CN105780534B - The technique dyed using myrobalan's pigment to silk fabric - Google Patents
The technique dyed using myrobalan's pigment to silk fabric Download PDFInfo
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- CN105780534B CN105780534B CN201610155907.4A CN201610155907A CN105780534B CN 105780534 B CN105780534 B CN 105780534B CN 201610155907 A CN201610155907 A CN 201610155907A CN 105780534 B CN105780534 B CN 105780534B
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- silk fabric
- myrobalan
- pigment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67358—Halides or oxyhalides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
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- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of technique dyed using myrobalan fruit pigment to silk fabric, using following technique：Pre- matchmaker's dyeing dyes silk fabric with matchmaker's dyeing or rear matchmaker's dyeing.Pre- mordant dyeing color mordant is stannous chloride, calcium chloride, cerium chloride, lanthanum chloride or aluminum sulfate, and silk fabric is dyed according to the technique of pre- matchmaker's processing → dyeing → post processing；It is calcium chloride with mordant dyeing color mordant, silk fabric is dyed according to the technique of dyeing → post processing；Mordant dyeing color mordant is stannous chloride, cerium chloride, lanthanum chloride or aluminum sulfate afterwards, and silk fabric is dyed according to the technique of dyeing → rear matchmaker's processing → post processing.Myrobalan's pigment dye silk fabric meets requirement of the people to environmental protection and health using the mordant of environment-friendly type, and dyeing product color and luster is soft, good color fastness, and the tone of dyeing product can be enriched by using different mordant dyeing agent.Myrobalan's pigment dyeing can assign the certain healthcare function of fabric and good ultraviolet resistance.
Description
Technical field
The invention belongs to the dyeing and finishing technique fields of fabric, and in particular to a kind of that silk fabric is contaminated using myrobalan's pigment
The technique of color.
Background technology
With gradually stepping up for people's life up-to-dateness, the common living environment of the protection mankind realizes sustainable development
Exhibition is increasingly becoming the Main way of countries in the world economic development, and people are safe to use to the dress of textile and TEXTILE CHEMICALS
Increasingly pay attention to health, natural pigment has attracted the eyeball of correlative study person with its again the characteristics of richly endowed by nature.Natural colour
Element is the pigment obtained from natural resources, is mainly extracted from animal, plant and microorganism.Natural pigment has good
Ecological, environmental protective effect, it is safe and non-toxic, coloring tone naturally, some natural pigments derive from Chinese herbal medicine, itself possess medicinal
Value, can assign institute's dyeing and weaving object special medicinal health-care function for dyeing, such as antibacterial, anti-inflammatory, insect prevention, antiallergy, anti-swollen
Knurl, anti-oxidant, radiation protection, decompression etc. increase the added value of textile, and therefore, natural pigment dyeing in recent years receives favor.
But the shortcomings of natural color dyeing is not complete there are chromatography, and colorant match is difficult, it is therefore desirable to a greater variety of natural pigment dyeing are developed,
To enrich the chromatography of natural pigment.
The content of the invention
The object of the present invention is to provide a kind of technique dyed using myrobalan's pigment to silk fabric, and assign dyeing
The excellent ultraviolet resistance of fabric.
To achieve the above object, the present invention uses following technical scheme：
A kind of technique dyed using myrobalan's pigment to silk fabric, using following technique：It is pre- matchmaker's dyeing, same
Matchmaker's dyeing or rear matchmaker's dyeing dye silk fabric.
The pre- mordant dyeing color processing step is as follows：
（1）Pre- matchmaker's processing：By mordant preparation mordanting bath soluble in water, the silk fabric for putting into warm water in 40 DEG C and soaking,
Bath raio 1:20~1:40,85 DEG C, isothermal holding 40min are warming up to the heating rate of 2 DEG C/min, then the washing silk fabric that cools down；
（2）Dyeing：Pre- matchmaker is handled and the silk fabric after washing is put into 40 DEG C of myrobalan's pigment dye liquor, bath raio 1:20
~1:40,75 ~ 85 DEG C are warming up to the heating rate of 2 DEG C/min, 40 ~ 60min of heat preservation dyeing；
（3）Post processing：Silk fabric after dyeing is washed, neutrality is soaped, is washed, is dehydrated, drying；Wherein, in
Property is soaped washes 3 ~ 5min with 3g/L neutral detergents in 80 ~ 85 DEG C.
The step of pre- mordant dyeing color（1）In mordant be stannous chloride, calcium chloride, cerium chloride, lanthanum chloride or sulfuric acid
Aluminium, mordant dosage are 1% (owf) ~ 6% (owf).
The step of pre- mordant dyeing color（2）The dosage of myrobalan's pigment is 2% (owf) ~ 5% in middle myrobalan's pigment dye liquor
(owf), with acetum tune pH values 3 ~ 4.5.
The same mordant dyeing color processing step is as follows：
（1）Dyeing：By myrobalan's pigment and calcium chloride preparation dye liquor soluble in water, with acetum tune pH values 3 ~ 4.5, in
The silk fabric of 40 DEG C of input warm water wettings, bath raio 1:20~1:40, then 75 ~ 85 are warming up to the heating rate of 2 DEG C/min
DEG C, 40 ~ 60min of heat preservation dyeing；
（2）Post processing：Silk fabric after dyeing is washed, neutrality is soaped, is washed, is dehydrated, drying；Wherein, in
Property is soaped washes 3 ~ 5min with 3g/L neutral detergents in 80 ~ 85 DEG C.
Same matchmaker's staining procedure（1）Dye liquor in, the dosage of myrobalan's pigment is 2% (owf) ~ 5% (owf), calcium chloride
Dosage be 1% (owf) ~ 4% (owf).
The rear mordant dyeing color processing step is as follows：
（1）Dyeing：By myrobalan's pigment preparation dye liquor soluble in water, with acetum tune pH values 3 ~ 4.5, put into 40 DEG C
The silk fabric of warm water wetting, bath raio 1:20~1:40, then 75 ~ 85 DEG C of institute, heat preservation dye are warming up to the heating rate of 2 DEG C/min
40 ~ 60min of color, then cooling washing；
（2）Matchmaker is handled afterwards：Silk fabric after dyed and washing is put into 40 DEG C of mordanting bath, bath raio 1:20~1:
40,85 DEG C are warming up to the heating rate of 2 DEG C/min, isothermal holding 40min；
（3）Post processing：Washing, neutrality are soaped, wash, are dehydrated, dried.Wherein, neutrality is soaped with 3g/L neutral detergents
3 ~ 5min is washed in 80 ~ 85 DEG C.
After described the step of matchmaker's dyeing（1）In dye liquor in myrobalan's pigment dosage be 2% (owf) ~ 5%
(owf)。
After described the step of matchmaker's dyeing（2）In mordant for stannous chloride, cerium chloride, lanthanum chloride or aluminum sulfate,
Mordant dosage is 1% (owf) ~ 6% (owf).
Beneficial effects of the present invention：Silk fabric is in bronzing through myrobalan's pigment dyeing；It is knitted with stannous chloride as mordant
Object changes of shade is apparent, and with apparent green light in yellow light, in green-yellow, brightness and vividness improve；Make matchmaker with aluminum sulfate
The feux rouges of stain fabric disappears, in isabelline；It is minimum to make mordant changes of shade with calcium chloride, still in bronzing；Use cerium chloride
Make mordant, feux rouges, the yellow light of fabric weaken, in isabelline；Make mordant with lanthanum chloride, fabric feux rouges weakens, and yellow light does not have
Significant change it is close to make mordant fabric color, in isabelline with cerium chloride.Mordant dyeing can enrich myrobalan's pigment dyeing fabric
Color, while the color fastness of dyed fabric can also be improved.Myrobalan's pigment source has antioxygen in the fruit of plant myrobalan, myrobalan fruit
Change, antibacterial, antiviral, convergence, spasmolysis, antidiarrheal, it is antitumor the effects that, the pigment composition of myrobalan fruit be also myrobalan fruit activity into
Point, myrobalan's pigment dyeing can assign fabric certain healthcare function, and myrobalan's pigment also has certain ultraviolet-absorbing in addition
Can, myrobalan's pigment dyeing fabric has good ultraviolet resistance.Silk fabric has fine and smooth submissive, smooth elegant matter
Sense, good sucting wet air permeability and pro-skin are esthetics, are high-grade garment materials, are well received by consumers.By myrobalan's pigment
The advantages of dyeing, both making for silk fabric perfect adaptation, brings out the best in each other, and meets people to environmental protection and health
It is required that there is very big market potential.
Specific embodiment
Embodiment 1
The pre- matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of mordanting baths containing 1% (owf) stannous chloride, bath raio 1:20,
85 DEG C are warming up to the heating rate of 2 DEG C/min, heat preservation 40min carries out mordant dyeing processing, then cooling washing silk fabric.It will be pre-
Silk fabric after matchmaker handles and washes is put into 40 DEG C of dye liquors containing myrobalan's pigment 2% (owf), with acetum tune pH
Value 3, bath raio 1:40,75 DEG C are warming up to the heating rate of 2 DEG C/min, then heat preservation dyeing 60min knits the silk after dyeing
Object is post-processed, and post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 2
The pre- matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of mordanting baths containing 6% (owf) cerium chloride, bath raio 1:30, with
The heating rate of 2 DEG C/min is warming up to 85 DEG C, and heat preservation 40min carries out mordant dyeing processing, then cooling washing silk fabric.By pre- matchmaker
Silk fabric after handling and washing is put into 40 DEG C of dye liquors containing myrobalan's pigment 5% (owf), with acetum tune pH values
4, bath raio 1:20,85 DEG C are warming up to the heating rate of 2 DEG C/min, heat preservation dyeing 40min, then to the silk fabric after dyeing
It is post-processed, post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 3
The pre- matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of mordanting baths containing 2% (owf) lanthanum chloride, bath raio 1:40, with 2
DEG C/heating rate of min is warming up to 85 DEG C, heat preservation 40min carries out mordant dyeing processing, then cooling washing silk fabric.By pre- matchmaker
Silk fabric after handling and washing is put into 40 DEG C of dye liquors containing myrobalan's pigment 3% (owf), with acetum tune pH values
4.5, bath raio 1:30,80 DEG C are warming up to the heating rate of 2 DEG C/min, then heat preservation dyeing 50min knits the silk after dyeing
Object is post-processed, and post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 4
The pre- matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of mordanting baths containing 4% (owf) calcium chloride, bath raio 1:25, with
The heating rate of 2 DEG C/min is warming up to 85 DEG C, and heat preservation 40min carries out mordant dyeing processing, then cooling washing silk fabric.By pre- matchmaker
Silk fabric after handling and washing is put into 40 DEG C of dye liquors containing myrobalan's pigment 4% (owf), with acetum tune pH values
3.5, bath raio 1:35,85 DEG C are warming up to the heating rate of 2 DEG C/min, then heat preservation dyeing 45min knits the silk after dyeing
Object is post-processed, and post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 5
The pre- matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of mordanting baths containing 3% (owf) aluminum sulfate, bath raio 1:35, with
The heating rate of 2 DEG C/min is warming up to 85 DEG C, and heat preservation 40min carries out mordant dyeing processing, then cooling washing silk fabric.By pre- matchmaker
Silk fabric after handling and washing is put into 40 DEG C of dye liquors containing myrobalan's pigment 3% (owf), with acetum tune pH values
4, bath raio 1:30,80 DEG C are warming up to the heating rate of 2 DEG C/min, heat preservation dyeing 55min, then to the silk fabric after dyeing
It is post-processed, post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 6
The same matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dyes containing 2% (owf) myrobalan pigment and 1% (owf) calcium chloride
In liquid, with acetum tune pH values 3, bath raio 1:20,85 DEG C, heat preservation dyeing 40min are warming up to the heating rate of 2 DEG C/min,
Then the silk fabric after dyeing is post-processed, post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 7
The same matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dyes containing 5% (owf) myrobalan pigment and 4% (owf) calcium chloride
In liquid, with acetum tune pH values 4.5, bath raio 1:40,75 DEG C are warming up to the heating rate of 2 DEG C/min, heat preservation dyeing
Then 60min post-processes the silk fabric after dyeing, post processing includes washing, neutrality is soaped, washes, is dehydrated, dried
It is dry.
Embodiment 8
The rear matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dye liquors containing 2% (owf) myrobalan's pigment, uses acetum
Adjust pH values 3, bath raio 1:20,75 DEG C, heat preservation dyeing 60min are warming up to the heating rate of 2 DEG C/min, then cooling washing.It will
Silk fabric after dyed and washing is put into 40 DEG C of mordanting baths containing 1% (owf) aluminum sulfate, bath raio 1:40, with 2 DEG C/
The heating rate of min is warming up to 85 DEG C, then isothermal holding 40min post-processes the silk fabric after dyeing, post processing
Including washing, neutrality is soaped, is washed, is dehydrated, drying.
Embodiment 9
The rear matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dye liquors containing 5% (owf) myrobalan's pigment, uses acetum
Adjust pH values 4.5, bath raio 1:40,85 DEG C, heat preservation dyeing 40min are warming up to the heating rate of 2 DEG C/min, then cooling washing.
Silk fabric after dyed and washing is put into 40 DEG C of mordanting baths containing 6% (owf) stannous chloride, bath raio 1:30, with
The heating rate of 2 DEG C/min is warming up to 85 DEG C, then isothermal holding 40min post-processes the silk fabric after dyeing, after
Processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Embodiment 10
The rear matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dye liquors containing 3% (owf) myrobalan's pigment, uses acetum
Adjust pH values 4, bath raio 1:30,85 DEG C, heat preservation dyeing 50min are warming up to the heating rate of 2 DEG C/min, then cooling washing.It will
Silk fabric after dyed and washing is put into 40 DEG C of mordanting baths containing 2% (owf) cerium chloride, bath raio 1:20, with 2 DEG C/
The heating rate of min is warming up to 85 DEG C, then isothermal holding 40min post-processes the silk fabric after dyeing, post processing
Including washing, neutrality is soaped, is washed, is dehydrated, drying.
Embodiment 11
The rear matchmaker's dyeing dyed using myrobalan's pigment to silk fabric of the present embodiment, step are as follows：
The silk fabric of warm water wetting is put into 40 DEG C of dye liquors containing 4% (owf) myrobalan's pigment, uses acetum
Adjust pH values 3.5, bath raio 1:35,80 DEG C, heat preservation 55 min of dyeing are warming up to the heating rate of 2 DEG C/min, then temperature lowering water
It washes.Silk fabric after dyed and washing is put into 40 DEG C of mordanting baths containing 4% (owf) lanthanum chloride, bath raio 1:30,
85 DEG C are warming up to the heating rate of 2 DEG C/min, then isothermal holding 40min post-processes the silk fabric after dyeing,
Post processing includes washing, neutrality is soaped, washes, is dehydrated, dried.
Fabric apparent shade depthK/SThe measure of value：With CE-7000A SCT high-precisions colour photometer (the color general limited public affairs of science and technology in Shenyang
Department) it measures, using D65Light source and 10°Viewing angle, each sample are surveyed 4 times, are averaged.
Crock fastness is tested：With reference to GB/T 3920-2008《Textile color stability tests colour fastness to rubbing》It carries out
Test.
Soaping fastness is tested；With reference to GB/T 3921.1-2008《Textile color stability tests color fastness to washing》It carries out
Test.
Color fastness to water：With reference to GB/T 5713-2013《Textile color stability tests color fastness to water》It is tested.
Colour fastness to perspiration：With reference to GB/T 3922-2013《Textile color stability tests colour fastness to perspiration》It is surveyed
Examination.
Ultraviolet resistance：With reference to GB/T 18830-2002《The evaluation of textile uv resistance energy》It is tested.
The color fastness for the stamp silk fabric that table 1 is measured into table 5 reaches GB/T 15551-2007《Light of Mulberry Silk Fabrics》
High-class product standard.Showing the silk fabric of myrobalan's pigment dyeing has excellent color fastness.From table 1 into table 5 as can be seen that with
Undyed silk fabric is compared, and silk fabric T (UVA), the T (UVB) of myrobalan's pigment dyeing are decreased obviously, and UPF is significantly increased,
Showing the silk fabric of myrobalan's pigment dyeing has good ultraviolet resistance.
K/S values, color fastness and the ultraviolet resistance of silk fabric after table 1 is dyed according to embodiment 3
K/S values, color fastness and the ultraviolet resistance of silk fabric after table 2 is dyed according to embodiment 5
K/S values, color fastness and the ultraviolet resistance of silk fabric after table 3 is dyed according to embodiment 7
K/S values, color fastness and the ultraviolet resistance of silk fabric after table 4 is dyed according to embodiment 9
K/S values, color fastness and the ultraviolet resistance of silk fabric after table 5 is dyed according to embodiment 10
Note：The T (UVA) of silk fabric is that 15.71%, T (UVB) is 4.55%, UPF 13.11 before dyeing.
Basic principle of the invention and main feature and advantages of the present invention has been shown and described above.The skill of the industry
Art personnel it should be appreciated that the present invention is not limited to the above embodiments, the above embodiments and description only describe
The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these
Changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and
Its equivalent thereof.
Claims (4)
1. a kind of technique dyed using myrobalan's pigment to silk fabric, it is characterised in that use following technique：Pre- mordant dyeing
Color technique dyes silk fabric with matchmaker's dyeing or rear matchmaker's dyeing；
The pre- mordant dyeing color processing step is as follows：
（1）Pre- matchmaker's processing：By mordant preparation mordanting bath soluble in water, the silk fabric for putting into warm water in 40 DEG C and soaking, bath raio
1:20~1:40,85 DEG C, isothermal holding 40min are warming up to the heating rate of 2 DEG C/min, then the washing silk fabric that cools down；
（2）Dyeing：Pre- matchmaker is handled and the silk fabric after washing is put into 40 DEG C of myrobalan's pigment dye liquor, bath raio 1:20~1:
40,75 ~ 85 DEG C are warming up to the heating rate of 2 DEG C/min, 40 ~ 60min of heat preservation dyeing；
（3）Post processing：Silk fabric after dyeing is washed, neutrality is soaped, is washed, is dehydrated, drying；Wherein, neutral soap
It washes and washes 3 ~ 5min in 80 ~ 85 DEG C with 3g/L neutral detergents；
The step of pre- mordant dyeing color（1）In mordant for stannous chloride, calcium chloride, cerium chloride, lanthanum chloride or aluminum sulfate, matchmaker
Stain dosage is 1%owf ~ 6%owf；
The same mordant dyeing color processing step is as follows：
（1）Dyeing：By myrobalan's pigment and calcium chloride preparation dye liquor soluble in water, with acetum tune pH values 3 ~ 4.5, in 40 DEG C
Put into the silk fabric of warm water wetting, bath raio 1:20~1:40,75 ~ 85 DEG C then are warming up to the heating rate of 2 DEG C/min, is protected
40 ~ 60min of temperature dyeing；
（2）Post processing：Silk fabric after dyeing is washed, neutrality is soaped, is washed, is dehydrated, drying；Wherein, neutral soap
It washes and washes 3 ~ 5min in 80 ~ 85 DEG C with 3g/L neutral detergents；
The rear mordant dyeing color processing step is as follows：
（1）Dyeing：By myrobalan's pigment preparation dye liquor soluble in water, with acetum tune pH values 3 ~ 4.5, warm water is put into 40 DEG C
The silk fabric of wetting, bath raio 1:20~1:40, then with the heating rate of 2 DEG C/min be warming up to institute 75 ~ 85 DEG C, heat preservation dyeing 40 ~
60min, then cooling washing；
（2）Matchmaker is handled afterwards：Silk fabric after dyed and washing is put into 40 DEG C of mordanting bath, bath raio 1:20~1:40, with
The heating rate of 2 DEG C/min is warming up to 85 DEG C, isothermal holding 40min；
（3）Post processing：Washing, neutrality are soaped, wash, are dehydrated, dried；Wherein, neutrality soap with 3g/L neutral detergents in 80 ~
85 DEG C are washed 3 ~ 5min；
After described the step of matchmaker's dyeing（2）In mordant for stannous chloride, cerium chloride, lanthanum chloride or aluminum sulfate, mordant dyeing
Agent dosage is 1%owf ~ 6%owf.
2. the technique according to claim 1 dyed using myrobalan's pigment to silk fabric, it is characterised in that：It is described
The step of pre- mordant dyeing color（2）The dosage of myrobalan's pigment is 2% (owf) ~ 5% (owf, with acetum tune in middle myrobalan's pigment dye liquor
PH value 3 ~ 4.5.
3. the technique according to claim 1 dyed using myrobalan's pigment to silk fabric, it is characterised in that：It is described
With matchmaker's staining procedure（1）Dye liquor in, the dosage of myrobalan's pigment is the owf of 2%owf ~ 5%, and the dosage of calcium chloride is 1%owf ~ 4%
owf。
4. the technique according to claim 1 dyed using myrobalan's pigment to silk fabric, it is characterised in that：It is described
The step of matchmaker's dyeing afterwards（1）In dye liquor in myrobalan's pigment dosage be 2%owf ~ 5%owf.
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| CN106320001A (en) * | 2016-08-19 | 2017-01-11 | 河南工程学院 | Method for dyeing wool by myrobalan pigment |
| CN107217503A (en) * | 2017-06-21 | 2017-09-29 | 河南工程学院 | The method of silk fabric is contaminated using gardenia blue pigment |
| CN107829315A (en) * | 2017-12-01 | 2018-03-23 | 河南工程学院 | The method of silk fabric green colouring |
| CN109162117B (en) * | 2018-08-06 | 2020-04-10 | 河南工程学院 | Method for dyeing cotton fabric green by using natural pigment |
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| CN102061633A (en) * | 2010-12-10 | 2011-05-18 | 江南大学 | Method for dyeing protein fiber and fabric thereof with natural dye extracted from grape seeds |
| CN102220705A (en) * | 2011-04-20 | 2011-10-19 | 盐城纺织职业技术学院 | Method for dying silk fabric by using natural dye of Suaeda salsa |
| CN103665926A (en) * | 2013-12-16 | 2014-03-26 | 江苏波波熊纺织品有限公司 | Preparation method and application of natural semen cuscutae dye |
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