CN105130937B - 用于提取植物黄酮的设备 - Google Patents
用于提取植物黄酮的设备 Download PDFInfo
- Publication number
- CN105130937B CN105130937B CN201510426928.0A CN201510426928A CN105130937B CN 105130937 B CN105130937 B CN 105130937B CN 201510426928 A CN201510426928 A CN 201510426928A CN 105130937 B CN105130937 B CN 105130937B
- Authority
- CN
- China
- Prior art keywords
- heat exchanger
- extractor
- stripper
- equipment
- storage tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229930003944 flavone Natural products 0.000 title claims abstract description 24
- 235000011949 flavones Nutrition 0.000 title claims abstract description 24
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title claims abstract description 13
- 150000002212 flavone derivatives Chemical class 0.000 title claims abstract description 13
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 43
- 238000003860 storage Methods 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 239000012530 fluid Substances 0.000 claims abstract description 12
- 239000011347 resin Substances 0.000 claims abstract description 8
- 229920005989 resin Polymers 0.000 claims abstract description 8
- 238000009434 installation Methods 0.000 claims abstract description 5
- 238000001694 spray drying Methods 0.000 claims abstract description 5
- 230000008676 import Effects 0.000 claims abstract description 4
- 230000007246 mechanism Effects 0.000 claims description 21
- 239000000463 material Substances 0.000 claims description 20
- 241000196324 Embryophyta Species 0.000 claims description 18
- 150000002213 flavones Chemical class 0.000 claims description 11
- 239000003480 eluent Substances 0.000 claims description 9
- 210000002683 foot Anatomy 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 4
- 230000005484 gravity Effects 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000009413 insulation Methods 0.000 abstract description 3
- 238000005292 vacuum distillation Methods 0.000 abstract description 3
- 238000007599 discharging Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- 241000208422 Rhododendron Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- BGOFCVIGEYGEOF-UJPOAAIJSA-N helicin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=CC=C1C=O BGOFCVIGEYGEOF-UJPOAAIJSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/28—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only
- C07D311/30—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only not hydrogenated in the hetero ring, e.g. flavones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0011—Heating features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/40—Separation, e.g. from natural material; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Claims (3)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710314506.3A CN106967032B8 (zh) | 2014-08-10 | 2015-07-18 | 对植物茎叶中黄酮的快速提取的设备及其工作方法 |
CN201710314511.4A CN107158740A (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
CN201510426928.0A CN105130937B (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2014204486781 | 2014-08-10 | ||
CN201420448678 | 2014-08-10 | ||
CN201510426928.0A CN105130937B (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710314511.4A Division CN107158740A (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
CN201710314506.3A Division CN106967032B8 (zh) | 2014-08-10 | 2015-07-18 | 对植物茎叶中黄酮的快速提取的设备及其工作方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105130937A CN105130937A (zh) | 2015-12-09 |
CN105130937B true CN105130937B (zh) | 2017-05-31 |
Family
ID=54716568
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510426928.0A Expired - Fee Related CN105130937B (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
CN201710314506.3A Active CN106967032B8 (zh) | 2014-08-10 | 2015-07-18 | 对植物茎叶中黄酮的快速提取的设备及其工作方法 |
CN201710314511.4A Withdrawn CN107158740A (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
Family Applications After (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710314506.3A Active CN106967032B8 (zh) | 2014-08-10 | 2015-07-18 | 对植物茎叶中黄酮的快速提取的设备及其工作方法 |
CN201710314511.4A Withdrawn CN107158740A (zh) | 2014-08-10 | 2015-07-18 | 用于提取植物黄酮的设备 |
Country Status (1)
Country | Link |
---|---|
CN (3) | CN105130937B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111909125B (zh) * | 2020-08-31 | 2023-09-12 | 苏州市海崴生物科技有限公司 | 一种铁皮石斛叶中提取黄酮的装置及方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2564443C (en) * | 2004-05-10 | 2016-04-26 | Instituto Tecnologico Y De Estudios Superiores De Monterrey (Itesm) | Cancer cell growth inhibition by black bean (phaseolus vulgaris l) extracts |
CN101485939B (zh) * | 2009-01-05 | 2010-12-29 | 天津大学 | 气液固循环流化床吸附分离装置及操作方法 |
CL2010000003A1 (es) * | 2010-01-04 | 2010-04-16 | Natural Response S A | Aparato para extraccion de principios activos de fuentes naturales, que comprende una carcasa que encierra y soporta un primer tornillo transportador, una tolva de entrada con un segundo tornillo, una tolva de salida, una linea de descarga de extracto liquido y un sistema de transduccion acustica, y un metodo para la extraccion. |
CN101816684A (zh) * | 2010-04-09 | 2010-09-01 | 华东理工大学 | 从草本植物中利用微波提取和大孔树脂纯化黄酮的方法 |
CN101879380B (zh) * | 2010-06-25 | 2012-07-18 | 戴群 | 提取植物有效成份的节能浓缩工艺及其浓缩装置 |
CN203750212U (zh) * | 2014-04-11 | 2014-08-06 | 王和能 | 一种从黄色杜鹃叶中提取黄酮的设备 |
CN103893991B (zh) * | 2014-04-22 | 2015-11-04 | 广东世信药业有限公司 | 一种中药热循环提取浓缩方法 |
-
2015
- 2015-07-18 CN CN201510426928.0A patent/CN105130937B/zh not_active Expired - Fee Related
- 2015-07-18 CN CN201710314506.3A patent/CN106967032B8/zh active Active
- 2015-07-18 CN CN201710314511.4A patent/CN107158740A/zh not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
CN106967032B8 (zh) | 2020-01-14 |
CN106967032A (zh) | 2017-07-21 |
CN105130937A (zh) | 2015-12-09 |
CN106967032B (zh) | 2019-12-20 |
CN107158740A (zh) | 2017-09-15 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Meiling Inventor after: Gong Yuting Inventor after: Hu Liuman Inventor before: Hu Liuman |
|
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Meiling Inventor after: Gong Yuting Inventor after: Liang Lizhu Inventor before: Li Meiling Inventor before: Gong Yuting Inventor before: Hu Liuman |
|
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20170505 Address after: 362000 Shigu City, Quanzhou province Yongchun County town of Dongan village, No. 269, No. Applicant after: Liang Lizhu Address before: 246002 Anhui province Anqing City Daguan District Jixian Road No. 148 Applicant before: Hu Liuman |
|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20190115 Address after: 221000 West Side of 252 Provincial Road, Biantang Town, Jiawang District, Xuzhou City, Jiangsu Province Patentee after: XUZHOU SHUANGYU AGRICULTURAL DEVELOPMENT Co.,Ltd. Address before: 362000 Dongan village, Shigu Town, Yongchun County, Quanzhou, Fujian 269 Patentee before: Liang Lizhu |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170531 |