CN105820865A - Metal cutting fluid and preparation method thereof - Google Patents

Metal cutting fluid and preparation method thereof Download PDF

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Publication number
CN105820865A
CN105820865A CN201610184649.2A CN201610184649A CN105820865A CN 105820865 A CN105820865 A CN 105820865A CN 201610184649 A CN201610184649 A CN 201610184649A CN 105820865 A CN105820865 A CN 105820865A
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China
Prior art keywords
parts
sodium
metalworking fluid
tetrachloroethylene
polyaniline
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CN201610184649.2A
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Chinese (zh)
Inventor
刘通
苑建涛
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Chongqing Golute New Material Technology Co Ltd
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Chongqing Golute New Material Technology Co Ltd
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Priority to CN201610184649.2A priority Critical patent/CN105820865A/en
Publication of CN105820865A publication Critical patent/CN105820865A/en
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00Lubricating compositions containing more than 10% water
    • C10M173/02Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/02Water
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/084Inorganic acids or salts thereof containing sulfur, selenium or tellurium
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087Boron oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02Hydroxy compounds
    • C10M2207/023Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/14Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/141Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings monocarboxylic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/02Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
    • C10M2211/022Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only aliphatic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/04Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2217/046Polyamines, i.e. macromoleculars obtained by condensation of more than eleven amine monomers
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • C10N2010/02Groups 1 or 11
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16Antiseptic; (micro) biocidal or bactericidal
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64Environmental friendly compositions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/22Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention relates to metal cutting fluid and a preparation method thereof.The metal cutting fluid is prepared from, by weight, 6-13 parts of tetramethylammonium hydroxide, 2-5 parts of polyaniline, 1-20 parts of polyethylene glycol, 1-40 parts of tetrachloroethylene, 5-20 parts of sodium tetraborate, 1-13 parts of sodium benzoate, 4-8 parts of sodium thiosulfate, 3-9 parts of dodecylphenol, 2-30 parts of ethylene triamine and 30-50 parts of water.The metal cutting fluid has good corrosion and rust resistance, energy saving and environment friendliness, high pressure resistance and excellent lubricating and antiwear performance and is suitable for multiple materials, cutting tumors can be avoided, and tools are effectively protected.

Description

A kind of metalworking fluid and preparation method thereof
Technical field
The present invention relates to a kind of metalworking fluid and preparation method thereof, belong to Metal Cutting manufacture field.
Background technology
Metalworking fluid has considerable effect in metal cutting, Grinding Process.It is at machine Tool processing to be applied extremely wide. cutting fluid should possess the effect of following several respects:
Cooling effect: in workpiece cutting process, can reduce the temperature of cutting region in time and rapidly, I.e. reduce temperature rise, the cooling generally caused because rubbing and also affect stock-removing efficiency, cutting quality and cutter life.
Lubrication: can reduce and rub between cutting tool and workpiece.Lubricating fluid can infiltrate to cutter and workpiece And between chip, reduce friction and bonding, reduce cutting resistance, it is ensured that cutting quality, extend cutter Life-span.
Cleaning function: make chip or abrasive particle be rinsed and leave the processing district of cutter and workpiece, in case They mutually bond and stick to hinder on workpiece, cutter and lathe.
Rust inhibition: have certain rustless property, prevents workpiece and lathe from getting rusty.As improved rustless property, Also can partly replace rust prevention during manufacture.
At present, domestic main use cutting fluid based on Dormant oils, vegetable oil, due to these oils Exist so that cutting fluid is easy to corrupt smelly, thus the cycle of use is the shortest, and exhaust emission is big, meanwhile, Aforesaid liquid antirust agent uses sodium nitrite more, although sodium nitrite rust-preventing characteristic is good, but has one Significantly weakness: one is to be irritating to the skin effect, is easily caused skin allergy after worker exposure;Two is sub- Amine in the amine of sodium nitrate and human body or cutting fluid reacts generation high carcinogenic material inferior ammonium nitrate.Use this A little cutting fluids, not only to consume substantial amounts of Dormant oils, vegetable oil, and also result in the pollution to environment.
Summary of the invention
The technical problem to be solved is to provide a kind of metalworking fluid and preparation method thereof, capital Belonging to cutting fluid and have good antiseptic and rustproof property, energy-conserving and environment-protective, higher resistance to pressure, excellent lubrication resists Mill performance, can avoid the generation of BUE, be effectively protected cutter, it is adaptable to various material.
The technical scheme is that a kind of metalworking fluid, by weighing as follows The raw material composition of amount part:
Tetramethylammonium hydroxide 6-13 part, polyaniline 2-5 part, Polyethylene Glycol 1-20 part, tetrachloroethylene 1-40 part, sodium tetraborate 5-20 part, sodium benzoate 1-13 part, sodium thiosulfate 4-8 part, dodecane Base phenol 3-9 part, second triamine 2-30 part, water 30-50 part.
On the basis of technique scheme, the present invention can also do following improvement.
Further, described metalworking fluid, it is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 12 parts, tetrachloroethylene 22 parts, Sodium tetraborate 13 parts, sodium benzoate 11 parts, 6 parts of sodium thiosulfate, dodecylphenol 7 parts, second three Amine 20 parts, 50 parts of water.
Further, described metalworking fluid, it is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 6 parts, polyaniline 5 parts, Polyethylene Glycol 17 parts, tetrachloroethylene 20 parts, Sodium tetraborate 17 parts, sodium benzoate 12 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 10 parts, 40 parts of water.
Further, described metalworking fluid, it is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 18 parts, tetrachloroethylene 20 parts, Sodium tetraborate 10 parts, sodium benzoate 13 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 16 parts, 30 parts of water.
The present invention also provides for the preparation method of a kind of metalworking fluid, including:
1) sodium benzoate, sodium thiosulfate and sodium tetraborate being mixed, 45-65 DEG C of insulated and stirred 5-10 is divided Clock;
2) Polyethylene Glycol is added to the water, 400-1000 rev/min of dispersed with stirring 4-5 minute;
3) by 1) and 2) process after each raw material mixing, be stirring evenly and then adding into Tetramethylammonium hydroxide, Polyaniline and tetrachloroethylene, 50-75 DEG C of insulated and stirred 10-50 minute, obtain mixture;
4) to 3) mixture that obtains adds dodecylphenol and second triamine, 300-1000 rev/min is stirred Mix dispersion 30-40 minute, obtain described metalworking fluid.
The invention has the beneficial effects as follows:
The metalworking fluid that the present invention provides can cool down, environmentally safe or pollution abatement, and There is good antiseptic and rustproof property, energy-conserving and environment-protective, higher resistance to pressure, excellent lubrication abrasion resistance, The generation of BUE can be avoided, be effectively protected cutter, it is adaptable to various material.This preparation method Simple, can be mass-produced.
Detailed description of the invention
Principle and feature to the present invention are described below, and example is served only for explaining the present invention, and Non-for limiting the scope of the present invention.
Embodiment 1
Described metalworking fluid, is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 12 parts, tetrachloroethylene 22 parts, Sodium tetraborate 13 parts, sodium benzoate 11 parts, 6 parts of sodium thiosulfate, dodecylphenol 7 parts, second three Amine 20 parts, 50 parts of water.
Preparation method is as follows:
1) sodium benzoate, sodium thiosulfate and sodium tetraborate are mixed, 45 DEG C of insulated and stirred 6 minutes;
2) Polyethylene Glycol is added to the water, 700 revs/min of dispersed with stirring 5 minutes;
3) by 1) and 2) process after each raw material mixing, be stirring evenly and then adding into Tetramethylammonium hydroxide, Polyaniline and tetrachloroethylene, at 75 DEG C, insulated and stirred 40 minutes, obtain mixture;
4) to 3) mixture that obtains adds dodecylphenol and second triamine, 600 revs/min of stirrings point Dissipate 40 minutes, obtain described metalworking fluid.
Embodiment 2
Described metalworking fluid, is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 6 parts, polyaniline 5 parts, Polyethylene Glycol 17 parts, tetrachloroethylene 20 parts, Sodium tetraborate 17 parts, sodium benzoate 12 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 10 parts, 40 parts of water.
1) sodium benzoate, sodium thiosulfate and sodium tetraborate are mixed, 65 DEG C of insulated and stirred 10 minutes;
2) Polyethylene Glycol is added to the water, 1000 revs/min of dispersed with stirring 4 minutes;
3) by 1) and 2) process after each raw material mixing, be stirring evenly and then adding into Tetramethylammonium hydroxide, Polyaniline and tetrachloroethylene, at 75 DEG C, insulated and stirred 30 minutes, obtain mixture;
4) to 3) mixture that obtains adds dodecylphenol and second triamine, 600 revs/min of stirrings point Dissipate 35 minutes, obtain described metalworking fluid.
Embodiment 3
Described metalworking fluid, is made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 18 parts, tetrachloroethylene 20 parts, Sodium tetraborate 10 parts, sodium benzoate 13 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 16 parts, 30 parts of water.
1) sodium benzoate, sodium thiosulfate and sodium tetraborate are mixed, 65 DEG C of insulated and stirred 7 minutes;
2) Polyethylene Glycol is added to the water, 1000 revs/min of dispersed with stirring 5 minutes;
3) by 1) and 2) process after each raw material mixing, be stirring evenly and then adding into Tetramethylammonium hydroxide, Polyaniline and tetrachloroethylene, at 65 DEG C, insulated and stirred 50 minutes, obtain mixture;
4) to 3) mixture that obtains adds dodecylphenol and second triamine, 1000 revs/min of stirrings point Dissipate 40 minutes, obtain described metalworking fluid.
Metalworking fluid prepared by detection embodiment 1-3, result is as shown in table 1:
Emulsion stability experiment (15-30 DEG C, 24h) of 5%: do not analyse oil, not graining;
Rust-preventing characteristic experiment (35 ± 2 DEG C, one-level casting pig monolithic 24h) >=76h, without rust staining;
Rust-preventing characteristic experiment (35 ± 2 DEG C, one-level casting pig lamination 8h) >=29h, without rust staining;
Rust-preventing characteristic experiment (35 ± 2 DEG C, iron and steel monolithic 24h) >=78h, without rust staining;
Rust-preventing characteristic experiment (35 ± 2 DEG C, iron and steel lamination 8h) >=30h, without rust staining;
Corrosion experiment (55 ± 2 DEG C, cast iron 24h) >=78h;
Corrosion experiment (55 ± 2 DEG C, red copper 8h) >=32h;
To lathe paint compatibility test: non-foaming, do not ftracture, the most tacky.
Table 1
Workpiece is processed by metalworking fluid respectively that use embodiment of the present invention 1-3 to prepare, experiment knot Fruit shows: the workpiece processed is changed without through 90 days non-corrosives of sea water immersion, cutting production line for 150 days Tank liquor is without rancid.
Four-ball tester method is used to survey the maximum nonseizure load value of the metalworking fluid that embodiment 1-3 obtains, knot Fruit is as shown in table 2.
Table 2
Project Embodiment 1 Embodiment 2 Embodiment 3
Maximum nonseizure load value (kg) 75kg 74.5kg 73.5kg
As shown in Table 2, the maximum nonseizure load value of the metalworking fluid that prepared by embodiment of the present invention 1-3 It is all higher than 73.5kg, illustrates that metalworking fluid prepared by the present invention is except having good anti-corrosion and mildew-resistant Outside degeneration energy, also there is good lubricity and resistance to extreme pressure.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all in the present invention Spirit and principle within, any modification, equivalent substitution and improvement etc. made, should be included in this Within bright protection domain.

Claims (5)

1. a metalworking fluid, it is characterised in that be made up of the raw material of following weight portion:
Tetramethylammonium hydroxide 6-13 part, polyaniline 2-5 part, Polyethylene Glycol 1-20 part, tetrachloroethylene 1-40 part, sodium tetraborate 5-20 part, sodium benzoate 1-13 part, sodium thiosulfate 4-8 part, dodecane Base phenol 3-9 part, second triamine 2-30 part, water 30-50 part.
Metalworking fluid the most according to claim 1, it is characterised in that by following weight portion Raw material forms:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 12 parts, tetrachloroethylene 22 parts, Sodium tetraborate 13 parts, sodium benzoate 11 parts, 6 parts of sodium thiosulfate, dodecylphenol 7 parts, second three Amine 20 parts, 50 parts of water.
Metalworking fluid the most according to claim 1, it is characterised in that by following weight portion Raw material forms:
Tetramethylammonium hydroxide 6 parts, polyaniline 5 parts, Polyethylene Glycol 17 parts, tetrachloroethylene 20 parts, Sodium tetraborate 17 parts, sodium benzoate 12 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 10 parts, 40 parts of water.
Metalworking fluid the most according to claim 1, it is characterised in that by following weight portion Raw material forms:
Tetramethylammonium hydroxide 13 parts, polyaniline 4 parts, Polyethylene Glycol 18 parts, tetrachloroethylene 20 parts, Sodium tetraborate 10 parts, sodium benzoate 13 parts, 8 parts of sodium thiosulfate, dodecylphenol 9 parts, second three Amine 16 parts, 30 parts of water.
5. a preparation method for the metalworking fluid as described in claim 1-4 is arbitrary, its feature exists In, including:
1) sodium benzoate, sodium thiosulfate and sodium tetraborate are mixed, 45-65 DEG C of insulated and stirred 5-10 Minute;
2) Polyethylene Glycol is added to the water, 400-1000 rev/min of dispersed with stirring 4-5 minute;
3) by 1) and 2) process after each raw material mixing, be stirring evenly and then adding into Tetramethylammonium hydroxide, Polyaniline and tetrachloroethylene, 50-75 DEG C of insulated and stirred 10-50 minute, obtain mixture;
4) to 3) mixture that obtains adds dodecylphenol and second triamine, 300-1000 rev/min is stirred Mix dispersion 30-40 minute, obtain described metalworking fluid.
CN201610184649.2A 2016-03-28 2016-03-28 Metal cutting fluid and preparation method thereof Pending CN105820865A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004339303A (en) * 2003-05-14 2004-12-02 Nikkintoo:Kk Water-soluble lubricating oil
CN103897792A (en) * 2013-11-06 2014-07-02 东南大学 Raw material and method for preparing water-based cutting fluid
CN104046470A (en) * 2014-06-27 2014-09-17 青岛扎西生物科技有限公司 Novel anticorrosion cutting fluid
CN104059756A (en) * 2014-06-27 2014-09-24 青岛极致节能环保有限公司 Improved cutting liquid
CN105296130A (en) * 2015-11-19 2016-02-03 苏州捷德瑞精密机械有限公司 Antirust aqueous cutting fluid and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004339303A (en) * 2003-05-14 2004-12-02 Nikkintoo:Kk Water-soluble lubricating oil
CN103897792A (en) * 2013-11-06 2014-07-02 东南大学 Raw material and method for preparing water-based cutting fluid
CN104046470A (en) * 2014-06-27 2014-09-17 青岛扎西生物科技有限公司 Novel anticorrosion cutting fluid
CN104059756A (en) * 2014-06-27 2014-09-24 青岛极致节能环保有限公司 Improved cutting liquid
CN105296130A (en) * 2015-11-19 2016-02-03 苏州捷德瑞精密机械有限公司 Antirust aqueous cutting fluid and preparation method thereof

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