CN105661618A - Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems - Google Patents
Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems Download PDFInfo
- Publication number
- CN105661618A CN105661618A CN201610166679.0A CN201610166679A CN105661618A CN 105661618 A CN105661618 A CN 105661618A CN 201610166679 A CN201610166679 A CN 201610166679A CN 105661618 A CN105661618 A CN 105661618A
- Authority
- CN
- China
- Prior art keywords
- water
- papermaking
- ash content
- reconstituted tobaccos
- swollen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Abstract
The invention discloses a method for improving the retention rate and the ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems and belongs to the technical field of papermaking-process reconstituted tobacco leaves. The method comprises the following steps: selecting the particle stems with the size of 20 meshes to 100 meshes as a filler adsorbent; expanding the particle stems with water at 20 DEG C to 70 DEG C; after expansion, mixing the particle stems with fillers; after uniformly mixing, washing the mixture with the water and drying to prepare a water and expanded stem mixture; then adding the prepared water and expanded stem mixture into coating liquid and/or paste; then preparing the papermaking-process reconstituted tobacco leaves by adopting a traditional method. The method disclosed by the invention is used for a papermaking-process reconstituted tobacco leaf production technology and the retention rate of the fillers and the ash content of the product can be improved, so that the comprehensive quality and yield of the reconstituted tobacco leaf products are improved. The method is simple to operate, has no pollution and is easily industrialized.
Description
Technical field
The invention belongs to papermaking-method reconstituted tobaccos field, it is specifically related to a kind of method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content.
Background technology
Papermaking-method reconstituted tobaccos fully utilizes the most effective mode of tobacco waste (offal, fragment, broken silk, offal, discarded tobacco leaf etc.) at present, and product is used in cigarette composition also have significant lowering harm and decreasing coking, strengthening style and features, improves product quality stability, reduces significance and the value such as production consumption. Domestic papermaking-method reconstituted tobaccos has now become one of important raw material of Chinese style cigarette.
In papermaking-method reconstituted tobaccos, filler adds the ash content that can improve papermaking-method reconstituted tobaccos and improves other physicalies. At present, the filler selected is calcium carbonate, but due to its particle diameter little, run off serious at web part of paper machine, cause finished product ash content on the low side, and ash content is on the low side brings the problems such as appearance property variation.
The production of papermaking-method reconstituted tobaccos often adds the retention that retention aid improves calcium carbonate, and improves ash content. In view of papermaking-method reconstituted tobaccos is sucking the particular requirement of secure context, selected retention aid must be nontoxic, and does not affect suction quality. Some synthesis retention aids conventional in papermaking, such as PAM etc., owing to considering security, therefore can not use it among papermaking-method reconstituted tobaccos production. In the production of current reconstituted tobacco, conventional guar gum and chitosan are as retention aid, though improve retention and the ash content of calcium carbonate, if but improving addition and can bring the problems such as evenness reduction, suction quality decline and production cost increase. Given this, it is necessary to a kind of method developing effective, simple, safety and easy raising papermaking-method reconstituted tobaccos filler retention and ash content is most important.
The method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content have not been reported.
Summary of the invention
It is an object of the invention to solve the deficiencies in the prior art, it is provided that a kind of method of effective, simple, safe and easy raising papermaking-method reconstituted tobaccos filler retention and ash content.The present invention, by the swollen stalk mixture that adds the water of preparation in coating fluid and/or slurry, improves filler retention and ash content in the production of papermaking-method reconstituted tobaccos, thus improves the integrated quality of reconstituted tobacco product.
The object of the present invention is achieved by the following technical programs:
Utilize granule peduncle to improve a method for papermaking-method reconstituted tobaccos filler retention and ash content, comprise the steps:
Step (1), immerses granule peduncle in 20-70 DEG C of water to its abundant water-swelling, is prepared into the swollen stalk of water;
Step (2), mixes the swollen stalk of water obtained for step (1) than for 1:0.5-2 by exhausted amount of dry matter with filler, after mixing, is washed to washing lotion colourless, then at 104-106 DEG C, is dried to constant weight, obtain the swollen stalk mixture of water;
Step (3), adds in coating fluid and/or slurry by the swollen stalk mixture of water that step (2) is obtained, then adopts traditional method to make papermaking-method reconstituted tobaccos;
Wherein, when being added in coating fluid by swollen for water stalk mixture, the quality of interpolation is the 5-15% of coating fluid quality;
When being added in slurry by swollen for water stalk mixture, the quality of interpolation is the 5-15% of stock quality;
Described coating fluid and slurry are conventional products used in existing papermaking-method reconstituted tobaccos production process;
Described filler is calcium carbonate conventional in existing papermaking-method reconstituted tobaccos production process.
Further, it is preferred that described granule peduncle particle diameter 20-100 order.
Further, it is preferred that the granule peduncle water-immersed time described in step (1) is 28-32 minute
Further, it is preferred that the granule peduncle water-immersed time described in step (1) is 30 minutes.
Further, it is preferred that the time that step (2) is washed is 5-10 minute.
Further, it is preferred that after step (2) washing, dry temperature is 105 DEG C.
Further, it is preferred that after step (2) washing, the dry time is 29-31 minute.
The swollen stalk mixture of the water of preparation of the present invention can suspend in coating fluid and evenly disperse, and when drying, mixture does not come off.
Compared with prior art, the invention has the beneficial effects as follows:
(1) the present invention selects granule peduncle to be filling adsorption agent; it is immersed in the water and makes it expand; mix with a certain amount of filler after expanding; evenly rear washing to be mixed, drying; it is prepared into the swollen stalk mixture of water; adding in coating fluid and/or slurry by swollen for obtained water stalk mixture, other process procedure is consistent with traditional method. With traditional method ratio, after adopting present method, the filler retention in reconstituted tobacco production and product ash content can distinguish at least raising 5-15% and 5-10%, thus improve integrated quality and the yield of reconstituted tobacco product.
(2) the inventive method is simple to operate, it is not necessary to add any harmful chemical assistant, safety and environmental protection, easy industrialization.
Accompanying drawing explanation
Fig. 1 is the electron-microscope scanning comparison diagram (1000X) of control sample 1;
Fig. 2 is the electron-microscope scanning comparison diagram (1000X) of experiment sample 1.
Wherein, the scale on Fig. 1 and Fig. 2 is equally divided into 4 sections, and overall length 120 μm, the height on Fig. 1 and Fig. 2 is 241 μm.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that, the following example is only for illustration of the present invention, and should not be considered as limiting the scope of the present invention. Unreceipted concrete technology or condition person in embodiment, according to the technology described by the document in this area or condition or carry out according to product description.The unreceipted production firm person of agents useful for same, product or instrument, is the conventional products that can obtain by buying.
Embodiment 1
Utilize granule peduncle to improve a method for papermaking-method reconstituted tobaccos filler retention and ash content, comprise the steps:
Step (1), immerses granule peduncle in 20 DEG C of water 32 minutes, is prepared into the swollen stalk of water; Described granule peduncle particle diameter 20-100 order;
Step (2), mixes the swollen stalk of water obtained for step (1) than for 1:0.5 by exhausted amount of dry matter with filler, after mixing, washes 5 minutes, and 104 DEG C of dryings obtain the swollen stalk mixture of water to constant weight in 29 minutes;
Step (3), adds in coating fluid and/or slurry by the swollen stalk mixture of water that step (2) is obtained, adopts traditional method to make papermaking-method reconstituted tobaccos;
Wherein, when being added in coating fluid by swollen for water stalk mixture, the quality of interpolation is the 15% of coating fluid quality;
When being added in slurry by swollen for water stalk mixture, the quality of interpolation is the 15% of stock quality;
Described coating fluid and slurry are conventional products used in existing papermaking-method reconstituted tobaccos production process;
Described filler is calcium carbonate conventional in existing papermaking-method reconstituted tobaccos production process.
Embodiment 2
Utilize granule peduncle to improve a method for papermaking-method reconstituted tobaccos filler retention and ash content, comprise the steps:
Step (1), immerses granule peduncle in 70 DEG C of water 28 minutes, is prepared into the swollen stalk of water; Described granule peduncle particle diameter 20-100 order;
Step (2), mixes the swollen stalk of water obtained for step (1) than for 1:2 by exhausted amount of dry matter with filler, after mixing, washes 10 minutes, and 106 DEG C of dryings obtain the swollen stalk mixture of water to constant weight in 31 minutes;
Step (3), adds in coating fluid and/or slurry by the swollen stalk mixture of water that step (2) is obtained, then adopts traditional method to make papermaking-method reconstituted tobaccos;
Wherein, when being added in coating fluid by swollen for water stalk mixture, the quality of interpolation is the 5% of coating fluid quality;
When being added in slurry by swollen for water stalk mixture, the quality of interpolation is the 5% of stock quality;
Described coating fluid and slurry are conventional products used in existing papermaking-method reconstituted tobaccos production process;
Described filler is calcium carbonate conventional in existing papermaking-method reconstituted tobaccos production process.
Embodiment 3
Utilize granule peduncle to improve a method for papermaking-method reconstituted tobaccos filler retention and ash content, comprise the steps:
Step (1), immerses granule peduncle in 50 DEG C of water 30 minutes, is prepared into the swollen stalk of water; Described granule peduncle particle diameter 20-100 order;
Step (2), mixes the swollen stalk of water obtained for step (1) than for 1:1 by exhausted amount of dry matter with filler, after mixing, washes 8 minutes, and 105 DEG C of dryings obtain the swollen stalk mixture of water to constant weight in 30 minutes;
Step (3), adds in coating fluid and/or slurry by the swollen stalk mixture of water that step (2) is obtained, adopts traditional method to make papermaking-method reconstituted tobaccos;
Wherein, when being added in coating fluid by swollen for water stalk mixture, the quality of interpolation is the 10% of coating fluid quality;
When being added in slurry by swollen for water stalk mixture, the quality of interpolation is the 10% of stock quality;
Described coating fluid and slurry are conventional products used in existing papermaking-method reconstituted tobaccos production process;
Described filler is calcium carbonate conventional in existing papermaking-method reconstituted tobaccos production process.
Embodiment 4
Granule peduncle immerses in 50 DEG C of water 30 minutes, is prepared into the swollen stalk of water;Described granule peduncle particle diameter 20-100 order; Swollen for obtained water stalk and filler being mixed than for 1:2 by exhausted amount of dry matter, mix and blend, after 10 minutes, is washed to colourless, and 105 DEG C of dryings obtain the swollen stalk mixture of water to constant weight in 30 minutes. Survey its dry weight and ash content, it is designated as experiment sample 1;
Not filled sample 1 in contrast, measures its ash content in addition.
Result shows, the ash content of the ash rate control sample 1 of experiment sample 1 improves 8.7%. Also can find out that filler-calcium carbonate is embedded in granule peduncle aperture preferably by electron-microscope scanning result, as depicted in figs. 1 and 2.
Embodiment 5
Carry out solid-liquid separation after being extracted in a conventional manner by tobacco material, tobacco liquid portion carries out refining, concentrated and reinforced after make coating fluid, coating fluid is divided into two parts.
When being joined in one part of coating fluid by the swollen stalk mixture of water of experiment sample 1, the quality of interpolation is the 5% of coating fluid quality, coats on corresponding sheet base after mixing, and the sheet base after coating balances 24h after drying, and is designated as experiment sample 2;
Another part of coating fluid does not add water swollen stalk mixture, and other and the present embodiment aforesaid method do identical process, and the product obtained is designated as control sample 2.
Measure filler retention and the ash content of control sample 2 and experiment sample 2 respectively. Result shows that the filler retention of experiment sample 2 and ash content contrast control sample 2 improve 7.3% and 6.5% respectively.
Embodiment 6
Carry out solid-liquid separation after conventionally being extracted by tobacco material, tobacco liquid portion carries out refining, concentrated and reinforced after make coating fluid. Adding the swollen stalk mixture of water that quality is its experiment sample 1 of 10% in the slurry, stir, manufacture paper with pulp shaping, be coated with and prepare sample, the sheet base after coating balances 24h after drying, and is designated as experiment sample 3;
Other one part except the swollen stalk mixture that do not add water, all the other and the present embodiment aforesaid method do identical process, and the product obtained is designated as control sample 3.
Measure filler retention and the ash content of control sample 3 and experiment sample 3 respectively. Result shows that the filler retention of experiment sample 3 and ash content contrast control sample 3 improve 8.2% and 6.9% respectively.
Embodiment 7
Carry out solid-liquid separation after conventionally being extracted by tobacco material, tobacco liquid portion carries out refining, concentrated and reinforced after make coating fluid, the swollen stalk mixture of water of experiment sample 1 is added in coating fluid, the quality of interpolation is the 5% of coating fluid quality, mixes. Meanwhile, adding in slurry by the swollen stalk mixture of water of experiment sample 1, the quality of interpolation is the 5% of stock quality, mixes; Slurry is manufactured paper with pulp shaping, is coated with and prepares sample, and the sheet base after coating balances 24h after drying, and is designated as experiment sample 4;
Except the swollen stalk mixture that do not add water, all the other and the present embodiment aforesaid method do identical process, and the product obtained is designated as control sample 4.
Measure filler retention and the ash content of control sample 4 and experiment sample 4 respectively. Result shows that the filler retention of experiment sample 4 and ash content contrast control sample 4 improve 10.5% and 7.8% respectively.
Claims (7)
1. one kind utilizes the method for granule peduncle raising papermaking-method reconstituted tobaccos filler retention and ash content, it is characterised in that, comprise the steps:
Step (1), immerses granule peduncle in 20-70 DEG C of water to its abundant water-swelling, is prepared into the swollen stalk of water;
Step (2), mixes the swollen stalk of water obtained for step (1) than for 1:0.5-2 by exhausted amount of dry matter with filler, after mixing, is washed to washing lotion colourless, then at 104-106 DEG C, is dried to constant weight, obtain the swollen stalk mixture of water;
Step (3), adds in coating fluid and/or slurry by the swollen stalk mixture of water that step (2) is obtained, then adopts traditional method to make papermaking-method reconstituted tobaccos;
Wherein, when being added in coating fluid by swollen for water stalk mixture, the quality of interpolation is the 5-15% of coating fluid quality;
When being added in slurry by swollen for water stalk mixture, the quality of interpolation is the 5-15% of stock quality;
Described coating fluid and slurry are conventional products used in existing papermaking-method reconstituted tobaccos production process;
Described filler is calcium carbonate conventional in existing papermaking-method reconstituted tobaccos production process.
2. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 1, it is characterised in that, described granule peduncle particle diameter 20-100 order.
3. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 1, it is characterised in that, the granule peduncle water-immersed time described in step (1) is 28-32 minute.
4. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 3, it is characterised in that, the granule peduncle water-immersed time described in step (1) is 30 minutes.
5. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 1, it is characterised in that, the time of the washing described in step (2) is 5-10 minute.
6. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 1, it is characterised in that, after step (2) washing, dry temperature is 105 DEG C.
7. the method utilizing granule peduncle to improve papermaking-method reconstituted tobaccos filler retention and ash content according to claim 1, it is characterised in that, after step (2) washing, the dry time is 29-31 minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610166679.0A CN105661618B (en) | 2016-03-22 | 2016-03-22 | Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610166679.0A CN105661618B (en) | 2016-03-22 | 2016-03-22 | Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105661618A true CN105661618A (en) | 2016-06-15 |
| CN105661618B CN105661618B (en) | 2017-05-10 |
Family
ID=56311542
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610166679.0A Active CN105661618B (en) | 2016-03-22 | 2016-03-22 | Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105661618B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393544A (en) * | 2018-12-21 | 2019-03-01 | 四川中烟工业有限责任公司 | A method of promoting reconstituted tobacco bulk and its aroma component |
| CN113712239A (en) * | 2021-09-07 | 2021-11-30 | 河北中烟工业有限责任公司 | Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5322076A (en) * | 1992-02-06 | 1994-06-21 | R. J. Reynolds Tobacco Company | Process for providing tobacco-containing papers for cigarettes |
| CN103798949A (en) * | 2014-03-11 | 2014-05-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of modified particles for recombinant tobacco leaves |
| CN103919271A (en) * | 2014-04-18 | 2014-07-16 | 湖北中烟工业有限责任公司 | Method for improving calcium carbonate retention rate through adding calcium carbonate before pulp beating |
| CN104770853A (en) * | 2015-04-21 | 2015-07-15 | 奚程 | Production method for tobacco sheet |
| CN105011346A (en) * | 2015-08-04 | 2015-11-04 | 湖南中烟工业有限责任公司 | Method for preparing reconstituted cut tobacco sheets |
-
2016
- 2016-03-22 CN CN201610166679.0A patent/CN105661618B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5322076A (en) * | 1992-02-06 | 1994-06-21 | R. J. Reynolds Tobacco Company | Process for providing tobacco-containing papers for cigarettes |
| CN103798949A (en) * | 2014-03-11 | 2014-05-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of modified particles for recombinant tobacco leaves |
| CN103919271A (en) * | 2014-04-18 | 2014-07-16 | 湖北中烟工业有限责任公司 | Method for improving calcium carbonate retention rate through adding calcium carbonate before pulp beating |
| CN104770853A (en) * | 2015-04-21 | 2015-07-15 | 奚程 | Production method for tobacco sheet |
| CN105011346A (en) * | 2015-08-04 | 2015-11-04 | 湖南中烟工业有限责任公司 | Method for preparing reconstituted cut tobacco sheets |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393544A (en) * | 2018-12-21 | 2019-03-01 | 四川中烟工业有限责任公司 | A method of promoting reconstituted tobacco bulk and its aroma component |
| CN109393544B (en) * | 2018-12-21 | 2022-04-05 | 四川中烟工业有限责任公司 | Method for improving bulk and aroma components of reconstituted tobacco |
| CN113712239A (en) * | 2021-09-07 | 2021-11-30 | 河北中烟工业有限责任公司 | Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105661618B (en) | 2017-05-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103266536B (en) | Preparation method and use of paper surface sizing agent | |
| CN103653233B (en) | A kind of method improving papermaking-method reconstituted tobaccos ash content | |
| CN105614942B (en) | A kind of method for the retention for improving papermaking-method reconstituted tobaccos piece based filler | |
| CN104705775A (en) | Preparation and application for paper-making process reconstituted tobacco sizing agent coated with calcium carbonate | |
| CN103859576A (en) | Method for improving retention of sizing agent fiber and filler in production of tobacco sheets through paper-making process | |
| CN102966002B (en) | Preparation of enhancer for nanofiber whisker paper and application method of enhancer to coating of paper-making tobacco sheets | |
| CN104005256A (en) | Raw tipping paper for waterproof and safe cigarettes and preparation method thereof | |
| CN105661618A (en) | Method for improving retention rate and ash content of papermaking-process reconstituted tobacco leaf fillers by using particle stems | |
| CN106495569A (en) | A kind of multi-functional zeolite environment protection interior wall wall material and construction method | |
| CN108677592A (en) | A kind of paper for daily use pulping process having both intensity and pliability | |
| CN105686056B (en) | It is a kind of to be used to improve swollen stalk product of water of papermaking-method reconstituted tobaccos filling adsorption performance and preparation method and application | |
| CN101283837A (en) | Cigarette flavouring process, flavouring reconstruction tobacco and preparation method thereof | |
| CN106522020B (en) | A kind of bamboo base filter stick for cigarettes forming paper and preparation method thereof | |
| CN110150720A (en) | The method for preparing Chinese style flue-cured tobacco type reconstituted tobacco based on suncured tabacco type tobacco material | |
| CN105077555B (en) | A kind of processing method of papermaking-method reconstituted tobaccos | |
| CN104005259A (en) | Highly-breathable flame-retardant tipping base paper and preparation method thereof | |
| CN104256881B (en) | A kind of leaf of bamboo pars fibrosa substitutes the method that reconstituted tobacco prepared by wood pulp cellulose | |
| CN107034712B (en) | A kind of novel papermaking method | |
| CN108219708A (en) | A kind of preparation method of environmental protection glutinous rice glue | |
| CN103849173B (en) | A kind of preparation method of moisture absorption humectation type filler and the application in papermaking-method reconstituted tobaccos is produced thereof | |
| CN104223344B (en) | A kind of be fibrous raw material with discarded gunnysack reconstituted tobacco preparation method | |
| CN105146716A (en) | Method of increasing calcium carbonate retention in paper-making reconstituted tobacco | |
| CN102934836A (en) | Method for improving filtering efficiency of tobacco powder extracting solution during production of tobacco sheets through paper-making process | |
| CN105077554B (en) | A kind of method improving papermaking-method reconstituted tobaccos slurry retention | |
| CN104957749A (en) | Method for increasing retention rate of sizing agent in paper-making reconstituted tobacco |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |