CN105725128A - Preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials - Google Patents
Preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials Download PDFInfo
- Publication number
- CN105725128A CN105725128A CN201610113809.4A CN201610113809A CN105725128A CN 105725128 A CN105725128 A CN 105725128A CN 201610113809 A CN201610113809 A CN 201610113809A CN 105725128 A CN105725128 A CN 105725128A
- Authority
- CN
- China
- Prior art keywords
- microcrystalline cellulose
- preparation
- rhizoma amorphophalli
- cellulose
- microcapsule
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000168 Microcrystalline cellulose Polymers 0.000 title claims abstract description 36
- 235000019813 microcrystalline cellulose Nutrition 0.000 title claims abstract description 36
- 239000008108 microcrystalline cellulose Substances 0.000 title claims abstract description 36
- 229940016286 microcrystalline cellulose Drugs 0.000 title claims abstract description 36
- 239000003094 microcapsule Substances 0.000 title claims abstract description 32
- 239000000463 material Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 229920002752 Konjac Polymers 0.000 title abstract 4
- 235000013312 flour Nutrition 0.000 title abstract 4
- 235000013305 food Nutrition 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002002 slurry Substances 0.000 claims abstract description 11
- 238000001694 spray drying Methods 0.000 claims abstract description 10
- 239000007864 aqueous solution Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 239000002245 particle Substances 0.000 claims abstract description 3
- 239000000843 powder Substances 0.000 claims description 32
- 235000010980 cellulose Nutrition 0.000 claims description 9
- 229920002678 cellulose Polymers 0.000 claims description 9
- 239000001913 cellulose Substances 0.000 claims description 9
- 229920000609 methyl cellulose Polymers 0.000 claims description 7
- 239000001923 methylcellulose Substances 0.000 claims description 7
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 2
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims description 2
- 229940031574 hydroxymethyl cellulose Drugs 0.000 claims description 2
- -1 salt radical derivative of ethyl cellulose Chemical class 0.000 claims 1
- 235000013373 food additive Nutrition 0.000 abstract description 5
- 239000002778 food additive Substances 0.000 abstract description 5
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 238000009835 boiling Methods 0.000 abstract description 2
- 235000019640 taste Nutrition 0.000 abstract description 2
- 239000001856 Ethyl cellulose Substances 0.000 description 7
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 7
- 229920001249 ethyl cellulose Polymers 0.000 description 7
- 235000019325 ethyl cellulose Nutrition 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 5
- 206010010774 Constipation Diseases 0.000 description 3
- 239000002775 capsule Substances 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical group O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 230000002496 gastric effect Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 235000019890 Amylum Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 238000001976 enzyme digestion Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 210000004211 gastric acid Anatomy 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Processes Of Treating Macromolecular Substances (AREA)
- Jellies, Jams, And Syrups (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention provides a preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials. The preparation method comprises the following steps: (1) adding the konjaku flour into water, and dissolving at the temperature of 50 to 100 DEG C to prepare an aqueous solution; (2) adding food-grade microcrystalline cellulose of which the particle size is 80 to 600 meshes to the aqueous solution, stirring for 0.5 to 10 hours at the temperature of 30 to 100 DEG C, and homogenizing to obtain slurries; (3) carrying out spray drying on the slurries to obtain the microcrystalline cellulose microcapsules, wherein while spray drying, the inlet air temperature is 120 to 300 DEG C, and the outlet air temperature is 50 to 200 DEG C. With the adoption of the preparation method disclosed by the invention, when the microcrystalline cellulose microcapsules prepared by taking the konjaku flour as the wall materials are used as low-energy food additives, tastes and flavors of foods are not changed for boiling resistance and good toughness, the qualities of the foods are not affected when the addition amounts of the microcrystalline cellulose microcapsules are 10% to 50%, and the food energy can be reduced by 10% to 50%, so that the microcrystalline cellulose microcapsules can be used as main additives of slimming foods.
Description
Technical field
The present invention relates to a kind of microcrystalline Cellulose microcapsule preparation method being wall material with Rhizoma amorphophalli powder, belong to low-energy food additive agent field.
Background technology
Microcrystalline Cellulose microcapsule is critically important low-energy food additive, and the heat energy that food human consumption can be made to absorb reduces 10%-50%, thus reaches to reduce the purpose of population of being obese.
When doing cellulose microcapsule wall material (capsule leather material) with plant amylum, animals and plants capsule, because starch, animals and plants capsule can be made cellulose exposed out by gastric acid and enzymic digestion.Exposed fiber have the strongest water absorption, is likely to cause constipation as being eaten for a long time, and particularly old people more easily causes constipation.
Summary of the invention
It is an object of the invention to provide a kind of microcrystalline Cellulose microcapsule preparation method being wall material with Rhizoma amorphophalli powder, using the method can be effectively prevented from the ill effect of existing microcrystalline Cellulose microcapsule with the microcrystalline Cellulose microcapsule made, it specifically includes following steps:
(1) Rhizoma amorphophalli powder is added to the water, dissolves at 50-100 DEG C, make aqueous solution；
(2) particle diameter is added in above-mentioned aqueous solution at the food stage microcrystalline Cellulose of 80-600 mesh, at 30-100 DEG C, stir 0.5-10h, and homogeneous rear prepared slurry；
(3) above-mentioned slurry is spray-dried, obtains microcrystalline Cellulose microcapsule；During spray drying, inlet temperature 120 DEG C-300 DEG C, leaving air temp 50 DEG C-200 DEG C；
The microcrystalline Cellulose microcapsule made contains the Rhizoma amorphophalli powder of 0.1-5.0wt%.
Further, the one during above-mentioned food stage microcrystalline Cellulose is the salt radical derivative of methylcellulose, ethyl cellulose, hydroxylated cellulose, hydroxymethyl cellulose, ethoxy microcrystalline Cellulose and above-mentioned cellulose.These food stage microcrystalline Cellulose the most all have sale, it is convenient to obtain.
High pressure homogenizer or emulsifying cutter is used to carry out homogeneous in step (2).High pressure homogenizer or emulsifying cutter are homogeneous conventional equipment, do not repeat them here.
Owing to the main component of Rhizoma amorphophalli powder is glucomannoglycan, the gastrointestinal of people can not digest glucomannoglycan and the most not produce energy.Doing cellulose microcapsule wall material with Rhizoma amorphophalli powder, after people is edible, cellulose is in coated state all the time, avoiding problems the adverse side effect causing constipation.Rhizoma amorphophalli powder itself also has the effect of intestine moistening.Rhizoma amorphophalli powder containing 0.1-5.0wt% can form stable protective layer at the outer layer of microcrystalline Cellulose microcapsule, it is possible to ensures that microcapsule is the most digested at the gastrointestinal of people.
In the application, a preferred formula and preparation method are: add in 500 kg of water by 2 kilograms of Rhizoma amorphophalli powders, after dissolving 50min at 98 DEG C, add the food stage methylcellulose 98 kilograms of 400 mesh, 90min is stirred again at 60 DEG C, finally with the homogeneous 3-6min of high pressure homogenizer, prepare slurry, finally slurry is spray-dried, prepare the microcrystalline Cellulose microcapsule of moisture content 13%；During spray drying, inlet temperature 210 DEG C, leaving air temp 90 DEG C.
Microcapsule prepared by above-mentioned optimization formula has good taste and flavor, can meet the needs of most people to lose weight.
The microcrystalline Cellulose microcapsule being wall material with Rhizoma amorphophalli powder using the present invention to make, during as low-energy food additive, due to water boiling resistance, good toughness, will not change the mouthfeel of food, local flavor；Not affecting the quality of food during addition 10%-50%, the energy of food but can reduce 10%-50%, can be as the main additive of diet food.
Detailed description of the invention
Embodiment 1
Selecting food stage methyl microcrystalline Cellulose and commercial one-level Rhizoma amorphophalli powder is raw material.The microcrystalline Cellulose microcapsule made contains the food stage methylcellulose 95%-99.9%, one-level Rhizoma amorphophalli powder 0.1%-5.0% of 400 mesh.
Idiographic flow is: Rhizoma amorphophalli powder is dissolved in water, and 50 DEG C-100 DEG C dissolvings, dissolution time is 5min-10h；The water consumption dissolving Rhizoma amorphophalli powder is food stage methylcellulose and 3-10 times of Rhizoma amorphophalli powder gross mass.Stirring 0.5-10h after adding food stage methylcellulose at 30 DEG C-100 DEG C, carry out encystation reaction, reaction uses the homogeneous 3-6min of high pressure homogenizer after terminating, and obtains slurry.Remove moisture with spray drying method and obtain the microcrystalline Cellulose microcapsule being wall material with Rhizoma amorphophalli powder.
In this enforcement, concrete parameter is, food stage methylcellulose 98 kilograms, Rhizoma amorphophalli powder 2 kilograms, 500 kilograms of water；Rhizoma amorphophalli powder solution temperature 98 DEG C, dissolution time is 50min；Encystation reaction temperature 60 DEG C, time 90min；During spray drying, inlet temperature 210 DEG C, leaving air temp 90 DEG C, the moisture content 13% of microcrystalline Cellulose microcapsule finished product.
Embodiment 2:
With food stage ethyl cellulose and Rhizoma amorphophalli powder as raw material, food stage ethyl cellulose 95%-99.9%, one-level Rhizoma amorphophalli powder 0.1%-5.0% containing 100 mesh in the microcrystalline Cellulose microcapsule made.
Idiographic flow is: Rhizoma amorphophalli powder is dissolved in water, and 50 DEG C-100 DEG C dissolvings, dissolution time is 0.5-6h；The water consumption dissolving Rhizoma amorphophalli powder is food stage ethyl cellulose and 3-8 times of Rhizoma amorphophalli powder gross mass；Adding ethyl cellulose, high pressure homogenization 5-600min, then at 30-100 DEG C, carry out encystation reaction 10-240min, finally carry out being spray-dried and obtain the microcrystalline Cellulose microcapsule being wall material with Rhizoma amorphophalli powder, during spray drying, inlet temperature 120 DEG C-300 DEG C, leaving air temp 50 DEG C-200 DEG C.
In this enforcement, concrete parameter is, food stage ethyl cellulose 99.7 kilograms, Rhizoma amorphophalli powder 0.3 kilogram, 600 kilograms of water；Rhizoma amorphophalli powder solution temperature 96 DEG C, encystation reaction temperature 60 DEG C, time 60min；During spray drying, inlet temperature 190 DEG C, leaving air temp 85 DEG C, the moisture content 9.5% of microcrystalline Cellulose microcapsule finished product.
The microcrystalline Cellulose microcapsule made of ethyl cellulose and Rhizoma amorphophalli powder, as addition during low-energy food additive up to 10%-50%.
Claims (4)
1. the microcrystalline Cellulose microcapsule preparation method being wall material with Rhizoma amorphophalli powder, comprises the steps:
(1) Rhizoma amorphophalli powder is added to the water, dissolves at 50-100 DEG C, make aqueous solution；
(2) particle diameter is added in above-mentioned aqueous solution at the food stage microcrystalline Cellulose of 80-600 mesh, stir at 30-100 DEG C
0.5-10h, homogeneous rear prepared slurry；
(3) above-mentioned slurry is spray-dried, obtains microcrystalline Cellulose microcapsule；During spray drying, inlet temperature 120 DEG C
-300 DEG C, leaving air temp 50 DEG C-200 DEG C.
The microcrystalline Cellulose microcapsule made contains the Rhizoma amorphophalli powder of 0.1-5.0wt%.
Preparation method the most according to claim 1, it is characterised in that above-mentioned food stage microcrystalline Cellulose be methylcellulose,
The salt radical derivative of ethyl cellulose, hydroxylated cellulose, hydroxymethyl cellulose, ethoxy microcrystalline Cellulose and above-mentioned cellulose
In one.
Preparation method the most according to claim 1, it is characterised in that use high pressure homogenizer or emulsifying in step (2)
Cutter carries out homogeneous.
Preparation method the most according to claim 1, it is characterised in that 2 kilograms of Rhizoma amorphophalli powders are added in 500 kg of water,
After dissolving 50min at 98 DEG C, add the food stage methylcellulose 98 kilograms of 400 mesh, then at 60 DEG C, stir 90min,
Finally with the homogeneous 3-6min of high pressure homogenizer, prepare slurry, finally slurry is spray-dried, prepare the micro-of moisture content 13%
Crystalline cellulose microcapsule；During spray drying, inlet temperature 210 DEG C, leaving air temp 90 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610113809.4A CN105725128A (en) | 2016-02-29 | 2016-02-29 | Preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610113809.4A CN105725128A (en) | 2016-02-29 | 2016-02-29 | Preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105725128A true CN105725128A (en) | 2016-07-06 |
Family
ID=56248895
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610113809.4A Pending CN105725128A (en) | 2016-02-29 | 2016-02-29 | Preparation method of microcrystalline cellulose microcapsules by taking konjaku flour as wall materials |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105725128A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106723234A (en) * | 2016-12-05 | 2017-05-31 | 华侨大学 | A kind of device and its application method for preparing probiotic microcapsule |
| CN110447837A (en) * | 2019-09-24 | 2019-11-15 | 四川徽记食品股份有限公司 | A kind of tea polyphenols microcapsule preparation method for the processing of plain intestines |
| CN113940429A (en) * | 2021-11-08 | 2022-01-18 | 陕西师范大学 | Pomegranate peel residue polyphenol microcapsule and preparation method thereof |
| CN115349614A (en) * | 2022-08-15 | 2022-11-18 | 宝得瑞（湖北）健康产业有限公司 | Instant nutrient pumpkin powder with good stability and preparation method thereof |
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| CN101502305A (en) * | 2009-01-20 | 2009-08-12 | 北京大学 | Emulsion stabilizer for food and preparation method thereof |
| KR20130142760A (en) * | 2012-06-20 | 2013-12-30 | 한국식품연구원 | Kimchi flavor microcapsule, kimchi sauce composition comprising it and preparation method thereof |
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2016
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Patent Citations (7)
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106723234A (en) * | 2016-12-05 | 2017-05-31 | 华侨大学 | A kind of device and its application method for preparing probiotic microcapsule |
| CN106723234B (en) * | 2016-12-05 | 2019-04-09 | 华侨大学 | A kind of device preparing probiotic microcapsule and its application method |
| CN110447837A (en) * | 2019-09-24 | 2019-11-15 | 四川徽记食品股份有限公司 | A kind of tea polyphenols microcapsule preparation method for the processing of plain intestines |
| CN113940429A (en) * | 2021-11-08 | 2022-01-18 | 陕西师范大学 | Pomegranate peel residue polyphenol microcapsule and preparation method thereof |
| CN113940429B (en) * | 2021-11-08 | 2024-01-09 | 陕西师范大学 | Pomegranate rind residue polyphenol microcapsule and preparation method thereof |
| CN115349614A (en) * | 2022-08-15 | 2022-11-18 | 宝得瑞（湖北）健康产业有限公司 | Instant nutrient pumpkin powder with good stability and preparation method thereof |
| CN115349614B (en) * | 2022-08-15 | 2024-04-16 | 宝得瑞（湖北）健康产业有限公司 | Instant nutritional pumpkin powder with good stability and preparation method thereof |
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