CN105860634B - A kind of art painting and preparation method thereof - Google Patents
A kind of art painting and preparation method thereof Download PDFInfo
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- CN105860634B CN105860634B CN201610293996.9A CN201610293996A CN105860634B CN 105860634 B CN105860634 B CN 105860634B CN 201610293996 A CN201610293996 A CN 201610293996A CN 105860634 B CN105860634 B CN 105860634B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of art painting and preparation method thereof, art painting is prepared from the following materials：Xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator, hydroxymethyl cellulose, ceramic microsphere, natural pigment, polyvinyl alcohol, drier, surfactant.Art painting of the present invention colours, and brightness is high, and persistence length, good with colouring substance compactness, instant component proportioning is scientific and reasonable, and preparation method is easily operated, and cost is cheap, is adapted to industrially large-scale promotion.
Description
Technical field
The present invention relates to pigment art, and in particular to a kind of art painting and preparation method thereof.
Background technology
Art painting general at present is divided to two kinds of organic pigment and inorganic pigment.Pigment characteristics includes sun-proof, resistance to water logging, resistance to
Sour, alkaline-resisting, organic solvent-resistant, heat-resisting, stable crystal form, dispersiveness and covering power etc..And the difference of organic pigment and dyestuff is
It does not have affinity with being colored object, and organic pigment only is attached into body surface by adhesive or film forming matter, or
Interior of articles is mixed in, colours object.It produces the production of required intermediate, production equipment and building-up process with dyestuff
It is similar, therefore organic pigment is often organized to production in dye industry.Organic pigment leads to compared with general inorganic pigment
Often with there is higher tinting strength, tinting power, particle easily grinds and disperseed, is not easy to precipitate, and color is also more bright-coloured, but sun-proof, heat-resisting, weather-proof
Poor-performing.
The art painting on market does not take into full account using chemical industry monomer as main raw material(s) in design process is formulated at present
Medium and working condition are used to it, causes existing art painting colouring, brightness, persistence, with colouring substance compactness
Etc. far can not meet requirement, therefore it is to have very much to find a kind of new art painting and preparation method thereof
It is necessary.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of art painting and preparation method thereof so that is produced
There is art painting art painting of the present invention to colour, and brightness is high, persistence length, with colouring substance compactness it is good the characteristics of.
To realize object above, the present invention is achieved by the following technical programs：The invention provides a kind of fine arts face
Material, is prepared by the raw material of following parts by weight：Xanthans：15-35 parts, distilled water：15-35 parts, polyoxyethylene oleic acid ester：
5-15 parts, vinyl triamine：1-8 parts, initiator：1-5 parts, hydroxymethyl cellulose：1-8 parts, ceramic microsphere：1-5 parts, aluminium powder：
1-5 parts, silica：1-5 parts, natural pigment：6-15 parts, polyvinyl alcohol：1-5 parts, drier：1-6 parts, surfactant：
1-4.5 part；
Its preparation method is as follows：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into machine
In agitating device, mixing A liquid is added drop-wise in agitating device with 80-100 drops/min speed and reacts 1-3h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, control mixing speed to turn/min for 350-400, be warming up to 60-80 DEG C of pre-emulsification 0.5-1 hour in advance；Then drop
Low mixing speed turns/min to 180-200, is again heated to 80-100 DEG C, carries out polymerisation 30-50min, must mix C liquid；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, while mixing speed rises to 250-320 and turns/min, is eventually adding natural pigment stirring 2-5h.
Preferably, it is prepared by the raw material of following parts by weight：Xanthans：16-33 parts, distilled water：18-33 parts, oil
Sour polyoxyethylene ester：6-12 parts, vinyl triamine：4-6 parts, initiator：2-3 parts, hydroxymethyl cellulose：2-6 parts, ceramics are micro-
Ball：1-5 parts, aluminium powder：2-3 parts, silica：2-3 parts, natural pigment：7-13 parts, polyvinyl alcohol：2-4 parts, drier：2-5
Part, surfactant：2-4 parts.
Preferably, it is prepared by the raw material of following parts by weight：Xanthans：16 parts, distilled water：18 parts, oleic acid polyoxy
Vinyl acetate：6 parts, vinyl triamine：4 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：3 parts, aluminium powder：2 parts,
Silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：3 parts, drier：3 parts, surfactant：3 parts.
Preferably, it is prepared by the raw material of following parts by weight：Xanthans：20 parts, distilled water：22 parts, oleic acid polyoxy
Vinyl acetate：8 parts, vinyl triamine：5 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：4 parts, aluminium powder：2 parts,
Silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：4 parts, drier：4 parts, surfactant：4 parts.
Preferably, it is dry to be that polyurethane drier, acrylic acid drier, EVA emulsions drier, polyester are urged for described drier
Agent, epoxy drier, the one of which of alkyd drier.
Preferably, described natural pigment be carotenoid, lycopene, natural Beta-carotene, mixing carotenoid,
Maize, kermes custom citraurin, safron, Gardenia Yellow, gardenia green pigment, capsicum red pigment, pimento red pigment
One of which.
Preferably, the whipping temp in described preparation method step (2) is 40-70 DEG C, the whipping temp in step (4)
For 80-95 DEG C.
Beneficial effect of the present invention：
Art painting of the present invention is used as raw material using xanthans, xanthans with to insoluble solid and oil droplet with well
Suspension effect, and can quickly be dissolved in water, have good water solubility, xanthan gum solution has low concentration high viscosity in addition
Characteristic, sufficiently stable to soda acid, in PH, its viscosity is unaffected between 5-10.Polyoxyethylene oleic acid ester is surface-active substance
Matter, there is hydrophilic group and lipophilic group simultaneously in molecule, art painting can be helped more rapidly easily to mix colours, oleic acid gathers in addition
Oxygen vinyl acetate biological degradability is good, and the pollution to environment is small；Vinyl triamine has good film performance, and (such as lustrous surface is excellent
It is different), it can prevent the bloom and water spots phenomenon of pigment, good colour stability, good adhesive property and resistant to chemical etching
It performance, can colour synthesized art painting, persistence length；The present invention, can using natural pigment as coloring pigment
It is more preferable to realize that synthesized pigment brightness is high, the natural good characteristic of color.The present invention passes through the scientific matching to raw material so that
The art painting produced not only colours, and brightness is high, persistence length, good with colouring substance compactness, and in use its
Very big change will not occur for performance, and shelf lives length, preparation method of the present invention is easily operated, and cost is cheap, is adapted to industrially
Large-scale promotion.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the implementation of the present invention
Example, the technical scheme in the embodiment of the present invention is clearly and completely described.Based on the embodiment in the present invention, this area
The every other embodiment that those of ordinary skill is obtained under the premise of creative work is not made, belongs to protection of the present invention
Scope.
Embodiment 1：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：16 parts, distilled water：18 parts, oil
Sour polyoxyethylene ester：8 parts, vinyl triamine：4 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：2 parts, aluminium
Powder：2 parts, silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：3 parts, polyurethane drier：3 parts, surfactant：3
Part, wherein natural pigment is carotenoid.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 40 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 80 drops/min speed and reacts 1h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 350 turns/min to control mixing speed, is warming up to 60 DEG C of pre-emulsifications in advance 0.5 hour；Then stirring speed is reduced
Degree is again heated to 80 DEG C, carries out polymerisation 30min, must mix C liquid to 180 turns/min；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 80 DEG C to set temperature, and mixing speed rises to 250 turns/min, is eventually adding natural pigment stirring 2h.
Embodiment 2：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：20 parts, distilled water：18 parts, oil
Sour polyoxyethylene ester：7 parts, vinyl triamine：4 parts, 3 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：3 parts,
Aluminium powder：2 parts, silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：3 parts, acrylic acid drier：3 parts, surfactant：3
Part, wherein natural pigment is maize.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 50 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 80 drops/min speed and reacts 2h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 350 turns/min to control mixing speed, is warming up to 60 DEG C of pre-emulsifications in advance 0.5 hour；Then stirring speed is reduced
Degree is again heated to 80 DEG C, carries out polymerisation 30min, must mix C liquid to 180 turns/min；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 80 DEG C to set temperature, and mixing speed rises to 250 turns/min, is eventually adding natural pigment stirring 3h.
Embodiment 3：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：18 parts, distilled water：20 parts, oil
Sour polyoxyethylene ester：8 parts, vinyl triamine：5 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：3 parts, aluminium
Powder：2 parts, silica：3 parts, natural pigment：8 parts, polyvinyl alcohol：4 parts, EVA emulsion drier：4 parts, surfactant：3
Part, wherein natural pigment is safron.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 60 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 80 drops/min speed and reacts 2h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 360 turns/min to control mixing speed, is warming up to 60 DEG C of pre-emulsifications in advance 0.5 hour；Then stirring speed is reduced
Degree is again heated to 80 DEG C, carries out polymerisation 40min, must mix C liquid to 180 turns/min；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 85 DEG C to set temperature, and mixing speed rises to 280 turns/min, is eventually adding natural pigment stirring 3h.
Embodiment 4：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：30 parts, distilled water：20 parts, oil
Sour polyoxyethylene ester：8 parts, vinyl triamine：5 parts, initiator：2 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：1 part, aluminium
Powder：2 parts, silica：3 parts, natural pigment：10 parts, polyvinyl alcohol：4 parts, polyester drier：5 parts, surfactant：4 parts,
Wherein natural pigment is kermes custom citraurin.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 50 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 80 drops/min speed and reacts 2h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 350 turns/min to control mixing speed, is warming up to 80 DEG C of pre-emulsifications in advance 1 hour；Then mixing speed is reduced
To 200 turns/min, 80 DEG C are again heated to, polymerisation 40min is carried out, C liquid must be mixed；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 80 DEG C to set temperature, and mixing speed rises to 250 turns/min, is eventually adding natural pigment stirring 3h.
Embodiment 5：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：33 parts, distilled water：30 parts, oil
Sour polyoxyethylene ester：8 parts, vinyl triamine：4 parts, initiator：2 parts, hydroxymethyl cellulose：3 parts, ceramic microsphere：5 parts, aluminium
Powder：2 parts, silica：2 parts, natural pigment：8 parts, polyvinyl alcohol：2 parts, polyester drier：2 parts, surfactant：2 parts,
Wherein natural pigment is safron.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 40 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 90 drops/min speed and reacts 2h, B liquid must be mixed；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 350 turns/min to control mixing speed, is warming up to 60 DEG C of pre-emulsifications in advance 1 hour；Then mixing speed is reduced
To 200 turns/min, 80 DEG C are again heated to, polymerisation 40min is carried out, C liquid must be mixed；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 85 DEG C to set temperature, and mixing speed rises to 250 turns/min, is eventually adding natural pigment stirring 3h.
Embodiment 6：
A kind of art painting, it is prepared by the raw material of following parts by weight：Xanthans：19 parts, distilled water：20 parts, oil
Sour polyoxyethylene ester：8 parts, vinyl triamine：6 parts, initiator：3 parts, hydroxymethyl cellulose：4 parts, ceramic microsphere：1 part, aluminium
Powder：3 parts, silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：4 parts, alkyd drier：3 parts, surfactant：3 parts,
Wherein natural pigment is gardenia green pigment.
Preparation method comprises the following steps：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first,
In well mixed suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into temperature
Spend in 70 DEG C of agitating devices, mixing A liquid to be added drop-wise in agitating device with 100 drops/min speed and reacts 3h, B must be mixed
Liquid；
(3) B liquid input will be mixed and is equipped with agitator, reflux condenser, the steam heating response kettle for measuring dropper
In, start stirring, it is 400 turns/min to control mixing speed, is warming up to 80 DEG C of pre-emulsifications in advance 1 hour；Then mixing speed is reduced
To 200 turns/min, 80 DEG C are again heated to, polymerisation 40min is carried out, C liquid must be mixed；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating equipped with mixing C liquid
In reactor, it is 85 DEG C to set temperature, and mixing speed rises to 250 turns/min, is eventually adding natural pigment stirring 3h.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to its middle part min technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (7)
1. a kind of art painting, it is characterised in that be prepared by the raw material of following parts by weight：Xanthans：15-35 parts, steam
Distilled water：15-35 parts, polyoxyethylene oleic acid ester：5-15 parts, vinyl triamine：1-8 parts, initiator：1-5 parts, hydroxylmethyl cellulose
Element：1-8 parts, ceramic microsphere：1-5 parts, aluminium powder：1-5 parts, silica：1-5 parts, natural pigment：6-15 parts, polyvinyl alcohol：1-
5 parts, drier：1-6 parts, surfactant：1-4.5 part；
Its preparation method is as follows：
(1) xanthans, distilled water, polyoxyethylene oleic acid ester, vinyl triamine, initiator are weighed in parts by weight first, is mixed
In even suction metering dropper, A liquid must be mixed；
(2) hydroxymethyl cellulose, ceramic microsphere, aluminium powder, silica are weighed in parts by weight, are added water dissolving and are poured into stirring dress
In putting, mixing A liquid is added drop-wise in agitating device with 80-100 drops/min speed and reacts 1-3h, B liquid must be mixed；
(3) B liquid input will be mixed to be equipped with the steam heating response kettle of agitator, reflux condenser, metering dropper, opened
Dynamic stirring, controls mixing speed to turn/min for 350-400, is warming up to 60-80 DEG C of pre-emulsification 0.5-1 hour in advance；Then reduce and stir
Mix speed and turn/min to 180-200, be again heated to 80-100 DEG C, carry out polymerisation 30-50min, C liquid must be mixed；
(4) polyvinyl alcohol, drier, surfactant are weighed in parts by weight is put into the steam heating response equipped with mixing C liquid
In kettle, while mixing speed rises to 250-320 and turns/min, is eventually adding natural pigment stirring 2-5h.
2. art painting as claimed in claim 1, it is characterised in that be prepared by the raw material of following parts by weight：Xanthan
Glue：16-33 parts, distilled water：18-33 parts, polyoxyethylene oleic acid ester：6-12 parts, vinyl triamine：4-6 parts, initiator：2-3
Part, hydroxymethyl cellulose：2-6 parts, ceramic microsphere：1-5 parts, aluminium powder：2-3 parts, silica：2-3 parts, natural pigment：7-13
Part, polyvinyl alcohol：2-4 parts, drier：2-5 parts, surfactant：2-4 parts.
3. art painting as claimed in claim 2, it is characterised in that be prepared by the raw material of following parts by weight：Xanthan
Glue：16 parts, distilled water：18 parts, polyoxyethylene oleic acid ester：6 parts, vinyl triamine：4 parts, initiator：3 parts, hydroxylmethyl cellulose
Element：4 parts, ceramic microsphere：3 parts, aluminium powder：2 parts, silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：3 parts, drier：3
Part, surfactant：3 parts.
4. art painting as claimed in claim 2, it is characterised in that be prepared by the raw material of following parts by weight：Xanthan
Glue：20 parts, distilled water：22 parts, polyoxyethylene oleic acid ester：8 parts, vinyl triamine：5 parts, initiator：3 parts, hydroxylmethyl cellulose
Element：4 parts, ceramic microsphere：4 parts, aluminium powder：2 parts, silica：3 parts, natural pigment：9 parts, polyvinyl alcohol：4 parts, drier：4
Part, surfactant：4 parts.
5. art painting as claimed in claim 1, it is characterised in that described drier is polyurethane drier, acrylic acid
Drier, EVA emulsions drier, polyester drier, epoxy drier, the one of which of alkyd drier.
6. art painting as claimed in claim 1, it is characterised in that described natural pigment is lycopene, natural carrot
Element, mixing carotenoid, maize, kermes custom citraurin, safron, Gardenia Yellow, gardenia green pigment, capsanthin
The one of which of pigment, pimento red pigment.
7. art painting as claimed in claim 1, it is characterised in that the whipping temp in described preparation method step (2)
For 40-70 DEG C, the whipping temp in step (4) is 80-95 DEG C.
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| CN107573736A (en) * | 2017-09-07 | 2018-01-12 | 代晓蕾 | A kind of art painting and preparation method thereof |
| CN108559335B (en) * | 2018-05-03 | 2022-05-20 | 仲恺农业工程学院 | Stable non-toxic environment-friendly pigment for printing and preparation method thereof |
| CN109796860A (en) * | 2019-02-28 | 2019-05-24 | 烟台南山学院 | A kind of drawing aqueous polyurethane art painting and preparation method thereof |
| CN111518426A (en) * | 2020-06-15 | 2020-08-11 | 山东科技大学 | Art pigment and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5582636A (en) * | 1995-06-19 | 1996-12-10 | Schiraldi; Michael T. | Medium for china paints for porcelain, ceramic, and stoneware articles |
| CN101696330B (en) * | 2009-10-27 | 2012-05-30 | 南昌航天文体用品有限公司 | Concentrated poster paint and preparation method thereof |
| CN102796420B (en) * | 2012-09-11 | 2014-08-13 | 上海实业马利画材有限公司 | Water-based ink color painting pigment with shading effect used on rice paper |
| CN104017436B (en) * | 2014-05-28 | 2016-11-23 | 南昌大学 | A kind of child's pigment being made up of comestible composition |
| CN105238115A (en) * | 2014-07-10 | 2016-01-13 | 上海国韵实业有限公司 | Gouache and preparation method therefor |
| CN105038354A (en) * | 2015-06-30 | 2015-11-11 | 河南行知专利服务有限公司 | Biological environment-friendly pigment for artistic designing with strong tinting strength |
-
2016
- 2016-05-05 CN CN201610293996.9A patent/CN105860634B/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN105860634A (en) | 2016-08-17 |
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