CN105853298A - Preparation method of natural camellia seed shampoo - Google Patents
Preparation method of natural camellia seed shampoo Download PDFInfo
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- CN105853298A CN105853298A CN201610348397.2A CN201610348397A CN105853298A CN 105853298 A CN105853298 A CN 105853298A CN 201610348397 A CN201610348397 A CN 201610348397A CN 105853298 A CN105853298 A CN 105853298A
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- camellia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a preparation method of a natural camellia seed shampoo, and belongs to the technical field of shampoo preparation. The camellia seed shampoo takes camellia seeds as the raw material, the camellia seeds are dried and smashed, one part of the camellia seeds are taken for deoiling through a supercritical CO2 extraction method, water boiling and filtration are conducted, an extracting solution is obtained, and the extracting solution is subjected to adsorption through a 101 macroporous resin column and subjected to elution with ethanol and then concentrated into thick paste A; the other part of the camellia seeds are subjected to deoiling through a squeezing method, water boiling and filtration are conducted to obtain an extracting solution, the extracting solution is concentrated and mixed with the thick paste A to be concentrated into thick paste, and the natural camellia seed shampoo is obtained. The effects of being complete in deoiling and benefiting tea saponin separation can be achieved through the supercritical CO2 extraction method, after deoiling is conducted through a traditional squeezing method, extraction and concentration are conducted, and the advantage of traditional tea bran hair washing can be preserved; therefore, by means of the preparation method, the shampoo which is rich in foam and keeps the pure natural property of the raw material is obtained easily.
Description
[technical field]
The invention belongs to bath accessory technical field in article of everyday use, be specifically related to a kind of natural Camellia hair shampoo article
Preparation method.
[background technology]
The tea bran that Camellia obtains after squeezing takes oil, is traditional hair shampoo article, has hair crow with its hair washing
Bright, be difficult to the effects such as alopecia.Modern science proves that tea bran contains amphoteric surfactant tea saponin, has hair washing
The effect of hair care.Traditional using method of tea bran is not suitable for modern consumption idea, and extracts merely tea saponin and use
Eliminate the most again the nutritive validity of tradition using method reached tea bran hair washing.
The method extracting tea saponin has alkaline process and resin adsorption method.Alkaline process environmental pollution weight, resin absorption rule
Owing to the residual oils and fats in tea bran does not reaches ideal effect to the damage of resin.
Therefore, need research and development badly a kind of to efficiently separate tea saponin, the hair shampoo article of nutritive validity can be retained again
Preparation method.
[summary of the invention]
The present invention provides the preparation method of a kind of natural Camellia hair shampoo article, prepares solving existing hair shampoo article
The problem that in method, tea saponin extraction effect is poor, nutritional labeling is low.
For solve above technical problem, the present invention by the following technical solutions:
The preparation method of a kind of natural Camellia hair shampoo article, comprises the following steps:
S1, the Camellia that will shell be dried, pulverize after, cross 32-42 mesh sieve；
S2, calculate with parts by weight, take the Camellia 100-300 part after sieving in step S1, use super facing
Boundary CO2Extraction carries out removing oil；
S3, the Camellia after removing oil in step S2 is transferred to 6m3Multi-functional extractor, after adding water boil, protects
Temperature 0.5-1.2 hour, is filtrated to get filtrate I, is stayed in multi-functional extractor by filtering residue；
S4, the filtering residue of step S3 is added water boil after, be incubated 0.5-1.2 hour, be filtrated to get filtrate II,
Merging filtrate I and filtrate II, obtain filtrate III, cooling；
S5, will in step S4 merge after filtrate III adsorb with 300kg 101 macroporous adsorbent resin after,
Carry out eluting with the ethanol of 65%-75% again, collect eluent；
S6, by step S5 collect eluent be condensed into thick paste A 10-20 part, stay stand-by；
S7, calculate with parts by weight, take the Camellia 50-150 part after sieving in step S1, use milling process
Carry out removing oil；
S8, the Camellia after removing oil in step S7 is transferred to 6m3Multi-functional extractor, adds water boil insulation
0.5-1.2 hour, it is filtrated to get filtrate IV, filtering residue is stayed in multi-functional extractor；
S9, the filtering residue of step S8 is added water boil be incubated 0.5-1.2 hour, be filtrated to get filtrate V, merge
Filtrate IV and filtrate V, obtain filtrate VI, cooling；
S10, by step S9 merge filtrate VI be condensed into thick paste B, merge with the thick paste A of step S6, dense
Shortening density into is 1.10～1.13g/cm3Thick paste 55-90 part；
S11, step S10 gained thick paste is added essence and preservative mix homogeneously, pack and i.e. obtain natural Flos Camelliae Japonicae
Seed hair shampoo article.
Preferably, the de-oiling temperature of step S2 is 30-42 DEG C, and pressure is 15-27KPa, duration 2-3 hour.
Preferably, the parts by weight added water in step S3 are the Camellia parts by weight after sieving in step S2
15 times.
Preferably, the parts by weight added water in step S4 are the Camellia parts by weight after sieving in step S2
10 times.
Preferably, in step S5, ethanol used is 800-950L.
Preferably, the parts by weight added water in step S8 are the Camellia parts by weight after sieving in step S7
15 times.
Preferably, the parts by weight added water in step S9 are the Camellia parts by weight after sieving in step S7
10 times.
Preferably, supercritical CO is used2The weight of the Camellia of extraction removing oil and the mountain of employing milling process removing oil
The weight ratio of camellia oleosa seed is 2:1.
The method have the advantages that
(1) preparation method of the present invention combines supercritical CO2Extraction and conventional press method carry out removing oil, can
Reaching the effect that removing oil is clean, the advantage that can retain again the hair washing of conventional tea bran, therefore, described preparation method is prone to
Prepare foaming abundancy, maintain the hair shampoo article of raw material pure natural character.
(2) supercritical CO is used2Extraction carries out removing oil, can be clean with removing oil, and the beneficially extraction of tea saponin divides
From, solve and effectively do not extract separation owing to the residual oils and fats in tea bran reaches tea saponin to the damage of resin
Problem.
[detailed description of the invention]
It is specifically described below in conjunction with specific embodiment.
Embodiment 1
The preparation method of a kind of natural Camellia hair shampoo article, comprises the following steps:
S1, the Camellia that will shell be dried, pulverize after, cross 32 mesh sieves；
S2, calculate with parts by weight, take the Camellia 100kg after sieving in step S1, use supercritical CO2
Extraction carries out removing oil, and de-oiling temperature is 30 DEG C, and pressure is 15KPa, duration 2 hours；
S3, the Camellia after removing oil in step S2 is transferred to 6m3Multi-functional extractor, adds 1.5m3Water boil
After, it is incubated 0.5 hour, is filtrated to get filtrate I, filtering residue is stayed in multi-functional extractor；
S4, the filtering residue of step S3 is added 1m3After water boil, it is incubated 0.5 hour, is filtrated to get filtrate II, close
And filtrate I and filtrate II, obtain filtrate III, cooling；
S5, will in step S4 merge after filtrate III adsorb with 300kg 101 macroporous adsorbent resin after,
Carry out eluting with the ethanol of 950L 65% again, collect eluent；
S6, by step S5 collect eluent be condensed into thick paste A 10kg, stay stand-by；
S7, calculate with parts by weight, take the Camellia 50kg after sieving in step S1, use milling process to carry out
Removing oil；
S8, the Camellia after removing oil in step S7 is transferred to 6m3Multi-functional extractor, adds 0.75m3Decocting in water
Boiling insulation 0.5 hour, is filtrated to get filtrate IV, is stayed in multi-functional extractor by filtering residue；
S9, the filtering residue of step S8 is added 0.5m3Water boil is incubated 0.5 hour, is filtrated to get filtrate V, merges
Filtrate IV and filtrate V, obtain filtrate VI, cooling；
S10, by step S9 merge filtrate VI be condensed into thick paste B, merge with the thick paste A of step S6, dense
Shortening density into is 1.10g/cm3Thick paste 55kg；
S11, step S10 gained thick paste is added essence and preservative mix homogeneously, pack and i.e. obtain natural Flos Camelliae Japonicae
Seed hair shampoo article.
Embodiment 2
The preparation method of a kind of natural Camellia hair shampoo article, comprises the following steps:
S1, the Camellia that will shell be dried, pulverize after, cross 40 mesh sieves；
S2, calculate with parts by weight, take the Camellia 200kg after sieving in step S1, use supercritical CO2
Extraction carries out removing oil, temperature 40 DEG C, pressure 25KPa, 2.5 hours time；
S3, the Camellia after removing oil in step S2 is transferred to 6m3Multi-functional extractor, adds 3m3After water boil,
It is incubated 1 hour, is filtrated to get filtrate I, filtering residue is stayed in multi-functional extractor；
S4, the filtering residue of step S3 is added 2m3After water boil, it is incubated 1 hour, is filtrated to get filtrate II, merge
Filtrate I and filtrate II, obtain filtrate III, cooling；
S5, will in step S4 merge after filtrate III adsorb with 300kg 101 macroporous adsorbent resin after,
Carry out eluting with the ethanol of 900L 70% again, collect eluent；
S6, by step S5 collect eluent be condensed into thick paste A16kg, stay stand-by；
S7, calculate with parts by weight, take the Camellia 100kg after sieving in step S1, use milling process to enter
Row removing oil；
S8, the Camellia after removing oil in step S7 is transferred to 6m3Multi-functional extractor, adds 1.5m3Water boil
It is incubated 1 hour, is filtrated to get filtrate IV, filtering residue is stayed in multi-functional extractor；
S9, the filtering residue of step S8 is added 1.0m3Water boil is incubated 1 hour, is filtrated to get filtrate V, merges filter
Liquid IV and filtrate V, obtain filtrate VI, cooling；
S10, by step S9 merge filtrate VI be condensed into thick paste B, merge with the thick paste A of step S6, dense
Shortening density into is 1.12g/cm3Thick paste 62kg；
S11, step S10 gained thick paste is added essence and preservative mix homogeneously, pack and i.e. obtain natural Flos Camelliae Japonicae
Seed hair shampoo article.
Embodiment 3
The preparation method of a kind of natural Camellia hair shampoo article, comprises the following steps:
S1, the Camellia that will shell be dried, pulverize after, cross 42 mesh sieves；
S2, calculate with parts by weight, take the Camellia 300kg after sieving in step S1, use supercritical CO2
Extraction carries out removing oil, temperature 42 DEG C, pressure 27KPa, 3 hours time；
S3, the Camellia after removing oil in step S2 is transferred to 6m3Multi-functional extractor, adds 4.5m3Water boil
After, it is incubated 1.2 hours, is filtrated to get filtrate I, filtering residue is stayed in multi-functional extractor；
S4, the filtering residue of step S3 is added 3m3After water boil, it is incubated 1.2 hours, is filtrated to get filtrate II, close
And filtrate I and filtrate II, obtain filtrate III, cooling；
S5, will in step S4 merge after filtrate III adsorb with 300kg 101 macroporous adsorbent resin after,
Carry out eluting with the ethanol of 800L 75% again, collect eluent；
S6, by step S5 collect eluent be condensed into thick paste A 20kg, stay stand-by；
S7, calculate with parts by weight, take the Camellia 150kg after sieving in step S1, use milling process to enter
Row removing oil；
S8, the Camellia after removing oil in step S7 is transferred to 6m3Multi-functional extractor, adds 2.25m3Decocting in water
After boiling, it is incubated 1.2 hours, is filtrated to get filtrate IV, filtering residue is stayed in multi-functional extractor；
S9, the filtering residue of step S8 is added 1.5m3Water boil is incubated 1.2 hours, is filtrated to get filtrate V, merges
Filtrate IV and filtrate V, obtain filtrate VI, cooling；
S10, by step S9 merge filtrate VI be condensed into thick paste B, merge with the thick paste A of step S6, dense
Shortening density into is 1.13g/cm3Thick paste 90kg；
S11, step S10 gained thick paste is added essence and preservative mix homogeneously, pack and i.e. obtain natural Flos Camelliae Japonicae
Seed hair shampoo article.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanation, for skill belonging to the present invention
For the those of ordinary skill in art field, without departing from the inventive concept of the premise, it is also possible to make some letters
Single deduction or replace, all should be considered as belonging to the patent protection model that the present invention is determined by the claims submitted to
Enclose.
Claims (8)
1. the preparation method of a natural Camellia hair shampoo article, it is characterised in that comprise the following steps:
S1, the Camellia that will shell be dried, pulverize after, cross 32-42 mesh sieve；
S2, calculate with parts by weight, take the Camellia 100-300 part after sieving in step S1, use super facing
Boundary CO2Extraction carries out removing oil；
S3, the Camellia after removing oil in step S2 is added water boil after, be incubated 0.5-1.2 hour, filter
To filtrate I, stay filtering residue standby；
S4, the filtering residue of step S3 is added water boil after, be incubated 0.5-1.2 hour, be filtrated to get filtrate II,
Merging filtrate I and filtrate II, obtain filtrate III；
S5, will step S4 merge after filtrate III adsorb with 101 macroporous adsorbent resins after, then use
The ethanol of 65%-75% carries out eluting, collects eluent；
S6, by step S5 collect eluent be condensed into thick paste A 10-20 part, stay stand-by；
S7, calculate with parts by weight, take the Camellia 50-150 part after sieving in step S1, use milling process
Carry out removing oil；
S8, the Camellia after removing oil in step S7 is added water boil be incubated 0.5-1.2 hour, be filtrated to get filter
Liquid IV, stays filtering residue standby；
S9, the filtering residue of step S8 is added water boil be incubated 0.5-1.2 hour, be filtrated to get filtrate V, merge
Filtrate IV and filtrate V, obtain filtrate VI；
S10, by step S9 merge filtrate VI be condensed into thick paste B, merge with the thick paste A of step S6, dense
Shortening density into is 1.10～1.13g/cm3Thick paste 55-90 part；
S11, step S10 gained thick paste is added essence and preservative mix homogeneously, pack and i.e. obtain natural Flos Camelliae Japonicae
Seed hair shampoo article.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
The de-oiling temperature of step S2 is 30-42 DEG C, and pressure is 15-27KPa, duration 2-3 hour.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
The parts by weight added water in step S3 are 15 times of the Camellia parts by weight after sieving in step S2.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
The parts by weight added water in step S4 are 10 times of the Camellia parts by weight after sieving in step S2.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
In step S5, ethanol used is 800-950L.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
The parts by weight added water in step S8 are 15 times of the Camellia parts by weight after sieving in step S7.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
The parts by weight added water in step S9 are 10 times of the Camellia parts by weight after sieving in step S7.
The preparation method of natural Camellia hair shampoo article the most according to claim 1, it is characterised in that
Use supercritical CO2The weight ratio of the Camellia of the weight of the Camellia of extraction removing oil and employing milling process removing oil
For 2:1.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN200994863Y (en) * | 2006-09-18 | 2007-12-26 | 曹维 | Health-care paper pants containing tea-seed essence |
| CN101838302A (en) * | 2010-05-25 | 2010-09-22 | 南昌大学 | Method for extracting sasanquasaponin |
| CN102641387A (en) * | 2012-05-03 | 2012-08-22 | 天津大学 | Method for supercritically extracting natural activity ingredient oil tea polyphenol from oil tea fruits |
| CN102670447A (en) * | 2012-05-22 | 2012-09-19 | 广州市娇兰化妆品有限公司 | Natural plant extract for hair care and preparation method and application thereof |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
| CN104042461A (en) * | 2013-03-12 | 2014-09-17 | 长沙理工大学 | Natural plant shampoo employing camellia seed products as base-material and preparation method thereof |
| CN104072468A (en) * | 2013-03-26 | 2014-10-01 | 宜春元博山茶油科技农业开发有限公司 | Proanthocyanidin extraction process from camellia seed hull |
-
2016
- 2016-05-24 CN CN201610348397.2A patent/CN105853298B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN200994863Y (en) * | 2006-09-18 | 2007-12-26 | 曹维 | Health-care paper pants containing tea-seed essence |
| CN101838302A (en) * | 2010-05-25 | 2010-09-22 | 南昌大学 | Method for extracting sasanquasaponin |
| CN102641387A (en) * | 2012-05-03 | 2012-08-22 | 天津大学 | Method for supercritically extracting natural activity ingredient oil tea polyphenol from oil tea fruits |
| CN102670447A (en) * | 2012-05-22 | 2012-09-19 | 广州市娇兰化妆品有限公司 | Natural plant extract for hair care and preparation method and application thereof |
| CN104042461A (en) * | 2013-03-12 | 2014-09-17 | 长沙理工大学 | Natural plant shampoo employing camellia seed products as base-material and preparation method thereof |
| CN104072468A (en) * | 2013-03-26 | 2014-10-01 | 宜春元博山茶油科技农业开发有限公司 | Proanthocyanidin extraction process from camellia seed hull |
| CN103385831A (en) * | 2013-07-19 | 2013-11-13 | 泉州市新益日用化妆品有限公司 | Novel oil tea shampoo and preparation method thereof |
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