CN105717086A - Frequency conversion control method for light source of atomic fluorescence spectrometer based on digital micro-mirror - Google Patents
Frequency conversion control method for light source of atomic fluorescence spectrometer based on digital micro-mirror Download PDFInfo
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
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- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N2021/6417—Spectrofluorimetric devices
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Abstract
The invention relates to a frequency conversion control method for a light source of an atomic fluorescence spectrometer based on a digital micro-mirror. The method includes the steps that at the collecting stage, high-frequency current and small direct current are used for controlling a hollow cathode lamp to work and controlling the digital micro-mirror to overturn at the same time; sampling is carried out in the lightened period of the hollow cathode lamp; at the non-collecting stage, low-frequency current and small direct current are used for controlling the hollow cathode lamp to work. According to the method, as low-frequency pulse current is added on the basis of small current preheating, the stability of the hollow cathode lamp can be improved, stabilization time can be shortened, multiple times of sampling can be carried out within the same time, the working efficiency of the instrument is improved, and the service life of the hollow cathode lamp can be prolonged. The method is suitable for frequency conversion control over a light source of a single-channel atomic fluorescence spectrometer with only one kind of elements capable of being detected at a time and also suitable for frequency conversion control over a light source of a multi-channel atomic fluorescence spectrometer with multiple kinds of elements capable of being detected at a time.
Description
Technical field
The invention belongs to atomic fluorescence spectrophotometry field, particularly relate to a kind of method for controlling frequency conversion being applicable to entirely compose atomic fluorescence spectrometer hollow cathode lamp based on digital micromirror array.
Background technology
As Novel atomic fluorescence spectrometer, entirely compose atomic fluorescence spectrometer based on digital micromirror array except including the air-channel system of original instrument, sampling system, hydride generating system, atomizer, igniter, hollow cathode lamp, photomultiplier tube etc., increase the dispersion system being made up of digital micro-mirror, dispersion harvester, light path, photomultiplier tube newly.The ground state atom generated by atomizer in above-mentioned spectrogrph produces fluorescence under the characteristic frequency radiation excitation of hollow cathode lamp, grating carries out light splitting, and digital micro-mirror selects particular spectral lines to pass through, photomultiplier tube detect, acquired device collection, carries out qualitative and quantitative analysis.
In prior art, working with constant frequency at acquisition phase hollow cathode lamp, non-acquired stage hollow cathode lamp only preheats under little DC current, and hollow cathode lamp is relatively long for stabilization time, make sampling number in the equal time relatively fewer, affect the work efficiency of instrument;Simultaneously because increase digital micro-mirror parts, control method before cannot realize gathering and synchronize, therefore a kind of method for controlling frequency conversion need to be invented and improve the stability of hollow cathode lamp, reduce hollow cathode lamp stabilization time and realize synchronous acquisition, not affecting the service life of hollow cathode lamp simultaneously.
So far there is no and apply low-frequency current pulses in the non-acquired stage and light the method for controlling frequency conversion of hollow cathode lamp, also not yet by the method and digital micro-mirror fit applications in atomic fluorescence spectrometer.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of preheating degree that can strengthen intrinsic small area analysis, improve hollow cathode lamp stability, reduce hollow cathode lamp response time the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror that hollow cathode lamp service life can be extended.
In order to solve above-mentioned technical problem, the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror of the present invention comprises the steps:
Step one, for element to be measured, the times of collection N of detection process is set, gather the once sampling number n in acquisition phase, the group number m (namely 1 sampling number lighted by hollow cathode lamp is m) of 1 digital micro-mirror upset lighted by hollow cathode lamp, often group digital micro-mirror columns q, the time t of one point of sampling2;
Step 2, in acquisition phase, controls hollow cathode lamp with high frequency electric and little DC current and starts working, control digital micro-mirror simultaneously and overturn;After hollow cathode lamp and digital micro-mirror are all stable, send signal to harvester and make it start fluorescence sampling;
It is as follows that 1 sampling control method lighted by hollow cathode lamp:
Every secondary control digital micro-mirror upset q row, harvester carries out fluorescence sampling;Sample count values i is added 1 after terminating by sampling;Judging the numerical value of i, if i is < m, then continue to light hollow cathode lamp, controlling digital micro-mirror upset, harvester carries out fluorescence sampling;If i=m, then making i=0, harvester sends sampling the finish command control hollow cathode lamp cut out simultaneously;So far, lighting of hollow cathode lamp terminates;
In acquisition phase, collection control method is as follows:
Hollow cathode lamp is lighted count value j and is added 1, it is judged that the numerical value of j while closing by each hollow cathode lamp: ifThen complete, after closedown duration, to repeat to light hollow cathode lamp, carry out fluorescent collecting until hollow cathode lamp;IfThen making j=0, acquisition phase completes, and starts the non-acquired stage;
Step 3, within the non-acquired stage, control hollow cathode lamp work with low-frequency current and little DC current, until this gatherer process terminates, times of collection count value s added 1;
Step 4, judge the numerical value of s, if s < N, then repeat step 2, three;If s=N, then complete the whole detection process of element to be measured.
The dutycycle of the high frequency electric of described acquisition phase is 1:k1, acquisition time is T1;The dutycycle of the low-frequency current in non-acquired stage is 1:k2, the non-acquired time is T2;K1、T1、k2, T2 meet formula (1):
Wherein k is the inverse that dutycycle demarcated by hollow cathode lamp.
Concrete, described acquisition time isWherein t0Stabilization time after turning on light for hollow cathode lamp, t1Stabilization time after overturning for digital micro-mirror.
Concrete, the frequency of described high frequency electricWherein t0Stabilization time after turning on light for hollow cathode lamp, t1Stabilization time after overturning for digital micro-mirror.
The average current of described high frequency electric isWherein, I1Current intensity when hollow cathode lamp is lighted is controlled for high frequency electric.
The average current of described low-frequency current isWhereinFor the intensity of the staking-out work electric current of hollow cathode lamp, I0Current intensity for little DC current;It is I that low-frequency current controls current intensity when hollow cathode lamp is lighted2,
The present invention is applicable to entirely compose atomic fluorescence spectrometer hollow cathode lamp method for controlling frequency conversion use when carrying out sample detection based on digital micromirror array, this technology can further improve the hollow cathode lamp stability in the non-acquired stage, research before shows, utilize the preheating of little DC current in the non-acquired stage and the stability of hollow cathode lamp can be improved compared with small area analysis preheating, so the present invention increases low frequency pulse current on the basis that small area analysis preheats, hollow cathode lamp can be preheated further, improve the stability of hollow cathode lamp, reduce its stabilization time, realize multiple repairing weld in the equal time, improve instrument work efficiency;And compared with the mode applying high frequency, heavy current pulse in whole gatherer process, greatly reduce the heavy current pulse impact to hollow cathode lamp, can increase the service life.According to different element hollow cathode lamp characteristics, light hollow cathode lamp at the adjustable high frequency of acquisition phase applying frequency, big electric current, high duty ratio Pulse Width Control electric current, improve fluorescence excitation efficiency.In addition, the method can coordinate entirely composes digital micro-mirror and the work schedule of harvester in atomic fluorescence spectrometer based on digital micromirror array, makes instrument efficient operation.The present invention is applicable not only to once can only to detect in the single channel atomic fluorescence spectrometer of a kind of element the VFC of light source, applies also for the VFC of light source in the Multicenter atomic fluorescence optical spectrometer that once can detect multiple element.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the present invention is described in further detail.
Fig. 1 is based on digital micromirror array and entirely composes the structural relation figure of the hollow cathode lamp of atomic fluorescence spectrometer, digital micro-mirror, harvester.
Fig. 2 a is the whole detection process schematic of sample;Fig. 2 b is a gatherer process schematic diagram;Fig. 2 c is that a gatherer process hollow cathode lamp controls process schematic;Fig. 2 d is that one sampled point of acquisition phase controls process schematic;Fig. 2 e is that non-acquisition phase hollow cathode lamp controls process schematic.
Fig. 3 is the control current diagram of gatherer process hollow core cathode modulation.
Fig. 4 is the full method flow diagram composing atomic fluorescence spectrometer hollow cathode lamp VFC of the present invention.
Detailed description of the invention
As shown in Figure 1, entirely compose atomic fluorescence spectrometer based on digital micromirror array and include atomizer, hollow cathode lamp, grating, digital micro-mirror, photomultiplier tube, harvester and host computer, wherein lighted by PC control hollow cathode lamp, control digital micro-mirror upset, and control harvester work.
As shown in Fig. 2 a~Fig. 2 c, one time sample detection process includes n times gatherer process, and one time gatherer process generates 1 width spectrogram, and symbiosis becomes N width spectrogram.Gatherer process is divided into acquisition phase, and (acquisition time is T1) and (the non-acquired time is T the non-acquired stage2).In acquisition phase with high frequency electric (for f1, dutycycle is 1:k1 to frequency) and little DC current I0Control hollow cathode lamp work, gather n sampled point;The non-acquired stage does not sample, with low-frequency current (for f2, dutycycle is 1:k2 to frequency) and little DC current I0Control hollow cathode lamp work.Wherein, N, n set according to the specific experiment of different elements to be measured.
As shown in Figure 2 d, hollow cathode lamp is often lighted once, controls digital micro-mirror upset m (m >=1) group, and often group comprises q (q >=1) column of figure micro mirror.Once m point of sampling often lighted by hollow cathode lamp, therefore when once adopting cluster sampling n point, need to light hollow cathode lampSecondary.Wherein, q, m set according to the specific experiment of different elements to be measured.
As shown in Figure 2 e, non-acquired stage hollow cathode lamp adopts dutycycle to be 1:k2, frequency is f2Low-frequency current and work low current (not shown) control.This stage digital micro-mirror and harvester do not work.
As it is shown on figure 3, the current intensity of acquisition phase is I1+I0, the current intensity in non-acquired stage is I2+I0, I0For little DC current, I1Current intensity when hollow cathode lamp is lighted, I is controlled for high frequency electric2Current intensity when hollow cathode lamp is lighted is controlled for low-frequency current.
Determination method for parameter:
In acquisition phase, hollow cathode lamp have after turning on light one section stabilization time t0, digital micro-mirror due to be machinery upset, also have after upset one section stabilization time t1, just can sample after hollow cathode lamp and digital micro-mirror are all stable, digital micro-mirror and hollow cathode lamp overlap stabilization time, can reduce the sampling period, improve instrument work efficiency.In acquisition phase, the time arranging one point of sampling is t2, then t0、t1、t2Determine lighting duration of hollow cathode lamp, for (t1+t2)(m-1)+(t0+t2), duration of turning off the light is (k1-1)[(t1+t2)(m-1)+(t0+t2)].Wherein t0、t1Determined by hollow cathode lamp and numeral micro-mirror structure, set t according to the specific experiment of different elements to be measured2。
Specific experiment according to different elements to be measured determines N, n, q, m.
Then the demarcation dutycycle 1:k according to hollow cathode lamp, the dutycycle 1:k of acquisition phase1, the dutycycle 1:k in non-acquired stage2, acquisition time T1With non-acquired time T2Relational expression (1) determine the scope of these parameters, first determine k again through experiment1、f2And T2Optimum.
T is determined according to formula (2)1Optimum;
F is determined according to formula (3)1Optimum;
The staking-out work electric current of hollow cathode lampRestriction acquisition phase average currentThe average current in non-acquired stageAnd small area analysis I0Span, namely
Little DC current I0All exist with fixed value in acquisition phase and non-acquired stage.By hollow cathode lamp principle it can be seen that operating currentMore little, hollow cathode lamp is more long for service life, and general hollow cathode lamp is demarcated average current and need to be met,I can be first determined by experiment according to the span of formula (4)1, determine further according to formula (5)I is determined according to formula (6) and formula (7)2。
The setting of above parameter, all the strongest the most surely for best to realize fluorescence intensity.
Wherein f1And 1:k1、f2And 1:k2Determine that hollow cathode lights duration at the lamp of acquisition phase and non-acquired stage respectively, there is certain impact in the service life of hollow cathode lamp, but non-principal affects;High frequency electric controls current intensity I when hollow cathode lamp is lighted1Ensureing to excite fluorescence intensity, low-frequency current controls current intensity I when hollow cathode lamp is lighted2With little DC current I0Improving the stability of hollow cathode lamp, three kinds of electric currents are the major effect in the service life of hollow cathode lamp.Controlling above six kinds of parameters makes hollow cathode lamp maximum for service life.
f1、1:k1、I1Fluorescent excitation intensity is guaranteed in acquisition phase;F2、1:k2、I2Improve fluorescent stability in the non-acquired stage, reduce its stabilization time, it is achieved multiple repairing weld in the equal time, improve instrument work efficiency.
All control pulses are Low level effective.
As shown in Figure 4, to realize step as follows for concrete grammar:
One, the sampling number n, sampling time t that gather once are set2, a lighting digital micro-mirror upset group number m, often group columns q, times of collection N, the HF current frequency f of hollow cathode lamp acquisition phase1, dutycycle 1:k1And high frequency electric controls current intensity I when hollow cathode lamp is lighted1, the low-frequency current frequency f in non-acquired stage2, dutycycle 1:k2, low-frequency current control hollow cathode lamp current intensity I when lighting2And working time T2, work end electric current I0;Setting sample count values i=0, hollow cathode lamp lights number of times evaluation number j=0, times of collection count value s=0;It is provided with, starts detection.
Two, the concrete grammar of 1 time lighted by acquisition phase hollow cathode lamp.
Digital micro-mirror receives after starting to detect instruction and overturns, and digital micro-mirror overturnsAfter, hollow cathode lamp starts with high frequency electric (frequency f1, dutycycle 1:k1, electric current I1) lighting, afterAfter, hollow cathode lamp and digital micro-mirror are all stable, send signal to harvester and make it start sampling, and sample t2After, once sampling terminates.Now the sample count values i in sample count module adds 1, judge sample count values i: if i is < m, represent that digital micro-mirror is not fully complete the upset of m group, then hollow cathode lamp continues with high frequency electric lighting, digital micro-mirror continues upset, and harvester continues sampling;If i=m, representing that digital micro-mirror has completed the upset of m group, then make i=0, the sampling the finish command of harvester transmission simultaneously controls hollow cathode lamp and closes.So far, lighting of hollow cathode lamp terminates.
Three, acquisition phase controls the concrete grammar of hollow cathode lamp
While step 2 hollow core cathode modulation is closed, hollow cathode lamp is lighted the hollow cathode lamp of counting how many times module and is lighted number of times evaluation number j and add 1, it is judged that the value of j: ifRepresent the collection being not fully complete n sampled point, then complete, after closedown duration, to repeat step 2 and control hollow cathode lamp until hollow cathode lamp;IfRepresenting that n sampling number collection completes, hollow cathode lamp is lightedSecondary complete, namely acquisition phase completes, and starts the non-acquired stage.
Four, the concrete grammar of non-acquired stage control hollow cathode lamp
After step 3 is finished, make j=0, make hollow cathode lamp with low-frequency current (dutycycle 1:k simultaneously2, frequency f2) at non-acquired stage work T2。T2The rear gatherer process that is finished terminates.
Five, the concrete grammar of n times acquisition controlling hollow cathode lamp is completed
After in step 4, a gatherer process terminates, the times of collection count value s in times of collection counting module three adds 1, it is judged that the value of s: if s < N, then repeats step 2, three, four carry out multi collect;If s=N, then whole detection process terminates, and waits sample detection next time.
Claims (6)
1. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror, it is characterised in that comprise the steps:
Step one, for element to be measured, the times of collection N of detection process is set, gathers the once sampling number n in acquisition phase, the group number m of 1 digital micro-mirror upset lighted by hollow cathode lamp, often group digital micro-mirror columns q, the time t of one point of sampling2;
Step 2, in acquisition phase, controls hollow cathode lamp with high frequency electric and little DC current and starts working, control digital micro-mirror simultaneously and overturn;After hollow cathode lamp and digital micro-mirror are all stable, send signal to harvester and make it start fluorescence sampling;
It is as follows that 1 sampling control method lighted by hollow cathode lamp:
Every secondary control digital micro-mirror upset q row, harvester carries out fluorescence sampling;Sample count values i is added 1 after terminating by sampling;Judging the numerical value of i, if i is < m, then continue to light hollow cathode lamp, controlling digital micro-mirror upset, harvester carries out fluorescence sampling;If i=m, then making i=0, harvester sends sampling the finish command control hollow cathode lamp cut out simultaneously;So far, lighting of hollow cathode lamp terminates;
In acquisition phase, collection control method is as follows:
Hollow cathode lamp is lighted count value j and is added 1, it is judged that the numerical value of j while closing by each hollow cathode lamp: ifThen complete, after closedown duration, to repeat to light hollow cathode lamp, carry out fluorescent collecting until hollow cathode lamp;IfThen making j=0, acquisition phase completes, and starts the non-acquired stage;
Step 3, within the non-acquired stage, control hollow cathode lamp work with low-frequency current and little DC current, until this gatherer process terminates, times of collection count value s added 1;
Step 4, judge the numerical value of s, if s < N, then repeat step 2, three;If s=N, then complete the whole detection process of element to be measured.
2. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror according to claim 1, it is characterised in that the dutycycle of the high frequency electric of described acquisition phase is 1:k1, acquisition time is T1;The dutycycle of the low-frequency current in non-acquired stage is 1:k2, the non-acquired time is T2;K1、T1、k2, T2 meet formula (1):
Wherein k is the inverse that dutycycle demarcated by hollow cathode lamp.
3. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror according to claim 2, it is characterised in that described acquisition time isWherein t0Stabilization time after turning on light for hollow cathode lamp, t1Stabilization time after overturning for digital micro-mirror.
4. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror according to claim 2, it is characterised in that the frequency of described high frequency electricWherein t0Stabilization time after turning on light for hollow cathode lamp, t1Stabilization time after overturning for digital micro-mirror.
5. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror according to claim 2, it is characterised in that the average current of described high frequency electric is Wherein, I1Current intensity when hollow cathode lamp is lighted is controlled for high frequency electric.
6. the atomic fluorescence spectrometer light source method for controlling frequency conversion based on digital micro-mirror according to claim 5, it is characterised in that the average current of described low-frequency current is WhereinFor the intensity of the staking-out work electric current of hollow cathode lamp, I0Current intensity for little DC current;It is I that low-frequency current controls current intensity when hollow cathode lamp is lighted2,
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