are prepared from.Rich in each in the extract
Amino acid, plant good protein, various organic state micro elements, various active enzyme, SOD enzymes and various chelant things are planted, can
Effective, many mechanism, complementary synergies are carried out with PQQ, promotes plant absorption.Simultaneously as plant extract
Thing is high enrichment powder, and what is be enriched with during various components therein are both from plant cell, therefore in extract various has
The Synergistic that organic microelement passes through PQQ, it is easier to be absorbed by plants and utilize.Additionally, in plant extracts
Soluble Fiber, can produce solidification with PQQ, further disperse active ingredient, so as to increase the long-acting of fertilizer
Effect.
Specific embodiment
Specific embodiment of the invention is described in further detail with reference to embodiments.
Embodiment 1
A kind of functional living being composite fertilizer, including following weight portion raw material：0.1 part of PQQ, mountain chinaberry extract 3
Part, 2 parts of microbial bacterial agent, 20 parts of the urea of leaded wastewater 46%, 55 parts of MAP, 30 parts of potassium chloride；
Also include calcium, the magnesium of 200ppm, the sulphur of 50ppm, the zinc of 500ppm, the 100ppm of above-mentioned raw materials gross weight 300ppm
Boron, the molybdenum of 50ppm.
The preparation method of described mountain chinaberry extract, comprises the following steps：
(1) immersion sterilizing：The harvesting fresh branches and leaves of mountain chinaberry, are immersed in salt solution and are sterilized, wherein, salt solution matter
Amount fraction is 4%, and soak time is 4h, and soaking temperature is 15 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；Described low temperature mill
The temperature of slurry is 0 DEG C；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is carried out into low temperature concentration, the temperature of low temperature concentration is 50 DEG C, dense
Volume ratio before and after contracting is 8:1, the mountain chinaberry extract for being concentrated；
(7) dry：The mountain chinaberry extract of concentration is circulated granulation by rolling pelletizer, is obtained final product.
Described microbial bacterial agent is bacillus subtilis, and living bacteria count is 2,000,000,000/g in microbial bacterial agent.
The preparation method of the functional living being composite fertilizer of the present embodiment, comprises the following steps：
(1) by Urea to molten condition, obtain urea melt, in urea melt add calcium, magnesium, sulphur, zinc, boron,
The corresponding raw material of molybdenum, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
Described calcium, magnesium, sulphur, zinc, boron, the corresponding raw material of molybdenum are respectively：Calcium comes from calcium superphosphate, calcium magnesium phosphate, and magnesium comes
From calcium magnesium phosphate, sulphur comes from ammonium sulfate, and zinc comes from zinc chloride, and boron comes from borax, and molybdenum comes from sodium molybdate；
Described calcium, magnesium, sulphur, zinc, boron, the grain graininess of the corresponding raw material of molybdenum are 150 mesh；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 45 DEG C, microbial bacterial agent, mountain chinaberry extract and PQQ are added, is carried out
Secondary granulation, while carry out normal temperature and air-drying and making particle water content control 3.5%, obtains functional living being composite fertilizer.
Embodiment 2
A kind of functional living being composite fertilizer, including following weight portion raw material：0.5 part of PQQ, Aphanamixis grandifolia BI are carried
Take 4 parts of thing, 3 parts of microbial bacterial agent, 21 parts of the urea of leaded wastewater 46%, 58 parts of MAP, 32 parts of potassium chloride；
Also include calcium, the magnesium of 300ppm, the sulphur of 60ppm, the zinc of 560ppm, the 160ppm of above-mentioned raw materials gross weight 400ppm
Boron, the molybdenum of 60ppm.
The preparation method of described Aphanamixis grandifolia BI extract, comprises the following steps：
(1) immersion sterilizing：The harvesting fresh branches and leaves of Aphanamixis grandifolia BI, are immersed in salt solution and are sterilized, wherein, salt is molten
Liquid mass fraction is 5%, and soak time is 1h, and soaking temperature is 10 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；Described low temperature mill
The temperature of slurry is 5 DEG C；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is carried out into low temperature concentration, the temperature of low temperature concentration is 40 DEG C, dense
Volume ratio before and after contracting is 9:1, the Aphanamixis grandifolia BI extract for being concentrated；
(7) dry：The Aphanamixis grandifolia BI extract of concentration is circulated granulation by rolling pelletizer, is obtained final product.
Described microbial bacterial agent is the mixture of bacillus subtilis and hydrogenlike silicon ion, withered grass bud in microbial bacterial agent
Spore bacillus living bacteria count is 1,000,000,000/g, and hydrogenlike silicon ion living bacteria count is 1,000,000,000/g.
The preparation method of the functional living being composite fertilizer of the present embodiment, comprises the following steps：
(1) by Urea to molten condition, obtain urea melt, in urea melt add calcium, magnesium, sulphur, zinc, boron,
The corresponding raw material of molybdenum, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
Described calcium, magnesium, sulphur, zinc, boron, the corresponding raw material of molybdenum are respectively：Calcium comes from calcium magnesium phosphate, and magnesium comes from calcium and magnesium phosphorus
Fertilizer, sulphur comes from potassium sulfate, and zinc comes from zinc chloride, and boron comes from borax, and molybdenum comes from sodium molybdate；
Described calcium, magnesium, sulphur, zinc, boron, the grain graininess of the corresponding raw material of molybdenum are 200 mesh；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 40 DEG C, microbial bacterial agent, Aphanamixis grandifolia BI extract and PQQ are added,
Secondary granulation is carried out, while carry out normal temperature and air-drying and making particle water content control 3.6%, functional living being composite fertilizer is obtained.
Embodiment 3
A kind of functional living being composite fertilizer, including following weight portion raw material：1.0 parts of PQQ, Huashan chinaberry are extracted
6 parts of thing, 4 parts of microbial bacterial agent, 22 parts of the urea of leaded wastewater 46%, 60 parts of MAP, 36 parts of potassium chloride；
Also include calcium, the magnesium of 280ppm, the sulphur of 80ppm, the zinc of 580ppm, the 180ppm of above-mentioned raw materials gross weight 460ppm
Boron, the molybdenum of 80ppm.
The preparation method of described Huashan chinaberry extract, comprises the following steps：
(1) immersion sterilizing：The harvesting fresh branches and leaves of Huashan chinaberry, are immersed in salt solution and are sterilized, wherein, salt solution
Mass fraction is 10%, and soak time is 2h, and soaking temperature is 25 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；Described low temperature mill
The temperature of slurry is 5 DEG C；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is carried out into low temperature concentration, the temperature of low temperature concentration is 45 DEG C, dense
Volume ratio before and after contracting is 10:1, the Huashan chinaberry extract for being concentrated；
(7) dry：The Huashan chinaberry extract of concentration is circulated granulation by rolling pelletizer, is obtained final product.
Described microbial bacterial agent is the mixture of bacillus subtilis and azotobacter chroococcum, withered grass bud in microbial bacterial agent
Spore bacillus living bacteria count is 1,000,000,000/g, and azotobacter chroococcum living bacteria count is 1,000,000,000/g.
The preparation method of the functional living being composite fertilizer of the present embodiment, comprises the following steps：
(1) by Urea to molten condition, obtain urea melt, in urea melt add calcium, magnesium, sulphur, zinc, boron,
The corresponding raw material of molybdenum, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
Described calcium, magnesium, sulphur, zinc, boron, the corresponding raw material of molybdenum are respectively：Calcium comes from calcium superphosphate, calcium magnesium phosphate, and magnesium comes
From calcium magnesium phosphate, sulphur comes from ammonium sulfate, and zinc comes from zinc chloride, and boron comes from borax, and molybdenum comes from sodium molybdate；
Described calcium, magnesium, sulphur, zinc, boron, the grain graininess of the corresponding raw material of molybdenum are 300 mesh；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 50 DEG C, microbial bacterial agent, Huashan chinaberry extract and PQQ are added, is entered
Row secondary granulation, while carry out normal temperature and air-drying and making particle water content control 3.7%, obtains functional living being composite fertilizer.
Embodiment 4
A kind of functional living being composite fertilizer, including following weight portion raw material：1.6 parts of PQQ, TaiWan, China mountain
8 parts of chinaberry extract, 3.6 parts of microbial bacterial agent, 28 parts of the urea of leaded wastewater 46%, 66 parts of MAP, 48 parts of potassium chloride；
Also including the calcium of above-mentioned raw materials gross weight 660ppm, the magnesium of 480ppm, the sulphur of 180ppm, the zinc of 680ppm,
The boron of 260ppm, the molybdenum of 180ppm.
The preparation method of described TaiWan, China mountain chinaberry extract, comprises the following steps：
(1) immersion sterilizing：The harvesting TaiWan, China mountain fresh branches and leaves of chinaberry, are immersed in salt solution and are sterilized, wherein, food
Salting liquid mass fraction is 12%, and soak time is 1h, and soaking temperature is 20 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；Described low temperature mill
The temperature of slurry is 3 DEG C；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is carried out into low temperature concentration, the temperature of low temperature concentration is 45 DEG C, dense
Volume ratio before and after contracting is 12:1, the TaiWan, China mountain chinaberry extract for being concentrated；
(7) dry：The TaiWan, China mountain chinaberry extract of concentration is circulated granulation by rolling pelletizer, is obtained final product.
Described microbial bacterial agent is the mixture of bacillus subtilis, azotobacter chroococcum and hydrogenlike silicon ion, microorganism
Bacillus subtilis living bacteria count is 1,000,000,000/g in microbial inoculum, and azotobacter chroococcum living bacteria count is 1,000,000,000/g, and class ball is red
Bacterium living bacteria count is 1,000,000,000/g.
The preparation method of the functional living being composite fertilizer of the present embodiment, comprises the following steps：
(1) by Urea to molten condition, obtain urea melt, in urea melt add calcium, magnesium, sulphur, zinc, boron,
The corresponding raw material of molybdenum, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
Described calcium, magnesium, sulphur, zinc, boron, the corresponding raw material of molybdenum are respectively：Calcium comes from calcium superphosphate, calcium magnesium phosphate, and magnesium comes
From calcium magnesium phosphate, sulphur comes from ammonium sulfate, and zinc comes from zinc chloride, and boron comes from borax, and molybdenum comes from sodium molybdate；
The calcium stated, magnesium, sulphur, zinc, boron, the grain graininess of the corresponding raw material of molybdenum are 200 mesh；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 50 DEG C, microbial bacterial agent, TaiWan, China mountain chinaberry extract and pyrroles's quinoline are added
Quinone, carries out secondary granulation, while carry out normal temperature and air-drying and making particle water content control 3.8%, obtains functional living being and is combined
Fertilizer.
Embodiment 5
Functional living being composite fertilizer of embodiment 5 and preparation method thereof and embodiment 4 are essentially identical, and difference is,
The functional living being composite fertilizer of the present embodiment, including following weight portion raw material：5.0 parts of PQQ, TaiWan, China mountain chinaberry
12 parts of extract, 6 parts of microbial bacterial agent, 30 parts of the urea of leaded wastewater 46%, 85 parts of MAP, 50 parts of potassium chloride；
Also including the calcium of above-mentioned raw materials gross weight 700ppm, the magnesium of 600ppm, the sulphur of 200ppm, the zinc of 900ppm,
The boron of 500ppm, the molybdenum of 300ppm.
Control group 1
Biological compound fertilizer of reference examples 1 and preparation method thereof and embodiment 2 are essentially identical, and difference is, this control
The biological compound fertilizer that Aphanamixis plant extracts, i.e. this reference examples are not contained in the biological compound fertilizer of example includes following weight portion
Raw material：0.5 part of PQQ, 3 parts of microbial bacterial agent, 21 parts of the urea of leaded wastewater 46%, 58 parts of MAP, potassium chloride 32
Part；
Also include calcium, the magnesium of 300ppm, the sulphur of 60ppm, the zinc of 560ppm, the 160ppm of above-mentioned raw materials gross weight 400ppm
Boron, the molybdenum of 60ppm.
Control group 2
Biological compound fertilizer of reference examples 2 and preparation method thereof and embodiment 2 are essentially identical, and difference is, this control
The biological compound fertilizer of PQQ, i.e. this reference examples is not contained in the biological compound fertilizer of example includes the raw material of following weight portion：
4 parts of Aphanamixis grandifolia BI extract, 3 parts of microbial bacterial agent, 21 parts of the urea of leaded wastewater 46%, 58 parts of MAP, 32 parts of potassium chloride；
Also include calcium, the magnesium of 300ppm, the sulphur of 60ppm, the zinc of 560ppm, the 160ppm of above-mentioned raw materials gross weight 400ppm
Boron, the molybdenum of 60ppm.
Influence of the functional living being composite fertilizer of the present invention of application examples 1 to Rice Production performance
Tested in Henan Academy of Agricultural Sciences experimental plot, trial crops are paddy rice, experiment is divided into 8 groups：1st group is arrived
The 5th group of functional living being composite fertilizer for applying embodiment of the present invention 1-5 respectively, the 6th group of biological compound fertilizer for applying control group 1,
The 7th group of biological compound fertilizer for applying control group 2, applies commercially available composite fertilizer for the 8th group and (contains urea 36kg, MAP per 180kg
78kg and potassium sulfate 66kg).
Method for culturing seedlings of the invention is with reference to paddy rice substrate seedling operational procedure, and specific nursery operating procedure is as follows：
1. do seedbed seedling cultivation of rice greenhouse and do high bed, bed surface is smooth, and the preferably autumn makees bed, while dug around greenhouse arranging
Water, drop stain ditch, temperature start button canopy and heat when ging up.Paper pot seedling-growing, after bed surface leveling, covers worn-out agricultural film or mulch film (root resistance
Film), leaking hole is beaten on film.
2. matrix selection selects the rice nursery substrate without addition nutrients with treatment.When using, by above-mentioned composite fertilizer
It is added in matrix (30kg/ mus), copying to mix makes that its is fluffy, do not lump, and the nature of matrix is kept after sabot, is not suppressed, often
Mu substrates quantity is in 100~150kg.
3. Seed Treatment (1) seed disinfection and impurity elimination.Stone, clod and flat kind in removal seed.(2) vernalization.Vernalization
Emergence rate can be improved, shorten seedling age, but note showing money or valuables one carries unintentionally in vernalization, bud can not be oversize.
4. sow
(1) sabot.Matrix after will be fluffy loads seed plate, strikes off, and keeps 2~2.5 cm thicks, is not required to suppression.(2) broadcast
Kind.Often disk uniformly broadcasts 120~150 grams of bud kind, typically keeps every square centimeter and is no less than 3 seeds, can not broadcast leakage and repeat broadcast
Kind, preferably with mechanical planting.(3) water.Vola water is poured, is made matrix saturation but water is not flowed out seedling and tries to get to the heart of a matter hole for principle.Note
With watering can it is a small amount of, gently pour, irrigate, can not flood wash away, in order to avoid wash away the nutrient in seed, leaching loss matrix.(4) base is covered
Matter.After pouring vola water, then seed is covered with matrix lid, struck off and removed unnecessary matrix, kept 0.5 centimetre of thickness.(5) balance.
Note that the short side of seed plate is outside during pendulum seed plate, ajust, put neat, pendulum tightly.(6) overlay film.One layer of mulch film, nothing are covered on seed plate surface
Cloth or 4~5 cm thick straw are spun, is burnt with insulation, moisturizing, anti-bud kind.
5. take off film, broken headkerchief (to occur " headkerchief ") when a large amount of germinations, coating matrix are by large stretch of jack-up, take off in time
The coverings such as film are fallen on the ground, coating matrix is dried, and is gently swept with whisk broom etc., matrix is scattering into rice shoot root, and suitably water
Wash away blade face matrix.
6. lifting fortune seedling matrix rice shoot well developed root system, transplants when rice shoot is up to 2.5~3.5 leaf age.Transplanting can pour 1 in first 1 day
Secondary water, " band medicine, band fertilizer " is transplanted, and the same day waters and is unfavorable for seedling taking, fortune seedling.Rice shoot can root system outwards roll after overlap entrucking fortune
Defeated, loading height is tried one's best no more than 6 layers.
Remaining field planting management method is consistent, counts the yield of paddy rice, is shown in Table 1.
Influence of the functional living being composite fertilizer of the present invention of table 1 to Rice Production performance
From table 1 it follows that using the paddy rice of functional living being composite fertilizer of the present invention, its mass of 1000 kernel, per total grain panicle number,
Setting percentage, the percentage of earbearing tiller, spike length and spike weight all significantly larger than apply the paddy rice of commercially available Common compound fertilizer, compared to applying reference examples
For the paddy rice of 1 and 2 composite fertilizers, also greatly improve.
Influence of the functional living being composite fertilizer of the present invention of application examples 2 to Wheat Production performance
Tested in Henan Academy of Agricultural Sciences experimental plot, trial crops are wheat, experiment is divided into 8 groups：1st group is arrived
The 5th group of functional living being composite fertilizer for applying embodiment of the present invention 1-5 respectively, the 6th group of biological compound fertilizer for applying control group 1,
The 7th group of biological compound fertilizer for applying control group 2, applies commercially available composite fertilizer for the 8th group and (contains urea 36kg, MAP per 180kg
78kg and potassium sulfate 66kg).
1. experimental field overview and field management
Experiment is carried out in the court's wheat experiment garden.Experiment physical features is flat, and middle fertility, soil types is loam, soil property
It is middle earth, to beat seed cucurbit, carried out the autumn after preceding stubble results turns over and soil moisture conservation of pouring water preceding stubble.Test and sowed on March 26th, 2015,
April 16~17 emerged.Fertilizing method is completed in strict accordance with testing program.Other same conventional cultivations of management.
2. field investigation project and method
0~30cm soil samples 6 are uniformly taken in trial zone before the investigation sowing of 2.1 soil samples, average each two cell takes a sample,
For determining the basic physicochemical character of soil (organic matter, pH, soil alkali-hydrolyzable nitrogen, rapid available phosphorus, quick-acting potassium content).
2.2 Basic Seedlings, mu spike number look into each cell of number experiment and have carried out multiple spot 1m in the neat rear and Heading filling mid-term of seedling respectively
The Basic Seedling of sample section, the investigation of mu spike number, and basic seedling amount, mu spike number in 1m samples section are converted to mu Basic Seedling and the effective fringe of mu
Number.
2.3 harvest before soil sampling harvest before takes 3 points of 0~30cm soil layers soil sample per cell, be mixed into 1 sample, altogether 12
Individual soil sample, for determining the nutrient contents such as soil alkali-hydrolyzable nitrogen, rapid available phosphorus, available potassium.
Leaving and taking for 2.4 species test samples takes 30 plants of samples and carries out species test before harvesting by every cell, and project includes：Yield and sample
Biological yield etc..
Influence of the functional living being composite fertilizer of the present invention of table 2 to Wheat Production performance
From Table 2, it can be seen that using the wheat of functional living being composite fertilizer of the present invention, its yield, sample biological yield
The wheat of commercially available Common compound fertilizer is all significantly larger than applied, compared to for the wheat for applying the composite fertilizer of reference examples 1 and 2, is also had
Greatly improve.
Claims (6)
1. a kind of functional living being composite fertilizer, it is characterised in that the raw material including following weight portion：PQQ 0.1-5.0
Part, 3-12 parts of Aphanamixis plant extracts, microbial bacterial agent 2-6 parts, urea 20-30 parts of leaded wastewater 46%, MAP 55-
85 parts, potassium chloride 30-50 parts；
Also include calcium, the magnesium of 200-600ppm, the sulphur of 50-200ppm, the 500- of above-mentioned raw materials gross weight 300-700ppm
The zinc of 900ppm, the boron of 100-500ppm, the molybdenum of 50-300ppm；
Described microbial bacterial agent is the mixing of one or more in bacillus subtilis, nitrogen-fixing bacteria, phosphate solubilizing bacteria, photosynthetic bacteria
Thing, living bacteria count is hundred million/g of 20-30 in microbial bacterial agent；
The preparation method of described functional living being composite fertilizer, comprises the following steps：
(1) by Urea to molten condition, urea melt is obtained, to addition calcium, magnesium, sulphur, zinc, boron, molybdenum pair in urea melt
The raw material answered, MAP and potassium chloride, are well mixed, the urea mixed slurry for being melted；
(2) the urea mixed slurry of melting is carried out into granulation of dusting, obtains particle germule；
(3) when particle germule is cooled to 40-50 DEG C, microbial bacterial agent, Aphanamixis plant extracts and PQQ are added,
Secondary granulation is carried out, while carry out normal temperature and air-drying and making particle water content control between 3.5-3.8%, functional living being is obtained
Composite fertilizer.
2. functional living being composite fertilizer according to claim 1, it is characterised in that described Aphanamixis plant is great Ye mountains
Chinaberry, Huashan chinaberry, mountain chinaberry or Taiwan mountain chinaberry.
3. functional living being composite fertilizer according to claim 1, it is characterised in that described Aphanamixis plant extracts
Preparation method, comprises the following steps：
(1) immersion sterilizing：The harvesting fresh branches and leaves of Aphanamixis plant, are immersed in salt solution and are sterilized, wherein, salt solution
Mass fraction is 4-12%, and soak time is 1-4h, and soaking temperature is 10-25 DEG C；
(2) clean：The branches and leaves after sterilizing will be soaked, cleaned with running water, dried；
(3) shred：Branches and leaves feeding shredding machine chopping after drying；
(4) defibrination：The branches and leaves of chopping are carried out into low temperature defibrination by fiberizer, branches and leaves slurry is obtained；
(5) squeeze the juice：Branches and leaves slurry feeding juice extractor is squeezed the juice, the fresh juice of plant is obtained；
(6) concentrate：The fresh juice feeding cold boiler of plant is concentrated, the volume ratio before and after concentration is 8-12:1, obtain dense
The Aphanamixis plant extracts of contracting；
(7) dry：The Aphanamixis plant extracts of concentration is circulated granulation by rolling pelletizer, is obtained final product.
4. functional living being composite fertilizer according to claim 3, it is characterised in that the temperature of described low temperature defibrination is 0-
5℃。
5. functional living being composite fertilizer according to claim 1, it is characterised in that described calcium, magnesium, sulphur, zinc, boron, molybdenum
Corresponding raw material is respectively：Calcium comes from double superhosphate, calcium superphosphate, calcium magnesium phosphate, and magnesium comes from calcium magnesium phosphate, and sulphur comes from sulfuric acid
Potassium, ammonium sulfate, zinc come from zinc chloride, and boron comes from borax, and molybdenum comes from sodium molybdate.
6. functional living being composite fertilizer according to claim 5, it is characterised in that described calcium, magnesium, sulphur, zinc, boron, molybdenum
The grain graininess of corresponding raw material is 150-300 mesh.
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| CN108727116A (en) * | 2018-08-15 | 2018-11-02 | 松桃如阿雅观光农业产业开发有限公司 | A kind of multi-Functional Fertilizers and preparation method thereof improving peach winter resistance |
| CN110121970A (en) * | 2019-03-06 | 2019-08-16 | 贵州省烟草公司黔西南州公司 | A method of improvement vega soil property |
| CN110720275B (en) * | 2019-09-24 | 2021-11-12 | 湖南农业大学 | Cultivation method for improving salt resistance of macleaya cordata |
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| CN1872808A (en) * | 2005-05-27 | 2006-12-06 | 于兰吉 | New type compound fertilizer, and production method |
| CN102643134A (en) * | 2012-03-28 | 2012-08-22 | 常熟市滨江农业科技有限公司 | Plant source biological organic fertilizer |
| CN102718595A (en) * | 2011-10-26 | 2012-10-10 | 岭南园林股份有限公司 | Multiple-effect instillation liquid for trees and use method thereof |
| CN104446968A (en) * | 2014-11-27 | 2015-03-25 | 湖北三宁化工股份有限公司 | Water-soluble high-concentration organic-inorganic compound fertilizer for trickle and sprinkling irrigation and preparation method thereof |
| CN104774090A (en) * | 2015-03-30 | 2015-07-15 | 安徽金农生态农业科技发展有限公司 | Acidic soil adjusting fertilizer |
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|---|---|---|---|---|
| CN1872808A (en) * | 2005-05-27 | 2006-12-06 | 于兰吉 | New type compound fertilizer, and production method |
| CN102718595A (en) * | 2011-10-26 | 2012-10-10 | 岭南园林股份有限公司 | Multiple-effect instillation liquid for trees and use method thereof |
| CN102643134A (en) * | 2012-03-28 | 2012-08-22 | 常熟市滨江农业科技有限公司 | Plant source biological organic fertilizer |
| CN104446968A (en) * | 2014-11-27 | 2015-03-25 | 湖北三宁化工股份有限公司 | Water-soluble high-concentration organic-inorganic compound fertilizer for trickle and sprinkling irrigation and preparation method thereof |
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