CN105802395A - Water-based, environment-friendly, sound-absorbing, noise-reducing, high-elasticity and waterproof emulsion and preparation method thereof - Google Patents

Water-based, environment-friendly, sound-absorbing, noise-reducing, high-elasticity and waterproof emulsion and preparation method thereof Download PDF

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Publication number
CN105802395A
CN105802395A CN201610211958.4A CN201610211958A CN105802395A CN 105802395 A CN105802395 A CN 105802395A CN 201610211958 A CN201610211958 A CN 201610211958A CN 105802395 A CN105802395 A CN 105802395A
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China
Prior art keywords
emulsion
parts
aqueous
sound
absorbing sound
Prior art date
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Pending
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CN201610211958.4A
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Chinese (zh)
Inventor
钟圣福
黄志强
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HEXIN WATERPROOF AND DECORATION MATERIAL Co Ltd
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HEXIN WATERPROOF AND DECORATION MATERIAL Co Ltd
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Priority to CN201610211958.4A priority Critical patent/CN105802395A/en
Publication of CN105802395A publication Critical patent/CN105802395A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D131/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
    • C09D131/02Homopolymers or copolymers of esters of monocarboxylic acids
    • C09D131/04Homopolymers or copolymers of vinyl acetate
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/70Additives characterised by shape, e.g. fibres, flakes or microspheres

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a water-based, environment-friendly, sound-absorbing, noise-reducing, high-elasticity and waterproof emulsion and a preparation method thereof. The emulsion is prepared from following raw materials in parts by weight through even mixing and full stirring: 250-450 parts of nano-composite latex, 0.2-2 parts of propylene glycol, 100-200 parts of inorganic filler, 100-300 parts of lightweight inorganic sound-absorbing fibers, 3-8 parts of a dispersing agent, 0.3-3 parts of a defoaming agent, 0.5-3 parts of a thickening agent, 15-20 parts of a coalescing agent, 2-4 parts of a bactericide and 160-240 parts of water. The lightweight inorganic sound-absorbing fibers are added to the waterproof emulsion, and a film has the characteristics of sound absorption, noise reduction, sound insulation, fire prevention, insect prevention, mold prevention and the like after being formed by the emulsion; organic solvent volatilization is avoided during construction, construction is safe, the environment-friendly performance is good, and the film is high in tensile strength, ageing resistance and chemical resistance and has the good mechanical performance after being formed by the emulsion; different inorganic fiber ratios can also be adjusted according to market demands in actual production, and products meeting different market demands are prepared.

Description

A kind of aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion and preparation method thereof
Technical field
The present invention relates to water-proof emulsion, specifically a kind of aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion and preparation method thereof.
Background technology
Water-proof emulsion kind for building surface is a lot of in the market, function singleness, quality is uneven, what have contains formaldehyde, the harmful substances such as benzene, this water-proof emulsion is used can human body and domestic environment to be harmful to, though some water-proof emulsions do not have noxious substance, but there is poor water resistance, adhesive force is not strong, the shortcomings such as easy foaming comes off, do not reach the effect of waterproof, although water-proofing treatment is carried out on some building surfaces, but additionally must do absorbing sound and lowering noise again to process according to customer demand, no small economy and material damage is brought to owner or enterprise, also bring many troubles to client simultaneously.
Summary of the invention
It is an object of the invention to for the deficiencies in the prior art, it is provided that one is nontoxic, resistance to water strong, be not easy foaming comes off, and can realize the high-elastic waterproof emulsion of absorbing sound and lowering noise.
A kind of aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion of the present invention, by the following raw material counted by weight ratio by evenly mixing, be sufficiently stirred for and make:
Nano-composite emulsion 250~450, propylene glycol 0.2~2, inorganic filler 100~200, light-weight inorganic acoutic fibre board 100~300, dispersant 3~8, defoamer 0.3~3, thickening agent 0.5~3, coalescents 15~20, antibacterial 2~4, water 160~240.
Wherein, described in:
Nano-composite emulsion is the weight ratio of the mixture of polyvinyl acetate and pure-acrylic emulsion, polyvinyl acetate and pure-acrylic emulsion is 1:1;
Inorganic filler is a kind of in titanium dioxide and precipitated calcium carbonate or both mixture, and the weight ratio of titanium dioxide and precipitated calcium carbonate is 1:1;
Light-weight inorganic acoutic fibre board is that a kind of high-efficiency sound-absorbing noise reduction sound insulation made after special process processes sprays formula material, for prior art;
Dispersant is the one in dispersant 8045,5040;
Defoamer is defoamer N × 2;
Thickening agent is thickening agent XJ-AT702;
Coalescents is coalescents TEXANOL;
Antibacterial is coating emulsion bactericidal liquid;
Water is the clear water after common filtration.
The preparation method that it is a further object to provide above-mentioned aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, this preparation method comprises the steps:
(1) propylene glycol, inorganic filler, water, coalescents, light-weight inorganic acoutic fibre board, dispersant, defoamer and thickening agent are added in agitator tank by weight ratio, with rotating speed 250~350r/min mixing and stirring;
(2) rotating speed is adjusted to 4500~5000r/min on Multi-functional dispersion machine, stirs 3.5~4.5 hours, by high speed shear, mixture is uniformly dispersed;
(3) rotating speed is adjusted to 350~450r/min, is slowly added to nano-composite emulsion;
(4) add antibacterial, be kept stirring for 1.5~2.5h;
(5) gauze filters, tinning packaging.
Products obtained therefrom is after testing: after film forming, acoustic absorptivity is more than 25%, and elongation percentage is 480%, and hot strength is 2.8Mpa.
Water-proof emulsion of the present invention:
1. add light-weight inorganic acoutic fibre board, there is after emulsion film forming the features such as absorbing sound and lowering noise, sound insulation, fire prevention, insect protected, mildew-resistant;
2. organic solvent-free volatilization, construction safety when construction, the feature of environmental protection is good, and emulsion film forming after-drawing degree is high, and resistance to ag(e)ing, chemical resistance are strong, have good mechanical performance;
3. in actual production, also according to the market demand, different inorfil ratios can be adjusted, make the product adapting to market difference demand.
Detailed description of the invention
The present invention is further elaborated by the examples below, but is not limiting the scope of the present invention.
Embodiment 1:
Configuration 1000kg aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, its proportioning raw materials (kg) is:
Nano-composite emulsion 260
Propylene glycol 2
Titanium dioxide 200
Light-weight inorganic acoutic fibre board 300
Dispersant 80458
Defoamer N × 23
Thickening agent XJ-AT7023
Coalescents TEXANOL20
Antibacterial 4
Water 200;
Wherein:
Nano-composite emulsion is polyvinyl acetate and pure-acrylic emulsion is made by the weight ratio mix homogeneously of 1:1;
Light-weight inorganic acoutic fibre board is process, through chemical mixing sludging process, a kind of high-efficiency sound-absorbing noise reduction sound insulation made to spray formula material;
Preparation method comprises the steps:
(1) propylene glycol, titanium dioxide, water, coalescents TEXANOL, light-weight inorganic acoutic fibre board, dispersant 8045, defoamer N × 2 and thickening agent XJ-AT702 are added in agitator tank by proportioning, with rotating speed 300r/min mixing and stirring;
(2) rotating speed is adjusted to 5000r/min on Multi-functional dispersion machine, stirs 4 hours, by high speed shear, mixture is uniformly dispersed;
(3) rotating speed is adjusted to 400r/min, is slowly added to nano-composite emulsion;
(4) add antibacterial, be kept stirring for 2h;
(5) gauze filters, tinning packaging.
Embodiment 2:
Configuration 800kg aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, its proportioning raw materials (kg) is:
Nano-composite emulsion 250
Propylene glycol 1.5
Precipitated calcium carbonate 100
Light-weight inorganic acoutic fibre board 220
Dispersant 50406
Defoamer N × 22.5
Thickening agent XJ-AT7022
Coalescents TEXANOL15
Antibacterial 3
Water 200;
Preparation method comprises the steps:
(1) propylene glycol, precipitated calcium carbonate, water, coalescents TEXANOL, light-weight inorganic acoutic fibre board, dispersant 5040, defoamer N × 2 and thickening agent XJ-AT702 are added in agitator tank by proportioning, with rotating speed 300r/min mixing and stirring;
(2) rotating speed is adjusted to 5000r/min on Multi-functional dispersion machine, stirs 4 hours, by high speed shear, mixture is uniformly dispersed;
(3) rotating speed is adjusted to 400r/min, is slowly added to nano-composite emulsion;
(4) add antibacterial, be kept stirring for 2h;
(5) gauze filters, tinning packaging.
Embodiment 3:
Configuration 1000kg aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, its proportioning raw materials (kg) is:
Nano-composite emulsion 260
Propylene glycol 2
Titanium dioxide 100
Precipitated calcium carbonate 100
Light-weight inorganic acoutic fibre board 300
Dispersant 80458
Defoamer N × 23
Thickening agent XJ-AT7023
Coalescents TEXANOL20
Antibacterial 4
Water 200;
Preparation method comprises the steps:
(1) propylene glycol, titanium dioxide, precipitated calcium carbonate, water, coalescents TEXANOL, light-weight inorganic acoutic fibre board, dispersant 8045, defoamer N × 2 and thickening agent XJ-AT702 are added in agitator tank by proportioning, with rotating speed 300r/min mixing and stirring;
(2) rotating speed is adjusted to 5000r/min on Multi-functional dispersion machine, stirs 4 hours, by high speed shear, mixture is uniformly dispersed;
(3) rotating speed is adjusted to 400r/min, is slowly added to nano-composite emulsion;
(4) add antibacterial, be kept stirring for 2h;
(5) gauze filters, tinning packaging.

Claims (9)

1. an aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, is characterized in that: by the following raw material counted by weight ratio by evenly mixing, be sufficiently stirred for and make:
Nano-composite emulsion 250~450, propylene glycol 0.2~2, inorganic filler 100~200, light-weight inorganic acoutic fibre board 100~300, dispersant 3~8, defoamer 0.3~3, thickening agent 0.5~3, coalescents 15~20, antibacterial 2~4, water 160~240.
2. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described nano-composite emulsion is the weight ratio of the mixture of polyvinyl acetate and pure-acrylic emulsion, polyvinyl acetate and pure-acrylic emulsion is 1:1.
3. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described inorganic filler is a kind of in titanium dioxide and precipitated calcium carbonate or both mixture, and the weight ratio of titanium dioxide and precipitated calcium carbonate is 1:1.
4. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described dispersant is the one in dispersant 8045,5040.
5. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described defoamer is defoamer N × 2.
6. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described thickening agent is thickening agent XJ-AT702.
7. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described coalescents is coalescents TEXANOL.
8. aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion according to claim 1, is characterized in that: described antibacterial is coating emulsion bactericidal liquid.
9. the preparation method of one of claim 1-8 described aqueous, environmental protective absorbing sound and lowering noise high-elastic waterproof emulsion, is characterized in that: comprise the steps:
(1) propylene glycol, inorganic filler, water, coalescents, light-weight inorganic acoutic fibre board, dispersant, defoamer and thickening agent are added in agitator tank by weight ratio, with rotating speed 250~350r/min mixing and stirring;
(2) rotating speed is adjusted to 4500~5000r/min on Multi-functional dispersion machine, stirs 3.5~4.5 hours, by high speed shear, mixture is uniformly dispersed;
(3) rotating speed is adjusted to 350~450r/min, is slowly added to nano-composite emulsion;
(4) add antibacterial, be kept stirring for 1.5~2.5h;
(5) gauze filters, tinning packaging.
CN201610211958.4A 2016-04-07 2016-04-07 Water-based, environment-friendly, sound-absorbing, noise-reducing, high-elasticity and waterproof emulsion and preparation method thereof Pending CN105802395A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400432A (en) * 2017-08-24 2017-11-28 南通捷皋家具有限公司 A kind of furniture aqueous, environmental protective water-proof emulsion and preparation method thereof
CN108300016A (en) * 2017-09-30 2018-07-20 江苏亿可得电子科技有限公司 A kind of television set method of producing waterproof coating material

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1269385A (en) * 1998-05-15 2000-10-11 株式会社三逊 Coating composition for fire-preventing and acoustics use
CN1817976A (en) * 2005-02-08 2006-08-16 庆东塞拉泰克有限公司 Coating composition for fire retardant and sound absorption
CN103450755A (en) * 2013-08-22 2013-12-18 江苏科技大学 Environmentally-friendly composite interior wall coating material and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1269385A (en) * 1998-05-15 2000-10-11 株式会社三逊 Coating composition for fire-preventing and acoustics use
CN1817976A (en) * 2005-02-08 2006-08-16 庆东塞拉泰克有限公司 Coating composition for fire retardant and sound absorption
CN103450755A (en) * 2013-08-22 2013-12-18 江苏科技大学 Environmentally-friendly composite interior wall coating material and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400432A (en) * 2017-08-24 2017-11-28 南通捷皋家具有限公司 A kind of furniture aqueous, environmental protective water-proof emulsion and preparation method thereof
CN108300016A (en) * 2017-09-30 2018-07-20 江苏亿可得电子科技有限公司 A kind of television set method of producing waterproof coating material

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