CN105887493A - Treatment method of down feather with long-acting far infrared health effect - Google Patents
Treatment method of down feather with long-acting far infrared health effect Download PDFInfo
- Publication number
- CN105887493A CN105887493A CN201610303201.8A CN201610303201A CN105887493A CN 105887493 A CN105887493 A CN 105887493A CN 201610303201 A CN201610303201 A CN 201610303201A CN 105887493 A CN105887493 A CN 105887493A
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- Prior art keywords
- far infrared
- eider down
- weight portion
- long
- down feather
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M19/00—Treatment of feathers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/12—Aldehydes; Ketones
- D06M13/123—Polyaldehydes; Polyketones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/262—Sulfated compounds thiosulfates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/356—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms
- D06M15/3562—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms containing nitrogen
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a treatment method of down feather with long-acting far infrared health effect. The treatment method comprises three steps: firstly, pre-treating down feather with a pre-treatment solution so as to improve surface properties of fibers and improve the reaction activity; secondly, carrying out grafting treatment with glutaraldehyde in a subsequent cross-linking modification treatment process; thirdly, carrying out functionalization treatment by utilizing a carboxylation far infrared ceramic micro-powder activating solution to graft far infrared ceramic micro-powder on the fibers and further treating the modified down feather fibers with a post-treatment solution to finally obtain the down feather with the long-acting far infrared health effect. The additional economic value of down feather products is extremely improved.
Description
Technical field
The present invention relates to down fiber processing technology field, particularly relate to a kind of processing method with long-acting far infrared health care effect eider down.
Background technology
Down fiber is a kind of natural animal protein fibre, and its lightweight is bulk, air-moisture-permeable, and warming effect is splendid, is commonly used for eider down dress ornament and goods.In process of production, eiderdown raw material needs to use as inserts after a series of process, eider down woollen will through over cleaning, grease removal, deodorizing, sterilize, the program such as drying, if pretreatment process is mishandling, it will directly affect the using effect of eider down.
Owing to eider down belongs to animal matter series products, itself have inflammable, easily damage by worms, easy cooperating microorganisms, added value of product are low, maintenance and washing require the shortcomings such as high, if eider down can be applied some process means, maximize favourable factors and minimize unfavourable ones, it will widen the range of down products greatly.That reports at present carries out the processing methods such as fire-retardant, antibacterial to eider down, is the most directly mixed with inorganic agent by eider down and carries out the process of simple surface, and after so processing, the effect of product is held time short, along with washing process performance can gradually lose efficacy." down fiber fire resistance after glutaraldehyde grafting dicyanodiamine processes " literary composition carries out fire-retardant graft modification process to down fiber, although improve the fire-retardant timeliness of eider down to a certain extent, but the dicyanodiamine of grafting has certain toxicity, directly contact skin has harm, and actual application value is on the low side.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of processing method with long-acting far infrared health care effect eider down.
The present invention is achieved by the following technical solutions:
A kind of processing method with long-acting far infrared health care effect eider down, described processing method comprises the following steps:
(1) pre-treatment: first carry out eider down washing, grease removal, be dried after removal of impurities, subsequently eider down is processed 10-15h with pretreatment liquid according to the volume ratio mix and blend of 1:4-5, process is taken out after washing 3-5 time standby after terminating, wherein said pretreatment liquid is by lauryl sodium sulfate: thiocarbamide: the weight ratio of deionized water=0.5:1:80-100 is formulated；
(2) cross-linking modified process: eider down step (1) obtained puts in the glutaraldehyde water solution that concentration is 2-5%, 1-1.5h is reacted under the conditions of 55-60 DEG C, reaction is filtered after terminating, filtrate puts in carboxylated far infrared ceramic micro powder activating solution, after being uniformly mixed under the conditions of 60-65 DEG C ultrasonic reaction 2-3h, reaction is filtered after terminating, and filtrate is standby after being heat-treated 1-2h under the conditions of 70-80 DEG C；
(3) post processing: the product of step (2) is put into after 1.5-2h is soaked in stirring in aftertreatment fluid and takes out, cleaning 3-5 post-drying by deionized water and i.e. obtain described eider down finished product, wherein said aftertreatment fluid is that polyquaternium-6, ethanol, deionized water form according to the proportions of 1-1.5:20-40:100-150.
In described step (2), eider down, the volume ratio of glutaraldehyde water solution are 1:2-3, and glutaraldehyde water solution is 1-2:1 with the weight ratio of carboxylated far infrared ceramic micro powder activating solution.
Described carboxylated far infrared ceramic micro powder activating solution compound method is: take the far infrared ceramic micro powder of 5-8 weight portion and the absolute ethyl alcohol and stirring mixed grinding 2-3h of 10-12 weight portion, it is subsequently added the maleic anhydride of 1 weight portion, the Silane coupling agent KH550 of 1 weight portion, lauryl sodium sulfate and the deionized water of 30-40 weight portion of 0.1 weight portion is added after reacting 1-2h under the conditions of 50-60 DEG C, the 6-8h of high-speed stirred mixing subsequently, to obtain final product.
Eider down is pre-processed by the present invention first with pretreatment liquid, improve the surface property of fiber, improve reactivity, grafting process is carried out first with glutaraldehyde in follow-up cross-linking modified processing procedure, re-use carboxylated far infrared ceramic micro powder activating solution subsequently and carry out functionalization, far infrared ceramic micro powder is grafted on fiber, the most post-treated liquid of modified down fiber processes further, finally give the eider down with long-acting far infrared health care effect, promote the added economic value of down products greatly.
Detailed description of the invention
This embodiment uses duck down feathers to process, and processes step and is:
(1) pre-treatment: first carry out eider down washing, grease removal, be dried after removal of impurities, subsequently eider down is processed 10h with pretreatment liquid according to the volume ratio mix and blend of 1:4, process is taken out after washing 3 times standby after terminating, wherein said pretreatment liquid is by lauryl sodium sulfate: thiocarbamide: the weight ratio of deionized water=0.5:1:80 is formulated；
(2) cross-linking modified process: eider down step (1) obtained puts in the glutaraldehyde water solution that concentration is 2%, 1h is reacted under the conditions of 55 DEG C, reaction is filtered after terminating, filtrate puts in carboxylated far infrared ceramic micro powder activating solution, after being uniformly mixed under the conditions of 60 DEG C ultrasonic reaction 2h, reaction is filtered after terminating, and filtrate is standby after being heat-treated 1h under the conditions of 70 DEG C；
(3) post processing: the product of step (2) is put into after 1.5h is soaked in stirring in aftertreatment fluid and takes out, cleaning 3 post-dryings by deionized water and i.e. obtain described eider down finished product, wherein said aftertreatment fluid is that polyquaternium, ethanol, deionized water form according to the proportions of 1:20:100.
In step (2), eider down, the volume ratio of glutaraldehyde water solution are 1:2, and glutaraldehyde water solution is 1:1 with the weight ratio of carboxylated far infrared ceramic micro powder activating solution.
Carboxylated far infrared ceramic micro powder activating solution compound method is: take the far infrared ceramic micro powder of 5 weight portions and the absolute ethyl alcohol and stirring mixed grinding 2h of 10 weight portions, it is subsequently added the maleic anhydride of 1 weight portion, the Silane coupling agent KH550 of 1 weight portion, lauryl sodium sulfate and the deionized water of 30 weight portions of 0.1 weight portion is added after reacting 1h under the conditions of 50 DEG C, the 6h of high-speed stirred mixing subsequently, to obtain final product.
Duck down feathers sample after process is fluffy pliable and tough, and vapor transfer rate is 10800WVT(g/m2.d)；Air penetrability is 380.0mm/s.
Claims (3)
1. a processing method with long-acting far infrared health care effect eider down, it is characterised in that described processing method comprises the following steps:
(1) pre-treatment: first carry out eider down washing, grease removal, be dried after removal of impurities, subsequently eider down is processed 10-15h with pretreatment liquid according to the volume ratio mix and blend of 1:4-5, process is taken out after washing 3-5 time standby after terminating, wherein said pretreatment liquid is by lauryl sodium sulfate: thiocarbamide: the weight ratio of deionized water=0.5:1:80-100 is formulated；
(2) cross-linking modified process: eider down step (1) obtained puts in the glutaraldehyde water solution that concentration is 2-5%, 1-1.5h is reacted under the conditions of 55-60 DEG C, reaction is filtered after terminating, filtrate puts in carboxylated far infrared ceramic micro powder activating solution, after being uniformly mixed under the conditions of 60-65 DEG C ultrasonic reaction 2-3h, reaction is filtered after terminating, and filtrate is standby after being heat-treated 1-2h under the conditions of 70-80 DEG C；
(3) post processing: the product of step (2) is put into after 1.5-2h is soaked in stirring in aftertreatment fluid and takes out, cleaning 3-5 post-drying by deionized water and i.e. obtain described eider down finished product, wherein said aftertreatment fluid is that polyquaternium-6, ethanol, deionized water form according to the proportions of 1-1.5:20-40:100-150.
A kind of processing method with long-acting far infrared health care effect eider down, it is characterized in that, in described step (2), eider down, the volume ratio of glutaraldehyde water solution are 1:2-3, and glutaraldehyde water solution is 1-2:1 with the weight ratio of carboxylated far infrared ceramic micro powder activating solution.
A kind of processing method with long-acting far infrared health care effect eider down, it is characterized in that, described carboxylated far infrared ceramic micro powder activating solution compound method is: take the far infrared ceramic micro powder of 5-8 weight portion and the absolute ethyl alcohol and stirring mixed grinding 2-3h of 10-12 weight portion, it is subsequently added the maleic anhydride of 1 weight portion, the Silane coupling agent KH550 of 1 weight portion, lauryl sodium sulfate and the deionized water of 30-40 weight portion of 0.1 weight portion is added after reacting 1-2h under the conditions of 50-60 DEG C, the 6-8h of high-speed stirred mixing subsequently, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610303201.8A CN105887493A (en) | 2016-05-10 | 2016-05-10 | Treatment method of down feather with long-acting far infrared health effect |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610303201.8A CN105887493A (en) | 2016-05-10 | 2016-05-10 | Treatment method of down feather with long-acting far infrared health effect |
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| Publication Number | Publication Date |
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| CN105887493A true CN105887493A (en) | 2016-08-24 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610303201.8A Pending CN105887493A (en) | 2016-05-10 | 2016-05-10 | Treatment method of down feather with long-acting far infrared health effect |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110004728A (en) * | 2019-04-12 | 2019-07-12 | 宁波博洋家纺集团有限公司 | A kind of preparation process for the eiderdown quilt that fluffy insulation is mould proof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103485186A (en) * | 2013-08-16 | 2014-01-01 | 陕西科技大学 | Method for improving filling power of down feather |
| CN105420835A (en) * | 2015-12-21 | 2016-03-23 | 上海德福伦化纤有限公司 | Manufacturing method of antibacterial and far infrared health polyester fibers |
-
2016
- 2016-05-10 CN CN201610303201.8A patent/CN105887493A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103485186A (en) * | 2013-08-16 | 2014-01-01 | 陕西科技大学 | Method for improving filling power of down feather |
| CN105420835A (en) * | 2015-12-21 | 2016-03-23 | 上海德福伦化纤有限公司 | Manufacturing method of antibacterial and far infrared health polyester fibers |
Non-Patent Citations (3)
| Title |
|---|
| 张建春等: "《化纤仿毛技术原理与生产实践》", 30 September 2003, 中国纺织出版社 * |
| 李秋雁等: ""羽绒纤维经戊二醛接枝二氰二胺处理后的阻燃性能"，李秋雁等，毛纺科技，第40卷第6期，第26-29页", 《毛纺科技》 * |
| 梁红: "《化学工程与工艺专业实验》", 30 April 2009, 广东科技出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110004728A (en) * | 2019-04-12 | 2019-07-12 | 宁波博洋家纺集团有限公司 | A kind of preparation process for the eiderdown quilt that fluffy insulation is mould proof |
| CN110004728B (en) * | 2019-04-12 | 2021-11-02 | 宁波博洋家纺集团有限公司 | Preparation process of fluffy warm-keeping mildew-proof down quilt |
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Application publication date: 20160824 |