CN105771313B - 一种映山红黄酮提取系统 - Google Patents
一种映山红黄酮提取系统 Download PDFInfo
- Publication number
- CN105771313B CN105771313B CN201610320994.4A CN201610320994A CN105771313B CN 105771313 B CN105771313 B CN 105771313B CN 201610320994 A CN201610320994 A CN 201610320994A CN 105771313 B CN105771313 B CN 105771313B
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- CN
- China
- Prior art keywords
- extractor
- sliding block
- stripper
- puddler
- heat exchanger
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- 241000208422 Rhododendron Species 0.000 title claims abstract description 13
- 229930003935 flavonoid Natural products 0.000 title claims abstract description 9
- 150000002215 flavonoids Chemical class 0.000 title claims abstract description 9
- 235000017173 flavonoids Nutrition 0.000 title claims abstract description 9
- 238000000605 extraction Methods 0.000 claims abstract description 51
- 239000000463 material Substances 0.000 claims abstract description 24
- 230000005484 gravity Effects 0.000 claims abstract description 5
- 238000002604 ultrasonography Methods 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 18
- 229930003944 flavone Natural products 0.000 claims description 16
- 235000011949 flavones Nutrition 0.000 claims description 16
- 150000002213 flavones Chemical class 0.000 claims description 15
- 241000196324 Embryophyta Species 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 10
- 239000003480 eluent Substances 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 8
- 238000004108 freeze drying Methods 0.000 claims description 7
- 238000007599 discharging Methods 0.000 claims description 6
- 238000010828 elution Methods 0.000 claims description 6
- 239000011347 resin Substances 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 230000008676 import Effects 0.000 claims description 3
- 238000013507 mapping Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims 1
- 238000007906 compression Methods 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000009413 insulation Methods 0.000 abstract description 3
- 238000005292 vacuum distillation Methods 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000011084 recovery Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/28—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only
- C07D311/30—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only not hydrogenated in the hetero ring, e.g. flavones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/40—Separation, e.g. from natural material; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
- C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
- C07H17/06—Benzopyran radicals
- C07H17/065—Benzo[b]pyrans
- C07H17/07—Benzo[b]pyran-4-ones
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Abstract
Description
Claims (1)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201420448612 | 2014-08-10 | ||
CN2014204486122 | 2014-08-10 | ||
CN201510426874.8A CN105056570B (zh) | 2014-08-10 | 2015-07-18 | 从映山红叶中快速提取黄酮的系统 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510426874.8A Division CN105056570B (zh) | 2014-08-10 | 2015-07-18 | 从映山红叶中快速提取黄酮的系统 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105771313A CN105771313A (zh) | 2016-07-20 |
CN105771313B true CN105771313B (zh) | 2017-11-24 |
Family
ID=54486213
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610320994.4A Expired - Fee Related CN105771313B (zh) | 2014-08-10 | 2015-07-18 | 一种映山红黄酮提取系统 |
CN201510426874.8A Active CN105056570B (zh) | 2014-08-10 | 2015-07-18 | 从映山红叶中快速提取黄酮的系统 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510426874.8A Active CN105056570B (zh) | 2014-08-10 | 2015-07-18 | 从映山红叶中快速提取黄酮的系统 |
Country Status (1)
Country | Link |
---|---|
CN (2) | CN105771313B (zh) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2198016Y (zh) * | 1994-07-26 | 1995-05-24 | 何晓东 | 动态多能提取罐 |
CN1240677A (zh) * | 1998-06-25 | 2000-01-12 | 李纪东 | 离心式草本植物提取器传动装置 |
CN202777910U (zh) * | 2012-08-08 | 2013-03-13 | 天津必佳药业集团有限公司 | 多调压阀式中药提取罐 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1172808A (zh) * | 1997-02-27 | 1998-02-11 | 罗海章 | 用葛根联合生产淀粉,异黄酮类、葛(全)根饮料的工艺方法 |
CN1127507C (zh) * | 1999-01-25 | 2003-11-12 | 南开大学 | 用吸附剂从植物中提取天然黄酮类和/或萜内酯类的方法 |
CN1093416C (zh) * | 1999-12-08 | 2002-10-30 | 中国科学院武汉植物研究所 | 防治心血管病的植物制剂的制备方法 |
CN1422855A (zh) * | 2001-12-03 | 2003-06-11 | 尹华清 | 工业化的用大豆豆粕生产大豆异黄酮的方法 |
CN1237896C (zh) * | 2003-07-18 | 2006-01-25 | 华南理工大学 | 一种甘甜味大豆异黄酮基料的生产方法 |
CN1473822A (zh) * | 2003-08-05 | 2004-02-11 | 西安翠宝首饰集团公司 | 浮萍中黄酮和多糖的提取工艺 |
CN1927857A (zh) * | 2006-09-25 | 2007-03-14 | 奈曼旗国有资产发展投资经营公司 | 荞麦苗总黄酮提取精制工艺 |
CL2010000003A1 (es) * | 2010-01-04 | 2010-04-16 | Natural Response S A | Aparato para extraccion de principios activos de fuentes naturales, que comprende una carcasa que encierra y soporta un primer tornillo transportador, una tolva de entrada con un segundo tornillo, una tolva de salida, una linea de descarga de extracto liquido y un sistema de transduccion acustica, y un metodo para la extraccion. |
BR112012024469B1 (pt) * | 2010-03-31 | 2020-05-05 | Desmet Ballestra North America Inc | extrator de solvente de camada baixa |
-
2015
- 2015-07-18 CN CN201610320994.4A patent/CN105771313B/zh not_active Expired - Fee Related
- 2015-07-18 CN CN201510426874.8A patent/CN105056570B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2198016Y (zh) * | 1994-07-26 | 1995-05-24 | 何晓东 | 动态多能提取罐 |
CN1240677A (zh) * | 1998-06-25 | 2000-01-12 | 李纪东 | 离心式草本植物提取器传动装置 |
CN202777910U (zh) * | 2012-08-08 | 2013-03-13 | 天津必佳药业集团有限公司 | 多调压阀式中药提取罐 |
Also Published As
Publication number | Publication date |
---|---|
CN105056570B (zh) | 2016-12-07 |
CN105771313A (zh) | 2016-07-20 |
CN105056570A (zh) | 2015-11-18 |
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CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Rao Lin Inventor before: Hu Liuman |
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Effective date of registration: 20171031 Address after: 312400 Zhejiang city of Shaoxing province Shengzhou City Zhijie Lake Yan Shengzhou Building No. 37 North Street Applicant after: Shengzhou Northern Star Investment Limited company of science and technology of the public record Address before: 2 No. 201, room 246620, Fan Ye resettlement area, Paradise Town, Yuexi County, Anqing, Anhui Applicant before: Hu Liuman |
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Effective date of registration: 20190415 Address after: 102600 3 floor, 2 building, No. 4 Daxing District Garden Road, Beijing, 1 unit 317 Patentee after: BEIJING ZHITOUJIA INTELLECTUAL PROPERTY OPERATION CO.,LTD. Address before: 312400 Shengzhou Building, 37 Beizhi Street, Chenghu Street, Shengzhou City, Shaoxing City, Zhejiang Province Patentee before: Shengzhou Northern Star Investment Limited company of science and technology of the public record |
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Effective date of registration: 20191126 Address after: Room 602, building H2, Changyuan road international enterprise community, Wuqing Development Zone, Wuqing District, Tianjin Patentee after: TIANJIN LEISHENG TECHNOLOGY Co.,Ltd. Address before: 102600 Unit 317, Unit 1, Building 3, No. 2, Yueyuan Road, Daxing District, Beijing Patentee before: BEIJING ZHITOUJIA INTELLECTUAL PROPERTY OPERATION CO.,LTD. |
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Effective date of registration: 20201106 Address after: No.99, Dongbao Road, Jiangdong Street, Gulou District, Nanjing, Jiangsu Province, 210000 Patentee after: Chai Fenfen Address before: Room 602, building H2, Changyuan road international enterprise community, Wuqing Development Zone, Wuqing District, Tianjin Patentee before: TIANJIN LEISHENG TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20220308 Address after: 100089 No. 6, unit 3, building 4, beixinjiayuan, yard 39, Jiancai Chengxi Road, Haidian District, Beijing Patentee after: Chen Feng Address before: No.99, Dongbao Road, Jiangdong Street, Gulou District, Nanjing, Jiangsu Province, 210000 Patentee before: Chai Fenfen |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171124 |