CN105853298B - A kind of preparation method of natural camellia seed hair shampoo article - Google Patents
A kind of preparation method of natural camellia seed hair shampoo article Download PDFInfo
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- CN105853298B CN105853298B CN201610348397.2A CN201610348397A CN105853298B CN 105853298 B CN105853298 B CN 105853298B CN 201610348397 A CN201610348397 A CN 201610348397A CN 105853298 B CN105853298 B CN 105853298B
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- camellia seed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a kind of preparation methods of natural camellia seed hair shampoo article, belong to hair shampoo article preparation technical field.The camellia seed hair shampoo article after camellia seed is dry, crushing, takes a part of camellia seed using supercritical CO using camellia seed as raw material2Extraction carries out de-oiling, and passes through boiling, extracting solution is obtained by filtration, and extracting solution is carried out after adsorbing and being eluted using ethyl alcohol by 101 large pore resin absorption columns, is condensed into thick paste A；It takes another part camellia seed to carry out de-oiling using squeezing method again, and passes through boiling, extracting solution is obtained by filtration, extracting solution is concentrated, merge thick paste A and be condensed into thick paste to obtain the final product.Using supercritical CO2Extraction can reach that de-oiling is clean, effect conducive to separation Tea Saponin, the advantages of conventional tea bran is had one's hair wash can be retained using concentration extraction is carried out again again after conventional press method de-oiling, therefore, the preparation method is easy to the hair shampoo article that foaming abundancy is made, maintains the pure natural property of raw material.
Description
[technical field]
The invention belongs to bath accessory technical fields in daily necessities, and in particular to a kind of system of natural camellia seed hair shampoo article
Preparation Method.
[background technique]
Camellia seed obtained tea bran after squeezing and taking oil, is traditional hair shampoo article, has hair glossy black, no with its hair washing
Easy alopecia and other effects.Modern science proves that tea bran contains amphoteric surfactant Tea Saponin, has the function of hair-washing hair-care.Tea bran
Traditional application method be not suitable for modern consumption idea, and extract Tea Saponin merely using then eliminating traditional application method institute
Reach the nutritive validity of tea bran hair washing.
The method for extracting Tea Saponin has alkaline process and resin adsorption method.Alkaline process environmental pollution weight, resin adsorption rule due to
Ideal effect is not achieved to the damage of resin in residual grease in tea bran.
Therefore, needing to research and develop a kind of can efficiently separate Tea Saponin but also retain the preparation of the hair shampoo article of nutritive validity
Method.
[summary of the invention]
The present invention provides a kind of preparation method of natural camellia seed hair shampoo article, to solve existing hair shampoo article preparation method
The problem that middle Tea Saponin extraction effect is poor, nutritional ingredient is low.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of preparation method of natural camellia seed hair shampoo article, comprising the following steps:
After S1, decladding camellia seed is dry, crushing, 32-42 mesh is crossed；
S2, it calculates based on parts by weight, 100-300 parts of camellia seed after being sieved in step S1 is taken, using supercritical CO2Extraction
Method carries out de-oiling；
S3, the camellia seed after de-oiling in step S2 is transferred to 6m3Multi-functional extractor after adding boiling to boil, keeps the temperature 0.5-
1.2 hours, filtrate I is obtained by filtration, filter residue is stayed in multi-functional extractor；
S4, after adding the filter residue of step S3 boiling to boil, 0.5-1.2 hours is kept the temperature, filtrate II, merging filtrate I is obtained by filtration
With filtrate II, filtrate III is obtained, it is cooling；
S5, it after being adsorbed the filtrate III after merging in step S4 with 101 macroporous absorbent resin of 300kg, then uses
The ethyl alcohol of 65%-75% is eluted, and eluent is collected；
S6, the step S5 eluent collected is condensed into 10-20 parts of thick paste A, left stand-by；
S7, it calculates based on parts by weight, takes 50-150 parts of camellia seed after being sieved in step S1, taken off using squeezing method
Oil；
S8, the camellia seed after de-oiling in step S7 is transferred to 6m3Multi-functional extractor adds boiling boiling heat preservation 0.5-1.2
Hour, filtrate IV is obtained by filtration, filter residue is stayed in multi-functional extractor；
S9, the filter residue of step S8 is added to boiling boiling heat preservation 0.5-1.2 hours, filtrate V, IV He of merging filtrate is obtained by filtration
Filtrate V obtains filtrate VI, cooling；
S10, the filtrate VI that step S9 merges is condensed into thick paste B, merged with the thick paste A of step S6, being condensed into density is
1.10~1.13g/cm355-90 parts of thick paste；
S11, the addition essence of thick paste obtained by step S10 and preservative are uniformly mixed, pack and has one's hair wash up to natural camellia seed
Articles.
Preferably, the de-oiling temperature of step S2 is 30-42 DEG C, pressure 15-27KPa, duration 2-3 hours.
Preferably, add the parts by weight of water for 15 times of the camellia seed parts by weight after sieving in step S2 in step S3.
Preferably, add the parts by weight of water for 10 times of the camellia seed parts by weight after sieving in step S2 in step S4.
Preferably, ethyl alcohol used is 800-950L in step S5.
Preferably, add the parts by weight of water for 15 times of the camellia seed parts by weight after sieving in step S7 in step S8.
Preferably, add the parts by weight of water for 10 times of the camellia seed parts by weight after sieving in step S7 in step S9.
Preferably, using supercritical CO2The weight of the camellia seed of extraction de-oiling and the camellia seed for using squeezing method de-oiling
Weight ratio be 2:1.
The invention has the following advantages:
(1) preparation method of the present invention combines supercritical CO2Extraction and conventional press method carry out de-oiling, can reach de-
The clean effect of oil, and the advantages of conventional tea bran is had one's hair wash can be retained, therefore, the preparation method is easy to be made foaming abundancy, protects
The hair shampoo article of the pure natural property of raw material is held.
(2) supercritical CO is used2Extraction carries out de-oiling, can be clean with de-oiling, separates, solves conducive to the extraction of Tea Saponin
Since the residual grease in tea bran the damage of resin is not achieved the problem of Tea Saponin effectively extracts separation.
[specific embodiment]
It is specifically described combined with specific embodiments below.
Embodiment 1
A kind of preparation method of natural camellia seed hair shampoo article, comprising the following steps:
After S1, decladding camellia seed is dry, crushing, 32 meshes are crossed；
S2, it calculates based on parts by weight, the camellia seed 100kg after being sieved in step S1 is taken, using supercritical CO2Extraction into
Row de-oiling, de-oiling temperature are 30 DEG C, pressure 15KPa, duration 2 hours；
S3, the camellia seed after de-oiling in step S2 is transferred to 6m3Multi-functional extractor, adds 1.5m3After boiling boiling, heat preservation
0.5 hour, filtrate I is obtained by filtration, filter residue is stayed in multi-functional extractor；
S4, the filter residue of step S3 is added into 1m3After boiling boiling, 0.5 hour is kept the temperature, filtrate II, I He of merging filtrate is obtained by filtration
Filtrate II obtains filtrate III, cooling；
S5, after being adsorbed the filtrate III after merging in step S4 with 101 macroporous absorbent resin of 300kg, then 950L is used
65% ethyl alcohol is eluted, and eluent is collected；
S6, the step S5 eluent collected is condensed into thick paste A 10kg, left stand-by；
S7, it calculates based on parts by weight, takes the camellia seed 50kg after being sieved in step S1, de-oiling is carried out using squeezing method；
S8, the camellia seed after de-oiling in step S7 is transferred to 6m3Multi-functional extractor, adds 0.75m3Boiling boiling heat preservation 0.5
Hour, filtrate IV is obtained by filtration, filter residue is stayed in multi-functional extractor；
S9, the filter residue of step S8 is added into 0.5m3Boiling boiling heat preservation 0.5 hour, filtrate V, IV He of merging filtrate is obtained by filtration
Filtrate V obtains filtrate VI, cooling；
S10, the filtrate VI that step S9 merges is condensed into thick paste B, merged with the thick paste A of step S6, being condensed into density is
1.10g/cm3Thick paste 55kg；
S11, the addition essence of thick paste obtained by step S10 and preservative are uniformly mixed, pack and has one's hair wash up to natural camellia seed
Articles.
Embodiment 2
A kind of preparation method of natural camellia seed hair shampoo article, comprising the following steps:
After S1, decladding camellia seed is dry, crushing, 40 meshes are crossed；
S2, it calculates based on parts by weight, the camellia seed 200kg after being sieved in step S1 is taken, using supercritical CO2Extraction into
Row de-oiling, 40 DEG C of temperature, pressure 25KPa, the time 2.5 hours；
S3, the camellia seed after de-oiling in step S2 is transferred to 6m3Multi-functional extractor, adds 3m3After boiling boiling, heat preservation 1 is small
When, filtrate I is obtained by filtration, filter residue is stayed in multi-functional extractor；
S4, the filter residue of step S3 is added into 2m3After boiling boiling, 1 hour is kept the temperature, filtrate II, merging filtrate I and filter is obtained by filtration
Liquid II obtains filtrate III, cooling；
S5, after being adsorbed the filtrate III after merging in step S4 with 101 macroporous absorbent resin of 300kg, then 900L is used
70% ethyl alcohol is eluted, and eluent is collected；
S6, the step S5 eluent collected is condensed into thick paste A16kg, left stand-by；
S7, it calculates based on parts by weight, takes the camellia seed 100kg after being sieved in step S1, de-oiling is carried out using squeezing method；
S8, the camellia seed after de-oiling in step S7 is transferred to 6m3Multi-functional extractor, adds 1.5m3Boiling boiling heat preservation 1 is small
When, filtrate IV is obtained by filtration, filter residue is stayed in multi-functional extractor；
S9, the filter residue of step S8 is added into 1.0m3Boiling boiling heat preservation 1 hour, filtrate V, merging filtrate IV and filter is obtained by filtration
Liquid V obtains filtrate VI, cooling；
S10, the filtrate VI that step S9 merges is condensed into thick paste B, merged with the thick paste A of step S6, being condensed into density is
1.12g/cm3Thick paste 62kg；
S11, the addition essence of thick paste obtained by step S10 and preservative are uniformly mixed, pack and has one's hair wash up to natural camellia seed
Articles.
Embodiment 3
A kind of preparation method of natural camellia seed hair shampoo article, comprising the following steps:
After S1, decladding camellia seed is dry, crushing, 42 meshes are crossed；
S2, it calculates based on parts by weight, the camellia seed 300kg after being sieved in step S1 is taken, using supercritical CO2Extraction into
Row de-oiling, 42 DEG C of temperature, pressure 27KPa, the time 3 hours；
S3, the camellia seed after de-oiling in step S2 is transferred to 6m3Multi-functional extractor, adds 4.5m3After boiling boiling, heat preservation
1.2 hours, filtrate I is obtained by filtration, filter residue is stayed in multi-functional extractor；
S4, the filter residue of step S3 is added into 3m3After boiling boiling, 1.2 hours are kept the temperature, filtrate II, I He of merging filtrate is obtained by filtration
Filtrate II obtains filtrate III, cooling；
S5, after being adsorbed the filtrate III after merging in step S4 with 101 macroporous absorbent resin of 300kg, then 800L is used
75% ethyl alcohol is eluted, and eluent is collected；
S6, the step S5 eluent collected is condensed into thick paste A 20kg, left stand-by；
S7, it calculates based on parts by weight, takes the camellia seed 150kg after being sieved in step S1, de-oiling is carried out using squeezing method；
S8, the camellia seed after de-oiling in step S7 is transferred to 6m3Multi-functional extractor, adds 2.25m3After boiling boiling, heat preservation
1.2 hours, filtrate IV is obtained by filtration, filter residue is stayed in multi-functional extractor；
S9, the filter residue of step S8 is added into 1.5m3Boiling boiling heat preservation 1.2 hours, filtrate V, IV He of merging filtrate is obtained by filtration
Filtrate V obtains filtrate VI, cooling；
S10, the filtrate VI that step S9 merges is condensed into thick paste B, merged with the thick paste A of step S6, being condensed into density is
1.13g/cm3Thick paste 90kg；
S11, the addition essence of thick paste obtained by step S10 and preservative are uniformly mixed, pack and has one's hair wash up to natural camellia seed
Articles.
The specific implementation of the invention is not to be limited to these illustrations for the above content, and technology belonging to the present invention is led
For the those of ordinary skill in domain, without departing from the inventive concept of the premise, a number of simple deductions or replacements can also be made,
It all shall be regarded as belonging to present invention scope of patent protection determined by the appended claims.
Claims (8)
1. a kind of preparation method of natural camellia seed hair shampoo article, which comprises the following steps:
After S1, decladding camellia seed is dry, crushing, 32-42 mesh is crossed；
S2, it calculates based on parts by weight, 100-300 parts of camellia seed after being sieved in step S1 is taken, using supercritical CO2Extraction into
Row de-oiling；
S3, after adding the camellia seed after de-oiling in step S2 boiling to boil, 0.5-1.2 hours is kept the temperature, filtrate I is obtained by filtration, leaves
Filter residue is spare；
S4, after adding the filter residue of step S3 boiling to boil, 0.5-1.2 hours are kept the temperature, filtrate II, merging filtrate I and filter is obtained by filtration
Liquid II obtains filtrate III；
S5, after the filtrate III after merging in step S4 is adsorbed with 101 macroporous absorbent resins, then with the second of 65%-75%
Alcohol is eluted, and eluent is collected；
S6, the step S5 eluent collected is condensed into 10-20 parts of thick paste A, left stand-by；
S7, it calculates based on parts by weight, takes 50-150 parts of camellia seed after being sieved in step S1, de-oiling is carried out using squeezing method；
S8, the camellia seed after de-oiling in step S7 is added to boiling boiling heat preservation 0.5-1.2 hours, filtrate IV is obtained by filtration, leaves filter
Slag is spare；
S9, the filter residue of step S8 is added to boiling boiling heat preservation 0.5-1.2 hours, filtrate V, merging filtrate IV and filtrate is obtained by filtration
V, obtain filtrate VI；
S10, the filtrate VI that step S9 merges is condensed into thick paste B, merged with the thick paste A of step S6, being condensed into density is 1.10
~1.13g/cm355-90 parts of thick paste；
S11, the addition essence of thick paste obtained by step S10 and preservative are uniformly mixed, are packed up to natural camellia seed hair shampoo article.
2. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that the de-oiling of step S2
Temperature is 30 DEG C, pressure 15-27KPa, duration 2-3 hours.
3. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that add water in step S3
Parts by weight be 15 times of camellia seed parts by weight after being sieved in step S2.
4. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that add water in step S4
Parts by weight be 10 times of camellia seed parts by weight after being sieved in step S2.
5. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that used in step S5
Ethyl alcohol is 800-950L.
6. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that add water in step S8
Parts by weight be 15 times of camellia seed parts by weight after being sieved in step S7.
7. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that add water in step S9
Parts by weight be 10 times of camellia seed parts by weight after being sieved in step S7.
8. the preparation method of natural camellia seed hair shampoo article according to claim 1, which is characterized in that use supercritical CO2
The weight of the camellia seed of extraction de-oiling and use squeezing method de-oiling camellia seed weight ratio for 2:1.
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| CN200994863Y (en) * | 2006-09-18 | 2007-12-26 | 曹维 | Health-care paper pants containing tea-seed essence |
| CN101838302A (en) * | 2010-05-25 | 2010-09-22 | 南昌大学 | Method for extracting sasanquasaponin |
| CN102641387A (en) * | 2012-05-03 | 2012-08-22 | 天津大学 | Method for supercritically extracting natural activity ingredient oil tea polyphenol from oil tea fruits |
| CN102670447A (en) * | 2012-05-22 | 2012-09-19 | 广州市娇兰化妆品有限公司 | Natural plant extract for hair care and preparation method and application thereof |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
| CN104042461A (en) * | 2013-03-12 | 2014-09-17 | 长沙理工大学 | Natural plant shampoo employing camellia seed products as base-material and preparation method thereof |
| CN104072468A (en) * | 2013-03-26 | 2014-10-01 | 宜春元博山茶油科技农业开发有限公司 | Proanthocyanidin extraction process from camellia seed hull |
-
2016
- 2016-05-24 CN CN201610348397.2A patent/CN105853298B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN200994863Y (en) * | 2006-09-18 | 2007-12-26 | 曹维 | Health-care paper pants containing tea-seed essence |
| CN101838302A (en) * | 2010-05-25 | 2010-09-22 | 南昌大学 | Method for extracting sasanquasaponin |
| CN102641387A (en) * | 2012-05-03 | 2012-08-22 | 天津大学 | Method for supercritically extracting natural activity ingredient oil tea polyphenol from oil tea fruits |
| CN102670447A (en) * | 2012-05-22 | 2012-09-19 | 广州市娇兰化妆品有限公司 | Natural plant extract for hair care and preparation method and application thereof |
| CN104042461A (en) * | 2013-03-12 | 2014-09-17 | 长沙理工大学 | Natural plant shampoo employing camellia seed products as base-material and preparation method thereof |
| CN104072468A (en) * | 2013-03-26 | 2014-10-01 | 宜春元博山茶油科技农业开发有限公司 | Proanthocyanidin extraction process from camellia seed hull |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
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