CN105755859A - Natural dye for textile and preparation method of natural dye - Google Patents
Natural dye for textile and preparation method of natural dye Download PDFInfo
- Publication number
- CN105755859A CN105755859A CN201610328127.5A CN201610328127A CN105755859A CN 105755859 A CN105755859 A CN 105755859A CN 201610328127 A CN201610328127 A CN 201610328127A CN 105755859 A CN105755859 A CN 105755859A
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- CN
- China
- Prior art keywords
- natural dye
- parts
- extract
- textile
- filtrate
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
Abstract
The invention discloses a natural dye for a textile. The natural dye comprises the following raw materials in parts by weight: 15-30 parts of a natural dye extract, 10-15 parts of xylitol, 5-10 parts of carboxymethyl chitosan, 2-5 parts of an organosilicone surface tension conditioning agent, 5-10 parts of hyaluronic acid, 1-4 parts of dyeing acid and 80-100 parts of deionized water. The natural dye is good in water solubility, bright in color, high in purity and fastness, soft and elegant in tone, and natural and environment-friendly, a dyed product has a certain antibacterial and antistatic performance, and also has a certain health effect, and besides plants are utilized as raw materials of the dye, so that energy can be saved, environment can be protected, the cost is low, material taking is convenient, and the production mode is simple.
Description
Technical field
The present invention relates to field of fabric producing technology, specifically a kind of textile natural dye and preparation method thereof.
Background technology
Along with the raising of people's living standard, gradually pursuing life taste, people had both pursued style and the effect of ready-made clothes, more pursue natural, ecological, allow harmony between man and nature develop.At present, the chemical dyestuff that dyeing is conventional has lovely luster, washable, sun-proof, the advantage that is prone to industrialized production, but chemical dyestuff dyeing length, equipment is many, energy consumption is high, and produce a large amount of contaminated wastewater environment, heavy damage ecological balance, additionally, partial synthesis dyestuff is possibly together with carcinogen.
Summary of the invention
Therefore, for solving the problems referred to above, the present invention provides a kind of textile natural dye, it is ensured that while dyestuff colouring power on yarn fabric and color homogeneity, also has, has excellent antibacterial and antistatic behaviour.
The technical solution used in the present invention is: a kind of textile natural dye, raw material including following weight portion: natural dye extract 15-30 part, xylitol 10-15 part, carboxymethyl chitosan 5-10 part, organosilyl surface tension regulator 2-5 part, hyaluronic acid 5-10 part, dyeing acid 1-4 part, deionized water 80-100 part.
Described natural dye extract includes one or more in Herba portulacae extract, Folium Camelliae sinensis extract or Rhizoma Curcumae Longae extract.
Described Herba portulacae extract, Folium Camelliae sinensis extract or Rhizoma Curcumae Longae extract are obtained by ultrasonic extraction or ultrasound wave, microwave combined extraction method.
The preparation method of above-mentioned textile natural dye, comprises the following steps:
(1) natural dye raw material is cleaned, with pure water as Extraction medium, the ultrasonic extraction equipment of 40KHZ processes 30min, ethanol extracts after 2-3 time, is filtrated to get filtrate, i.e. natural dye extract；
(2) xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) joining in the mixed liquor that step (2) obtains by the filtrate that step (1) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
The invention has the beneficial effects as follows: 1, the natural dye good water solubility of the present invention, bright-colored, purity is high, fastness is high, the soft elegance of tone, natural environmental-protective, containing carboxymethyl chitosan in dyestuff, make the product after dyeing have certain antibacterial and antistatic behaviour, also there is certain health-care effect.2, utilizing plant as the raw material of dyestuff, energy-conserving and environment-protective, low cost, draw materials conveniently, the mode of production is simple.
Detailed description of the invention
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment is only used for explaining the present invention, is not intended that limiting the scope of the present invention.
Embodiment 1
A kind of textile natural dye, including the raw material of following weight portion: Herba portulacae extract 15 parts, xylitol 15 parts, carboxymethyl chitosan 5 parts, organosilyl surface tension regulator 5 parts, hyaluronic acid 5 parts, dyeing acid 4 parts, deionized water 80 parts.
The preparation method of above-mentioned textile natural dye, comprises the following steps:
(1) choose new fresh Herba Portulacae raw material clean, with pure water as Extraction medium, the ultrasonic extraction equipment of 40KHZ processes 30min, ethanol extracts after 2-3 time, is filtrated to get filtrate；
(2) proportionally xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) filtrate that step (1) obtains being proportionally added into in the mixed liquor that step (2) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
Embodiment 2
A kind of textile natural dye, including the raw material of following weight portion: Folium Camelliae sinensis and Rhizoma Curcumae Longae extract 30 parts, xylitol 10 parts, carboxymethyl chitosan 10 parts, organosilyl surface tension regulator 2 parts, hyaluronic acid 10 parts, dyeing acid 1 part, deionized water
100 parts.
The preparation method of above-mentioned textile natural dye, comprises the following steps:
(1) choose fresh tea leaf and Rhizoma Curcumae Longae raw material is cleaned, with pure water as Extraction medium, after processing 30min in the ultrasonic extraction equipment of 40KHZ, again through frequency be the Microwave Extraction Equipment of 1250KHZ, extracting 15-20min during microwave radiation, extracting solution, through filtering, obtains filtrate；
(2) proportionally xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) filtrate that step (1) obtains being proportionally added into in the mixed liquor that step (2) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
Embodiment 3
A kind of textile natural dye, including the raw material of following weight portion: Rhizoma Curcumae Longae extract 20 parts, xylitol 12 parts, carboxymethyl chitosan 8 parts, organosilyl surface tension regulator 3 parts, hyaluronic acid 8 parts, dyeing acid 2 parts, deionized water 90 parts.
The preparation method of above-mentioned textile natural dye, comprises the following steps:
(1) choose fresh Rhizoma Curcumae Longae raw material to clean, with pure water as Extraction medium, after process 30min, ethanol extract 2-3 time in the ultrasonic extraction equipment of 40KHZ, be filtrated to get filtrate；
(2) proportionally xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) filtrate that step (1) obtains being proportionally added into in the mixed liquor that step (2) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
Embodiment 4
A kind of textile natural dye, including the raw material of following weight portion: Folium Camelliae sinensis extract 25 parts, xylitol 15 parts, carboxymethyl chitosan 10 parts, organosilyl surface tension regulator 4 parts, hyaluronic acid 9 parts, dyeing acid 4 parts, deionized water 90 parts.
The preparation method of above-mentioned textile natural dye, comprises the following steps:
(1) choose fresh tea leaf raw material to clean, with pure water as Extraction medium, after process 30min, ethanol extract 2-3 time in the ultrasonic extraction equipment of 40KHZ, be filtrated to get filtrate；
(2) proportionally xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) filtrate that step (1) obtains being proportionally added into in the mixed liquor that step (2) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
Claims (4)
1. a textile natural dye, it is characterised in that include the raw material of following weight portion:
Natural dye extract 15-30 part,
Xylitol 10-15 part,
Carboxymethyl chitosan 5-10 part,
Organosilyl surface tension regulator 2-5 part,
Hyaluronic acid 5-10 part,
Dyeing acid 1-4 part,
Deionized water 80-100 part.
A kind of textile natural dye the most according to claim 1, it is characterised in that described natural dye extract includes one or more in Herba portulacae extract, Folium Camelliae sinensis extract or Rhizoma Curcumae Longae extract.
A kind of textile natural dye the most according to claim 2, it is characterised in that described Herba portulacae extract, Folium Camelliae sinensis extract or Rhizoma Curcumae Longae extract are obtained by ultrasonic extraction or ultrasound wave, microwave combined extraction method.
The preparation method of a kind of textile natural dye the most according to claim 1, it is characterised in that: comprise the following steps
:
(1) natural dye raw material is cleaned, with pure water as Extraction medium, the ultrasonic extraction equipment of 40KHZ processes 30min, ethanol extracts after 2-3 time, is filtrated to get filtrate, i.e. natural dye extract；
(2) xylitol, carboxymethyl chitosan, organosilyl surface tension regulator, hyaluronic acid and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；
(3) joining in the mixed liquor that step (2) obtains by the filtrate that step (1) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder natural dye.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610328127.5A CN105755859A (en) | 2016-05-18 | 2016-05-18 | Natural dye for textile and preparation method of natural dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610328127.5A CN105755859A (en) | 2016-05-18 | 2016-05-18 | Natural dye for textile and preparation method of natural dye |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105755859A true CN105755859A (en) | 2016-07-13 |
Family
ID=56323129
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610328127.5A Pending CN105755859A (en) | 2016-05-18 | 2016-05-18 | Natural dye for textile and preparation method of natural dye |
Country Status (1)
| Country | Link |
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| CN (1) | CN105755859A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085971A (en) * | 2017-12-18 | 2018-05-29 | 吴安婕 | Antistatic combines liquid |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102041689A (en) * | 2010-12-30 | 2011-05-04 | 东华大学 | Application of natural dyes from balsamine in dyeing |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
| CN105421099A (en) * | 2015-11-30 | 2016-03-23 | 浙江辰鸿纺织品科技有限公司 | Method for dyeing dacron fabric through natural dye |
-
2016
- 2016-05-18 CN CN201610328127.5A patent/CN105755859A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102041689A (en) * | 2010-12-30 | 2011-05-04 | 东华大学 | Application of natural dyes from balsamine in dyeing |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
| CN105421099A (en) * | 2015-11-30 | 2016-03-23 | 浙江辰鸿纺织品科技有限公司 | Method for dyeing dacron fabric through natural dye |
Non-Patent Citations (1)
| Title |
|---|
| 王淑君: "《美容产品制剂学》", 28 February 2012 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085971A (en) * | 2017-12-18 | 2018-05-29 | 吴安婕 | Antistatic combines liquid |
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Application publication date: 20160713 |
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