CN106967032B8 - 对植物茎叶中黄酮的快速提取的设备及其工作方法 - Google Patents

对植物茎叶中黄酮的快速提取的设备及其工作方法 Download PDF

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Publication number
CN106967032B8
CN106967032B8 CN201710314506.3A CN201710314506A CN106967032B8 CN 106967032 B8 CN106967032 B8 CN 106967032B8 CN 201710314506 A CN201710314506 A CN 201710314506A CN 106967032 B8 CN106967032 B8 CN 106967032B8
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China
Prior art keywords
leaves
equipment
plant stems
working method
flavone
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CN201710314506.3A
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English (en)
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CN106967032B (zh
CN106967032A (zh
Inventor
林焕新
张森烽
其他发明人请求不公开姓名
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Guangdong Xianglong flavor Co., Ltd
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Guangdong Xianglong Flavor Co ltd
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
    • C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
    • C07D311/28—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only
    • C07D311/30—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only not hydrogenated in the hetero ring, e.g. flavones
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/0011—Heating features
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/30—Accessories for evaporators ; Constructional details thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D36/00—Filter circuits or combinations of filters with other separating devices
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
    • C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
    • C07D311/40—Separation, e.g. from natural material; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

本发明涉及一种对植物茎叶中黄酮的快速提取的设备及其工作方法，包括依次设置的提取装置、过滤装置、提取液储罐、树脂床、洗脱液储罐、减压浓缩装置、喷雾干燥装置，减压浓缩装置与提取装置之间设置有换热器，洗脱液储罐内设置有换热管，换热管的入口与减压浓缩装置的气体出口相连接，换热管的出口与换热器的热流体进口相连接，换热器冷流体入口与提取剂储罐的出口相连接，换热器冷、热流体的出口与提取装置的提取剂进口相连接。上述技术方案可实现对植物茎叶中黄酮的快速提取，且提取液中黄酮的浓度高，便于后续的浓缩纯化处理和节约能源。
CN201710314506.3A 2014-08-10 2015-07-18 对植物茎叶中黄酮的快速提取的设备及其工作方法 Active CN106967032B8 (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201420448678 2014-08-10
CN2014204486781 2014-08-10
CN201510426928.0A CN105130937B (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201510426928.0A Division CN105130937B (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备

Publications (3)

Publication Number Publication Date
CN106967032A CN106967032A (zh) 2017-07-21
CN106967032B CN106967032B (zh) 2019-12-20
CN106967032B8 true CN106967032B8 (zh) 2020-01-14

Family

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Family Applications (3)

Application Number Title Priority Date Filing Date
CN201710314511.4A Withdrawn CN107158740A (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备
CN201510426928.0A Expired - Fee Related CN105130937B (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备
CN201710314506.3A Active CN106967032B8 (zh) 2014-08-10 2015-07-18 对植物茎叶中黄酮的快速提取的设备及其工作方法

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Application Number Title Priority Date Filing Date
CN201710314511.4A Withdrawn CN107158740A (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备
CN201510426928.0A Expired - Fee Related CN105130937B (zh) 2014-08-10 2015-07-18 用于提取植物黄酮的设备

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CN (3) CN107158740A (zh)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111909125B (zh) * 2020-08-31 2023-09-12 苏州市海崴生物科技有限公司 一种铁皮石斛叶中提取黄酮的装置及方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101485939A (zh) * 2009-01-05 2009-07-22 天津大学 气液固循环流化床吸附分离装置及操作方法
CN101816684A (zh) * 2010-04-09 2010-09-01 华东理工大学 从草本植物中利用微波提取和大孔树脂纯化黄酮的方法
CN101879380A (zh) * 2010-06-25 2010-11-10 戴群 提取植物有效成份的节能浓缩工艺及其浓缩装置
EP2311476A2 (en) * 2004-05-10 2011-04-20 Instituto Tecnologico y de Estudios Superiores de Monterrey Cancer cell growth inhibition by black bean (phaseolus vulgaris l) extracts
CN103893991A (zh) * 2014-04-22 2014-07-02 广东世信药业有限公司 一种中药热循环提取浓缩方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CL2010000003A1 (es) * 2010-01-04 2010-04-16 Natural Response S A Aparato para extraccion de principios activos de fuentes naturales, que comprende una carcasa que encierra y soporta un primer tornillo transportador, una tolva de entrada con un segundo tornillo, una tolva de salida, una linea de descarga de extracto liquido y un sistema de transduccion acustica, y un metodo para la extraccion.
CN203750212U (zh) * 2014-04-11 2014-08-06 王和能 一种从黄色杜鹃叶中提取黄酮的设备

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2311476A2 (en) * 2004-05-10 2011-04-20 Instituto Tecnologico y de Estudios Superiores de Monterrey Cancer cell growth inhibition by black bean (phaseolus vulgaris l) extracts
CN101485939A (zh) * 2009-01-05 2009-07-22 天津大学 气液固循环流化床吸附分离装置及操作方法
CN101816684A (zh) * 2010-04-09 2010-09-01 华东理工大学 从草本植物中利用微波提取和大孔树脂纯化黄酮的方法
CN101879380A (zh) * 2010-06-25 2010-11-10 戴群 提取植物有效成份的节能浓缩工艺及其浓缩装置
CN103893991A (zh) * 2014-04-22 2014-07-02 广东世信药业有限公司 一种中药热循环提取浓缩方法

Also Published As

Publication number Publication date
CN106967032B (zh) 2019-12-20
CN105130937A (zh) 2015-12-09
CN106967032A (zh) 2017-07-21
CN107158740A (zh) 2017-09-15
CN105130937B (zh) 2017-05-31

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Legal Events

Date Code Title Description
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Lin Huanxin

Inventor after: Zhang Senfeng

Inventor after: Other inventors request that names not be published

Inventor before: Request for anonymity

TA01 Transfer of patent application right

Effective date of registration: 20191122

Address after: 213000 No. 38 Hanjiang Road, Xinbei District, Changzhou City, Jiangsu Province

Applicant after: Ding Xueqiang

Address before: 213000 No. 38 Hanjiang Road, Xinbei District, Changzhou City, Jiangsu Province

Applicant before: Ge Yunlong

TA01 Transfer of patent application right
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20191219

Address after: 510080 No.13, Heyun Road, Jianggao Town, Baiyun District, Guangzhou City, Guangdong Province

Patentee after: Guangdong Xianglong flavor Co., Ltd

Address before: 213000 No. 38 Hanjiang Road, Xinbei District, Changzhou City, Jiangsu Province

Patentee before: Ding Xueqiang

CI03 Correction of invention patent

Correction item: Patentee|Address|Patent agency|Agent

Correct: Guangdong Xianglong flavor Co., Ltd|510080 No.13, Heyun Road, Jianggao Town, Baiyun District, Guangzhou City, Guangdong Province|Hangzhou Jubang Intellectual Property Agency Co., ltd.33269|Jiang Quanqiang

False: Ding Xueqiang|213000 No. 38 Hanjiang Road, Xinbei District, Changzhou City, Jiangsu Province|Hangzhou Jubang Intellectual Property Agency Co., ltd.33269|Zhou Meifeng

Number: 51-02

Page: The title page

Volume: 35

Correction item: Patentee|Address|Patent agency|Agent

Correct: Guangdong Xianglong flavor Co., Ltd|510080 No.13, Heyun Road, Jianggao Town, Baiyun District, Guangzhou City, Guangdong Province|Hangzhou Jubang Intellectual Property Agency Co., ltd.33269|Jiang Quanqiang

False: Ding Xueqiang|213000 No. 38 Hanjiang Road, Xinbei District, Changzhou City, Jiangsu Province|Hangzhou Jubang Intellectual Property Agency Co., ltd.33269|Zhou Meifeng

Number: 51-02

Volume: 35

CI03 Correction of invention patent