CN105832570A - Hair recombination repair liquid and preparation method thereof - Google Patents
Hair recombination repair liquid and preparation method thereof Download PDFInfo
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- CN105832570A CN105832570A CN201610375574.6A CN201610375574A CN105832570A CN 105832570 A CN105832570 A CN 105832570A CN 201610375574 A CN201610375574 A CN 201610375574A CN 105832570 A CN105832570 A CN 105832570A
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- hair
- repair liquid
- recombination repair
- carboxylic acid
- pyrrolidone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention discloses hair recombination repair liquid. The hair recombination repair liquid comprises 0.04-0.06 wt% of sodium hyaluronate, 4.5-5.5 wt% of glycerin, 2-3 wt% of hydrolyzed keratin, 1.5-2.5 wt% of hydrolyzed collagen, 0.3-1.7 wt% of pyrrolidone carboxylic acid, 0.9-1.1 wt% of sodium lactate, 0.7-0.9 wt% of arginine, 0.5-0.7 wt% of aspartic acid, 0.25-0.35 wt% of pyrrolidone carboxylic acid, 0.18-0.22 wt% of glycine, 0.18-0.22 wt% of alanine, 0.18-0.22 wt% of serine, 0.18-0.22 wt% of valine, 0.18-0.22 wt% of proline, 0.18-0.22 wt% of theronine, 0.18-0.22 wt% of isoleucine, 0.18-0.22 wt% of histidine and the balance of water. The hair recombination repair liquid is good in moisturizing effect and can effectively improve hair coarseness and hair wear resistance. In addition, the invention further provides a p[reparation method of the hair recombination repair liquid.
Description
Technical field
The present invention relates to household chemicals field, particularly a kind of hair recombination repair liquid and preparation method thereof.
Background technology
Chinese patent application CN201210552369.4 discloses a kind of rich in amino acid whose sprayable hair care emulsion, its feature
It is: comprise following components by weight percentage: aminoacid 0.02%～5.0%, volatile silicone oils 10%～30%, poly-two
Methylsiloxane 0.5%～10%, cationic emulsifier 0.05%～0.25%, cation opsonizing agent 0.1%～2.0%, plant
Oil 0.05%～1.0%, sunscreen 0.05～5.0%, preservative 0.1～1.0%, deionized water surplus.Aminoacid is paddy ammonia
A kind of in acid, arginine, serine, cystine, L-hydroxyproline or their mixture；The advantage of this invention is
Sprayable use, hair repairing effect are good, effect long shelf-life rich in amino acid whose hair care emulsion.
But it is poor at moistening effect, to improving hair hairy effect not that the article of everyday use that design hair of the prior art is repaired exists
Significantly problem.
Summary of the invention
It is an object of the invention to provide the energy that a kind of moistening effect is good, it is crude to be effectively improved hair, raising hair is wear-resistant
The hair recombination repair liquid of power, the present invention also provides for the preparation method of above-mentioned hair recombination repair liquid simultaneously.
The technical scheme is that a kind of hair recombination repair liquid, it is characterised in that: include following components:
Hyaluronate sodium 0.04-0.06wt%；
Glycerol 4.5-5.5wt%；
Hydrolysis of keratin matter 2-3wt%；
Hydrolytic collagen 1.5-2.5wt%；
2-pyrrolidone-5-carboxylic acid 1.3-1.7wt%；
Sodium lactate 0.9-1.1wt%；
Arginine 0.7-0.9wt%；
Aspartic acid 0.5-0.7wt%；
2-pyrrolidone-5-carboxylic acid 0.25-0.35wt%；
Glycine 0.18-0.22wt%；
Alanine 0.18-0.22wt%；
Serine 0.18-0.22wt%；
Valine 0.18-0.22wt%；
Proline 0.18-0.22wt%；
Threonine 0.18-0.22wt%；
Isoleucine 0.18-0.22wt%；
Histidine 0.18-0.22wt%；
The water of surplus.
In above-mentioned hair recombination repair liquid, also include preservative 0.08-0.12wt%；Essence 0.08-0.12wt%；Increase
Solvent 0.25-0.35wt%.
In above-mentioned hair recombination repair liquid, described hair recombination repair liquid is composed of the following components:
Hyaluronate sodium 0.05wt%；
Glycerol 5wt%；
Hydrolysis of keratin matter 2.5wt%；
Hydrolytic collagen 2wt%；
2-pyrrolidone-5-carboxylic acid 1.5wt%；
Sodium lactate 1wt%；
Arginine 0.8wt%；
Aspartic acid 0.6wt%；
2-pyrrolidone-5-carboxylic acid 0.3wt%；
Glycine 0.2wt%；
Alanine 0.2wt%；
Serine 0.2wt%；
Valine 0.2wt%；
Proline 0.2wt%；
Threonine 0.2wt%；
Isoleucine 0.2wt%；
Histidine 0.2wt%；
Preservative 0.1wt%；
Essence 0.1wt%；
Solubilizing agent 0.3wt%
The water of surplus.
The invention also discloses the preparation method of above-mentioned hair recombination repair liquid, comprise the following steps:
Step 1: hyaluronate sodium and glycerol being stirring evenly and then adding in deionized water, stirring and dissolving is complete.
Step 2: be sequentially added into hydrolytic collagen, hydrolysis of keratin, Anjidew NL50, sodium lactate, arginine, aspartic acid, pyrrole
Pyrrolidone carboxylic acid, glycine, alanine, serine, valine, proline, threonine, isoleucine, histidine,
Stir.
5, the preparation method of hair recombination repair liquid according to claim 4, it is characterised in that: in step 2 also
Add preservative, and also include step 3 after step 2 terminates；
Step 3: add essence and solubilizing agent, stir.
Beneficial effects of the present invention is as follows:
The present invention uses glycerol, up to about ten kinds aminoacid and salt combination thereof, can be effectively to hair moisturizing, in moisturizing
The opposing lesion capability of hair, particularly corresponding dye can be comprehensively improved in combination with hydrolysis of keratin matter, hydrolytic collagen
The resistivity having a perm improves notable.
Detailed description of the invention
Below in conjunction with detailed description of the invention, technical scheme is described in further detail, but does not constitute this
Bright any restriction.
Specific embodiment 1:
The preparation method of a kind of hair recombination repair liquid, comprises the following steps:
Step 1: hyaluronate sodium and glycerol being stirring evenly and then adding in deionized water, stirring and dissolving is complete.
Step 2: be sequentially added into hydrolytic collagen, hydrolysis of keratin, Anjidew NL50, sodium lactate, arginine, aspartic acid, pyrrole
Pyrrolidone carboxylic acid, glycine, alanine, serine, valine, proline, threonine, isoleucine, histidine,
Methylisothiazolinone stirs；
Step 3: addition essence and solubilizing agent nonyl phenol, according to ether-14, stir.
Above-mentioned each component is as follows:
Hyaluronate sodium 0.05wt%；
Glycerol 5wt%；
Hydrolysis of keratin matter 2.5wt%；
Hydrolytic collagen 2wt%；
2-pyrrolidone-5-carboxylic acid 1.5wt%；
Sodium lactate 1wt%；
Arginine 0.8wt%；
Aspartic acid 0.6wt%；
2-pyrrolidone-5-carboxylic acid 0.3wt%；
Glycine 0.2wt%；
Alanine 0.2wt%；
Serine 0.2wt%；
Valine 0.2wt%；
Proline 0.2wt%；
Threonine 0.2wt%；
Isoleucine 0.2wt%；
Histidine 0.2wt%；
Methylisothiazolinone 0.1wt%；
Essence 0.1wt%；
Nonyl phenol is according to ether-140.3wt%
The water of surplus.
Specific embodiment 2
The preparation method of a kind of hair recombination repair liquid, comprises the following steps:
Step 1: hyaluronate sodium and glycerol being stirring evenly and then adding in deionized water, stirring and dissolving is complete.
Step 2: be sequentially added into hydrolytic collagen, hydrolysis of keratin, Anjidew NL50, sodium lactate, arginine, aspartic acid, pyrrole
Pyrrolidone carboxylic acid, glycine, alanine, serine, valine, proline, threonine, isoleucine, histidine,
Methylisothiazolinone stirs；
Step 3: addition essence and solubilizing agent nonyl phenol, according to ether-14, stir.
Above-mentioned each component is as follows:
Hyaluronate sodium 0.04wt%；
Glycerol 4.5wt%；
Hydrolysis of keratin matter 3wt%；
Hydrolytic collagen 1.5wt%；
2-pyrrolidone-5-carboxylic acid 1.7wt%；
Sodium lactate 0.9wt%；
Arginine 0.9wt%；
Aspartic acid 0.5wt%；
2-pyrrolidone-5-carboxylic acid 0.35wt%；
Glycine 0.18wt%；
Alanine 0.22wt%；
Serine 0.18wt%；
Valine 0.22wt%；
Proline 0.18wt%；
Threonine 0.22wt%；
Isoleucine 0.18wt%；
Histidine 0.22wt%；
Methylisothiazolinone 0.08wt%；
Essence 0.12wt%；
Nonyl phenol is according to ether-140.25wt%
The water of surplus.
Specific embodiment 3
The preparation method of a kind of hair recombination repair liquid, comprises the following steps:
Step 1: hyaluronate sodium and glycerol being stirring evenly and then adding in deionized water, stirring and dissolving is complete.
Step 2: be sequentially added into hydrolytic collagen, hydrolysis of keratin, Anjidew NL50, sodium lactate, arginine, aspartic acid, pyrrole
Pyrrolidone carboxylic acid, glycine, alanine, serine, valine, proline, threonine, isoleucine, histidine,
Methylisothiazolinone stirs；
Step 3: addition essence and solubilizing agent nonyl phenol, according to ether-14, stir.
Above-mentioned each component is as follows:
Hyaluronate sodium 0.06wt%；
Glycerol 5.5wt%；
Hydrolysis of keratin matter 2wt%；
Hydrolytic collagen 2.5wt%；
2-pyrrolidone-5-carboxylic acid 1.3wt%；
Sodium lactate 1.1wt%；
Arginine 0.7wt%；
Aspartic acid 0.7wt%；
2-pyrrolidone-5-carboxylic acid 0.25wt%；
Glycine 0.22wt%；
Alanine 0.18wt%；
Serine 0.22wt%；
Valine 0.18wt%；
Proline 0.22wt%；
Threonine 0.18wt%；
Isoleucine 0.22wt%；
Histidine 0.18wt%；
Methylisothiazolinone 0.12wt%；
Essence 0.08wt%；
Nonyl phenol is according to ether-140.35wt%
The water of surplus.
Performance test
(1) taking Aisan's hair, a length of 10cm, 10 is one group, totally 16 groups.The each group hair chosen is divided
Do not wash with the sodium dodecyl sulfate solution 2g of mass concentration 3%, and each group of hair is carried out machinery rubbing 5 minutes, so
After examine under a microscope each group of hair surface hair scale sheet cellularity destroy situation and count, labelling.
(2) above-mentioned each group of hair is soaked in the keratin with different molecular weight respectively (according to retaining relative molecular weight not
With changing the dialysis bag of different size, prepare gained according to the method for embodiment 6) prepared by method as described in embodiment 10
In shampoo, and constantly stir, respectively 5 minutes, 10 minutes, 15 minutes, take out after 20 minutes, rinse with clear water
3 times, each 1 minute, the most naturally dry.
(3) each group hair after drying is examined under a microscope respectively, and in counting step (1), mark hair surface is subject to
Damage hair scale sheet cellularity repair situation and calculate repair rate: repair rate=reparation hair scale sheet total cellular score * 100%/impaired hair scale
Sheet total cellular score；
Test result is as follows: the repair rate of embodiment 1,2,3 is respectively 86%；88%；88%.
The above-described presently preferred embodiments of the present invention that is only, all made in the range of the spirit and principles in the present invention any repair
Change, equivalent and improvement etc., should be included within the scope of the present invention.
Claims (5)
1. a hair recombination repair liquid, it is characterised in that: include following components:
Hyaluronate sodium 0.04-0.06wt%；
Glycerol 4.5-5.5wt%；
Hydrolysis of keratin matter 2-3wt%；
Hydrolytic collagen 1.5-2.5wt%；
2-pyrrolidone-5-carboxylic acid 1.3-1.7wt%；
Sodium lactate 0.9-1.1wt%；
Arginine 0.7-0.9wt%；
Aspartic acid 0.5-0.7wt%；
2-pyrrolidone-5-carboxylic acid 0.25-0.35wt%；
Glycine 0.18-0.22wt%；
Alanine 0.18-0.22wt%；
Serine 0.18-0.22wt%；
Valine 0.18-0.22wt%；
Proline 0.18-0.22wt%；
Threonine 0.18-0.22wt%；
Isoleucine 0.18-0.22wt%；
Histidine 0.18-0.22wt%；
The water of surplus.
Hair recombination repair liquid the most according to claim 1, it is characterised in that: also include preservative 0.08-0.12wt%；
Essence 0.08-0.12wt%；Solubilizing agent 0.25-0.35wt%.
Hair recombination repair liquid the most according to claim 2, it is characterised in that: described hair recombination repair liquid by
Following components forms:
Hyaluronate sodium 0.05wt%；
Glycerol 5wt%；
Hydrolysis of keratin matter 2.5wt%；
Hydrolytic collagen 2wt%；
2-pyrrolidone-5-carboxylic acid 1.5wt%；
Sodium lactate 1wt%；
Arginine 0.8wt%；
Aspartic acid 0.6wt%；
2-pyrrolidone-5-carboxylic acid 0.3wt%；
Glycine 0.2wt%；
Alanine 0.2wt%；
Serine 0.2wt%；
Valine 0.2wt%；
Proline 0.2wt%；
Threonine 0.2wt%；
Isoleucine 0.2wt%；
Histidine 0.2wt%；
Preservative 0.1wt%；
Essence 0.1wt%；
Solubilizing agent 0.3wt%
The water of surplus.
4. the preparation method of the hair recombination repair liquid as described in claim 1-3 is arbitrary, it is characterised in that: include
Following steps:
Step 1: hyaluronate sodium and glycerol being stirring evenly and then adding in deionized water, stirring and dissolving is complete.
Step 2: be sequentially added into hydrolytic collagen, hydrolysis of keratin, Anjidew NL50, sodium lactate, arginine, aspartic acid, pyrrole
Pyrrolidone carboxylic acid, glycine, alanine, serine, valine, proline, threonine, isoleucine, histidine,
Stir.
The preparation method of hair recombination repair liquid the most according to claim 4, it is characterised in that: in step 2 also
Add preservative, and also include step 3 after step 2 terminates；
Step 3: add essence and solubilizing agent, stir.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610375574.6A CN105832570A (en) | 2016-05-30 | 2016-05-30 | Hair recombination repair liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610375574.6A CN105832570A (en) | 2016-05-30 | 2016-05-30 | Hair recombination repair liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105832570A true CN105832570A (en) | 2016-08-10 |
Family
ID=56595977
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610375574.6A Pending CN105832570A (en) | 2016-05-30 | 2016-05-30 | Hair recombination repair liquid and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112263500A (en) * | 2020-10-28 | 2021-01-26 | 齐鲁工业大学 | Biological hair care repair liquid prepared by compounding TG enzyme with keratin/amino acid |
| CN112426378A (en) * | 2020-12-03 | 2021-03-02 | 广州环亚化妆品科技有限公司 | Moisturizing and repairing composition and application thereof |
| WO2021037322A1 (en) | 2019-08-27 | 2021-03-04 | Portillo Rosado Rosa Maria | Composition for delaying and dyeing grey hair |
| CN114795990A (en) * | 2022-05-10 | 2022-07-29 | 广州千羽化妆品有限公司 | Mild shampoo for controlling water-oil balance and preparation method thereof |
| CN116196247A (en) * | 2023-03-16 | 2023-06-02 | 浙江章光101有限公司 | Rosa roxburghii amino acid hair care essence |
-
2016
- 2016-05-30 CN CN201610375574.6A patent/CN105832570A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021037322A1 (en) | 2019-08-27 | 2021-03-04 | Portillo Rosado Rosa Maria | Composition for delaying and dyeing grey hair |
| EP4035737A1 (en) | 2019-08-27 | 2022-08-03 | Portillo Rosado, Rosa Maria | Composition for delaying and dyeing grey hair |
| CN112263500A (en) * | 2020-10-28 | 2021-01-26 | 齐鲁工业大学 | Biological hair care repair liquid prepared by compounding TG enzyme with keratin/amino acid |
| CN112263500B (en) * | 2020-10-28 | 2022-11-15 | 齐鲁工业大学 | Biological hair care repair liquid prepared by compounding TG enzyme with keratin/amino acid |
| CN112426378A (en) * | 2020-12-03 | 2021-03-02 | 广州环亚化妆品科技有限公司 | Moisturizing and repairing composition and application thereof |
| CN112426378B (en) * | 2020-12-03 | 2023-01-13 | 广州环亚化妆品科技股份有限公司 | Moisturizing and repairing composition and application thereof |
| CN114795990A (en) * | 2022-05-10 | 2022-07-29 | 广州千羽化妆品有限公司 | Mild shampoo for controlling water-oil balance and preparation method thereof |
| CN114795990B (en) * | 2022-05-10 | 2022-12-30 | 广州千羽化妆品有限公司 | Mild shampoo for controlling water-oil balance and preparation method thereof |
| CN116196247A (en) * | 2023-03-16 | 2023-06-02 | 浙江章光101有限公司 | Rosa roxburghii amino acid hair care essence |
| CN116196247B (en) * | 2023-03-16 | 2023-08-29 | 浙江章光101有限公司 | Rosa roxburghii amino acid hair care essence |
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Application publication date: 20160810 |